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lj337219286

银虫 (小有名气)

[求助] 急求 微谱求助 已有1人参与

一.C谱数据

     化学位移:175.7,174.2,172.6,172.2,171.2,170.1,138.6,137.0,130.9,   
     130.8,130.2,129.5,128.9,127.8,62.8,62.5,56.5,56.2,47.9,47.7,
     44.5,42.9,38.8,38.5,32.0,30.9,30.1,26.4,22.9


                  谢谢

[ Last edited by 卓越_先锋 on 2015-5-5 at 18:24 ]
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笑多会怀孕

铁杆木虫 (著名写手)

格式不对

» 本帖已获得的红花(最新10朵)

2楼2015-05-05 12:22:07
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lj337219286

银虫 (小有名气)

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送红花一朵
卓越_先锋: 金币-5, 注意发帖格式,微谱求助请到 分类微谱求助发帖 2015-05-05 18:23:15
引用回帖:
2楼: Originally posted by 笑多会怀孕 at 2015-05-05 12:22:07
格式不对

嗯 是不是数值与数值应该用英文状态下的符号 谢谢你哈
3楼2015-05-05 14:55:41
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sydong

铁杆木虫 (著名写手)

【答案】应助回帖

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感谢参与,应助指数 +1
lj337219286: 金币+15 2015-05-05 18:37:07
查询结果:共查到20个化合物(查询结果仅供参考)
1 .     dianthin F
C30H37N5O5     相似度:72.4%
Journal of Natural Products          2004          67          1522-1527
New Cytotoxic Cyclic Peptides and Dianthramide from Dianthus superbus
Pei-Wen Hsieh, Fang-Rong Chang, Ching-Chung Wu,Kuen-Yuh Wu, Chien-Ming Li, Su-Li Chen, and Yang-Chang Wu
Structure      13C NMR   碳谱模拟图
2 .     Cyclo(-L-tyrosinyl-L-phenylalanyl-L-prolyl-glycyl-L-leucyl-L-prolyl-)
C36H46N6O7     相似度:70.9%
Journal of Medicinal Plants Research          2010          4          1960-1966
Synthetic and pharmacological studies on a natural cyclopeptide from Gypsophila Arabica
Rajiv Dahiya and Hemendra Gautam
Structure      13C NMR   碳谱模拟图
3 .     segelin I
C39H44N6O7     相似度:69.6%
Phytochemistry Letters          2015          11          240−244
A new diantheramide and a new cyclic peptide from the seeds of Vaccaria hispanica
Meng-Fei Zheng, Hui Ren, Ying Luo, Li-Mei Dong, Ling-Qiong Wang, Zhong-Yu Zhou, Jian-Wen Tan
Structure      13C NMR   碳谱模拟图
4 .     cyclosquamosin A
C31H43N708     相似度:68.9%
Tetrahedron          1999          55          7509-7518
Cyclosquamosins A - G, cyclic peptides from the seeds of Annona squamosa
Hiroshi Morita, Yumiko Sato, Jun'ichi Kobayashi
Structure      13C NMR   碳谱模拟图
5 .     yunnanin A
C34H42N7O8     相似度:66.6%
Chemistry Letters          1994          23          2415-2418
Two Novel Cyclic Peptides, Yunnanins A and B from Stellaria yunnanensis
Hiroshi Morita, Akira Shishido, Takashi Kayashita, Masako Shimomura, Koichi Takeya and Hideji Itokawa
Structure      13C NMR   碳谱模拟图
6 .     cyclo(pro-(R)-β3hVal-(R)-Orn-(R)-β2hLeu-(R)-Phe)2
C64H100N12O10     相似度:66.6%
Chemistry & Biodiversity          2012          9          2494-2506
Synthesis and Biological Evaluation of Gramicidin S-Inspired Cyclic Mixed /β-Peptides
Matthijs van der Knaap, Fatih Basalan, Henny C. van de Mei, Henk J. Busscher, Gijsbert A. van der Marel, Herman S. Overkleeft and Mark Overhand
Structure      13C NMR   碳谱模拟图
7 .     dianthin B
C36H46N6O6     相似度:65.6%
Phytochemistry          1998          49          1453-1456
Cyclopeptides from dianthus superbus
You-Chu Wang, Ning-Hua Tan, Jun Zhou, Hou-Ming Wu
Structure      13C NMR   碳谱模拟图
8 .     cyclo(pro-(S)-β2hVal-Orn-(R)-β3hLeu-(R)-Phe)2
C64H100N12O10     相似度:63.3%
Chemistry & Biodiversity          2012          9          2494-2506
Synthesis and Biological Evaluation of Gramicidin S-Inspired Cyclic Mixed /β-Peptides
Matthijs van der Knaap, Fatih Basalan, Henny C. van de Mei, Henk J. Busscher, Gijsbert A. van der Marel, Herman S. Overkleeft and Mark Overhand
Structure      13C NMR   碳谱模拟图
9 .     Compound 2
C36H49N9O9     相似度:62.5%
Bioorganic & Medicinal Chemistry Letters          2002          12          547-549
Solid-phase synthesis of c(RGDfK) derivatives: on-resin cyclisation and lysine functionalisation
Catherine F. McCusker, Philip J. Kocienski, F. Thomas Boyle, Andreas G. Schätzlein
