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qiupingdafo新虫 (初入文坛)
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[求助]
微谱求助14-1 已有1人参与
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溶剂：氘代氯仿 碳谱数据：24.6,29.4,29.7,32.0,55.9,63.8,111.5,114.3,114.5,120.2,121,6 |
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yangyinhe
至尊木虫 (著名写手)
- 应助: 1566 (讲师)
- 金币: 15048.4
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- 帖子: 2773
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- 专业: 天然有机化学
【答案】应助回帖
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感谢参与，应助指数 +1
qiupingdafo(卓越_先锋代发): 金币+10, ok 2015-04-26 12:30:12
感谢参与，应助指数 +1
qiupingdafo(卓越_先锋代发): 金币+10, ok 2015-04-26 12:30:12
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1 . 2-{6-[(6-methoxy-4H-3,1-benzothiazin-2-yl)sulfanyl]hexylsulfanyl}-4H-3,1-benzothiazine C24H28N2O2S4 相似度:58.3% Heterocycles 2013 87 1311-1317 Synthesis of 2-Sulfanyl-4H-3,1-benzothiazine Derivatives by the Reaction of 2-(Bromomethyl)phenyl Isothiocyanates with Thiols Kosuke Ezaki, Miyuki Tanmatsu, and Kazuhiro Kobayashi* Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . 6-endo-8-phenyl-2-oxo-8-azabicyclo[3,2,1]octane-6-carbonitrile 相似度:58.3% Bulletin des Sociétés Chimiques Belges 1981 90 49-56 Synthesis, 1H-and 13C-NMR Spectra of 2-Tropanone Derivatives. The “6-Endo” or “6-Exo”-8-Methyl or Phenyl-2-Oxo-8-Azabicyclo of 3,2,1]-Oct-3-Ene-6-Carbonitrile and 3,4-Dihydrogenated Analogues J. A. Lepoivre, R. A. Dommisse, E. L. Esmans, J. J. van Luppen, E. M. Merckx and F. C. Alderweireldt Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 4-Iodobutyl-1-phenoxyacetate 相似度:58.3% Tetrahedron 2012 68 7787-7793 Preparation of N3-thymidine–butylene–N3-thymidine interstrand cross-linked DNA via an orthogonal deprotection strategy Gang Sun, Anne Noronha, Christopher Wilds Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . 5-(m-methoxyphenyl)pentan-1-ol 相似度:58.3% Tetrahedron 2014 70 4942-4946 Ring-opening of cyclic ethers with carbon–carbon bond formation by Grignard reagents Stig Holden Christensen, Torkil Holm, Robert Madsen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . S-[4-(3-Indolyl)but-1-yl]homocysteine C16H22O2N2S 相似度:57.1% Journal of Medicinal Chemistry 1983 26 1470-1477 Multisubstrate adducts as potential inhibitors of S-adenosylmethionine dependent methylases: inhibition of indole N-methyltransferase by (5H-deoxyadenosyl)[3-(3-indolyl)propyl-1-yl]methylsulfonium and (5'-deoxyadenosyl)[4-(3-indolyl)but-1-yl]methylsulfoni Eric Benghiat, Peter A. Crooks Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . ;S-[3-(3-Indolyl)prop-1-yl]homocysteine C15H20O2N2S 相似度:57.1% Journal of Medicinal Chemistry 1983 26 1470-1477 Multisubstrate adducts as potential inhibitors of S-adenosylmethionine dependent methylases: inhibition of indole N-methyltransferase by (5H-deoxyadenosyl)[3-(3-indolyl)propyl-1-yl]methylsulfonium and (5'-deoxyadenosyl)[4-(3-indolyl)but-1-yl]methylsulfoni Eric Benghiat, Peter A. Crooks Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 2,7-Diamino-9,9-dihexylfluorene 相似度:53.8% Canadian Journal of Chemistry 2010 88 945-953 Understanding the reversible anodic behaviour and fluorescence properties of fluorenylazomethines -A structure-property study Satyananda Barik, Sayuri Friedland, and W.G. Skene Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 3-[(E)-octa-2,7-dienyl]-1H-indole C16H19N 相似度:53.3% Heterocycles 2010 80 779-785 Boron Trichloride Mediated Alkyne-Aldehyde Coupling Reactions Min-Liang Yao, Michael P. Quinn, and George W. Kabalka Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . 6-methoxy-2-(6-sulfanylhexylsulfanyl)-4H-3,1-benzothiazine C15H21NOS3 相似度:53.3% Heterocycles 2013 87 1311-1317 Synthesis of 2-Sulfanyl-4H-3,1-benzothiazine Derivatives by the Reaction of 2-(Bromomethyl)phenyl Isothiocyanates with Thiols Kosuke Ezaki, Miyuki Tanmatsu, and Kazuhiro Kobayashi* Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 3-(1-(4-Methoxyphenyl)pyrrolidin-2-yl)-N-methylpyridin-2-amine C17H21N3O 相似度:53.3% Tetrahedron 2015 71 1930−1939 Substituent-directed reduction of cyclic aminals leading to two different heterocycles selectively: syntheses of functionalized nicotines and pyrido[2,3-b]azepines Yuewei Zhang, Lianyou Zheng, Fengzhi Yang, Zhuoqi Zhang, Qun Dang, Xu Bai Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
2楼2015-04-14 10:55:13
