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faair

铜虫 (正式写手)

[交流] 【请教】CNTs能做出C-NMR吗?

看到有的文献做出了碳管的C核磁,也有文献说cnt做不出核磁
自己拿CNTs试了一下,用氘代DMF

什么峰都没做出来

想问下是什么原因? 为什么没有信号

固体核磁可以做出来?


谢谢~

[ Last edited by jackchen145 on 2008-7-5 at 18:12 ]
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weirr06@lzu.cn

木虫 (小有名气)

很有意思的研究课题,俺也很感兴趣
2楼2008-07-07 15:58:10
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haiyun805

铜虫 (小有名气)

固体核磁氢谱一点问题也无,碳谱困难,。
放荡形骸,修身养性!
3楼2008-07-08 03:51:37
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faair

铜虫 (正式写手)

那是什么原因呢?

CNT做氢谱?CNT上有H?
4楼2008-07-08 23:46:05
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ibkpci

铁杆木虫 (正式写手)


jackchen145(金币+1,VIP+0):谢谢讨论!欢迎常来纳米版!
1, CNT free of magnetic catalysts.
2, prepare CNT with 13C rather than normal 12C.
Then, NMR CNT will work
5楼2008-07-09 04:08:44
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faair

铜虫 (正式写手)

it seems rather difficult to prepare CNT with 13C for me. I use commercial available CNTs but have no equipment to prepare CNTs

You mean I should have 13C source, then get 13C-CNTs

What's more, i wanna to know what degree do the magnetic catalysts influence the 13C-NMR signal?

Thanks a lot~
6楼2008-07-09 23:31:55
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ibkpci

铁杆木虫 (正式写手)

★ ★
jackchen145(金币+2,VIP+0):谢谢讨论,欢迎常来纳米版!
In my experience, you need 13C to produce CNT, 13C is more expensive than 12C, we use laser ablation to synthesize 13C SWNTs, the yield is much lower than 12C CNT.

"i wanna to know what degree do the magnetic catalysts influence the 13C-NMR signal?"
What do you means?
If buckypaper has the magnetic catalysts inside, the NMR signal you got is only from the magnetic catalysts. So.....
7楼2008-07-13 05:50:56
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