Structure      13C NMR   碳谱模拟图
10 .     cherimolacyclopeptide E
C33H42N6O7     相似度:62.0%
Phytochemistry          2005          66          2376-2380
Two cyclopeptides from the seeds of Annona cherimola
Alassane Wélé, Yanjun Zhang, Jean-Paul Brouard,Jean-Louis Pousset, Bernard Bodo
Structure      13C NMR   碳谱模拟图
11 .     delavayin A
C32H42N6O8     相似度:62.0%
Journal of Natural Products          1997          60          212-215
Cyclic Peptides from Higher Plants. 33. Delavayins A-C, Three New Cyclic Peptides from Stellaria delavayi
Hiroshi Morita, Takashi Kayashita, Akihiro Uchida, Koichi Takeya, and Hideji Itokawa
Structure      13C NMR   碳谱模拟图
12 .     yunnanin B
C32H43N6O8     相似度:62.0%
Chemistry Letters          1994          23          2415-2418
Two Novel Cyclic Peptides, Yunnanins A and B from Stellaria yunnanensis
Hiroshi Morita, Akira Shishido, Takashi Kayashita, Masako Shimomura, Koichi Takeya and Hideji Itokawa
Structure      13C NMR   碳谱模拟图
13 .     CJ-15,183
C28H38O13     相似度:62.0%
The Journal of Antibiotics          2001          54          904-910
CJ-15, 183, a New Inhibitor of Squalene Synthase Produced by a Fungus, Aspergillus aculeatm
SHUZO WATANABE,HIDEO HIRAI,MASARU ISHIGURO,TAKAHITO KAMBARA,YASUHIRO KOJIMA,TOMOYUKI MATSUNAGA,HIROYUKI NISHIDA,YUMIKO SUZUKI,AYUMU SUGIURA,H. JAMES HARWOOD,LIANG HSIUNG HUANG and NAKAO KOJIMA
Structure      13C NMR   碳谱模拟图
14 .     cyclo(pro-(S)-β2hVal-(S)-Orn-(R)-β3hLeu-(R)-Phe)2
C64H100N12O10     相似度:62.0%
Chemistry & Biodiversity          2012          9          2494-2506
Synthesis and Biological Evaluation of Gramicidin S-Inspired Cyclic Mixed /β-Peptides
Matthijs van der Knaap, Fatih Basalan, Henny C. van de Mei, Henk J. Busscher, Gijsbert A. van der Marel, Herman S. Overkleeft and Mark Overhand
Structure      13C NMR   碳谱模拟图
15 .     Cherimolacyclopeptide E
C33H42N6O7     相似度:62.0%
Journal of Natural Products          2012          75          1882-1887
Solid-Phase Total Synthesis of Cherimolacyclopeptide E and Discovery of More Potent Analogues by Alanine Screening
Farzana Shaheen, Tania S. Rizvi, Syed G. Musharraf, A. Ganesan, Kai Xiao, Jared B. Townsend, Kit S. Lam, and M. Iqbal Choudhary
Structure      13C NMR   碳谱模拟图
16 .     Cyclo(N-methyl-L-Phe-L-Pro-L-Leu-D-Ile-L-Val)
C32H49N5O5     相似度:62.0%
Natural Products and Bioprospecting          2011          1          75-80
Chemical investigation on the cultures of the fungus Xylaria carpophila
Xia Yin, Tao Feng, Zheng-Hui Li, Jia Su, Yan Li, Ning-Hua Tan, Ji-Kai Liu
Structure      13C NMR   碳谱模拟图
17 .     Cyclo[Valψ{(CdS)NH}-Ser-D-Pheψ{(CdS)NH}-Ser-Phe-Proallo-Thr]
    相似度:61.7%
Journal of the American Chemical Society          1996          118          12358-12367
Total Synthesis and Assignment of Configuration of Lissoclinamide 7
Peter Wipf and Paul C. Fritch
Structure      13C NMR   碳谱模拟图
18 .     rhopeptin A
C33H37N5O8     相似度:61.2%
Helvetica Chimica Acta          2013          96          114-118
Rhopeptin A: First Cyclopeptide Isolated from Rhodobryum giganteum
Wei Jiao, Zhijun Wu, Xiaozhen Chen, Runhua Lu and Huawu Shao
Structure      13C NMR   碳谱模拟图
19 .     HO-D-Pro-L-Phe-CO-(CH2)7-CO-L-Phe-D-Pro-OH
C37H48N4O8     相似度:60%
European Journal of Organic Chemistry          2011                   3082-3088
L-Phe-D-Oxd: A Privileged Scaffold for the Formation of Supramolecular Materials
Nicola Castellucci, Gaetano Angelici, Giuseppe Falini, Magda Monari and Claudia Tomasini
Structure      13C NMR   碳谱模拟图
20 .     Cyclo[D-Val-Ser-D-Phe-Ser-Phe-Pro-allo-Thr(oxaz)]
C38H49N7O9     相似度:60%
Journal of the American Chemical Society          1996          118          12358-12367
Total Synthesis and Assignment of Configuration of Lissoclinamide 7
Peter Wipf and Paul C. Fritch
Structure      13C NMR   碳谱模拟图
思路决定出路!
4楼2015-05-05 15:43:53
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