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hycome木虫 (正式写手)
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[求助]
求助 C 谱 已有1人参与
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13C NMR (101 MHz, CDCl3) δ173.46, 130.38, 128.22, 128.03, 69.02, 62.24, 34.20, 32.07, 31.08, 29.85, 25.01, 22.84, 14.26. 样品不太纯，部分信号如上，谢谢 |
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hycome
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4楼2015-04-07 21:10:25
yangyinhe
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2楼2015-04-07 18:54:42
CloudWhisper
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【答案】应助回帖
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感谢参与，应助指数 +1
hycome: 金币+10, ★★★很有帮助, 谢谢 2015-04-07 23:30:26
感谢参与，应助指数 +1
hycome: 金币+10, ★★★很有帮助, 谢谢 2015-04-07 23:30:26
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1 . N-methybenzylammonium salt C10H21O4P 相似度:76.9% Heterocycles 2008 76 657-665 Selective Synthesis of Cyclic Phosphoric Acid Diesters through Oxorhenium(VII)-Catalyzed Dehydrative Condensation of Phosphoric Acid with Alcohols Akira Sakakura, Masayuki Sakuma, Mikimoto Katsukawa, and Kazuaki Ishihara Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . glycerol 1,3-dioleate-2-stearate 相似度:76.9% Archives of Pharmacal Research 2004 27 734-737 Cytotoxic constituents of diadema setosum Chau Van Minn, Phan Van Kiem, Le Mai Huong and Young Ho Kim Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . 2-hydroxyethylcarboxylic acid-5,9-eicodien-carboxylate C24H42O5 相似度:71.4% Chemistry of Natural Compounds 2007 43 652-654 TWO NEW COMPONENTS FROM THE ROOTS OF Angelicae koreana KITAGAWA Shin Yoosoo, Lee Ogyu Park Chungberm Lee Hakju Choi Bongjae, Ham Inhye, Choi Hoyoung,Seong Naksul, and Cha Sunwoo Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . compound 16 相似度:71.4% Tetrahedron Letters 2005 46 5999-6003 TiCl4-promoted addition of nucleophiles to open chain α-amidoalkylphenyl sulfones Marino Petrini, Elisabetta Torregiani Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . (7Z,10Z)-hexadecadienoic acid 相似度:71.4% Chemistry of Natural Compounds 2015 51 26−30 Synthesis of the ω6 (5Z,8Z)-Tetradecadienoic and (7Z,10Z)-Hexadecadienoic Polyene Fatty Acids A. B. Golovanov, K. D. Ganina, N. V. Groza, S. V. Eremin, G. I. Myagkova Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . Methyl Undec-5Z-enoate 相似度:69.2% Chemistry of Natural Compounds 1991 27 497-499 INSECT PHEROMONES AND THEIR ANALOGUES XXXI. SYNTHESIS OF DEC-5Z-EN-I-YL ACETATE AND HENEICOS- 6Z-EN-II-ONE FROM A FUNCTIONALLY DIFFERENTIATED PRODUCT OF THE OZONOLYSIS OF CYCLOPENTENE V. N. Odinokov, V. R. Akhmetova, Kh.,D. Khasanov,A. A. Abduvakhabov, and G. A. Tolstikov Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . hexadecanoic acid,2,3-dihydroxypropyl ester 相似度:69.2% Journal of Shenyang Pharmaceutical University 2002 19 25-26 Study on the chemical constituents of the Ovum Oil of Rana temporaria chensinensis David(II) LU Li-ming, SONG Shao-jiang, WU Yong, ZHANG Lin-lin, XU Sui-xu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . 4-octyl-benzoic acid 相似度:69.2% Bioorganic & Medicinal Chemistry 2009 17 6123-6136 Synthesis and biological evaluation of sphingosine kinase substrates as sphingosine-1-phosphate receptor prodrugs Frank W. Foss Jr., Thomas P. Mathews, Yugesh Kharel, Perry C. Kennedy, Ashley H. Snyder, Michael D. Davis, Kevin R. Lynch, Timothy L. Macdonald Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . trimyristin 相似度:69.2% Agricultural and Biological Chemistry 1988 52 2589-2595 Cell Aggregation Factor Produced by Streptomyces sp. Strain No. A-3315 Keitarou SUZUKI, Nahoko NAKANO, Rie TANAKA, Masaru UYEDA, Motoo SHIBATA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . 4-(2-hexyloxyethyl)phenol C14H22O2 相似度:69.2% Food Chemistry 2011 129 1169-1178 Preparation and antioxidant activity of tyrosyl and homovanillyl ethers A. Madrona, G. Pereira-Caro, L. Bravo, R. Mateos, J.L. Espartero Structure 13C NMR Structure & 13C NMR 碳谱模拟图 11 . 4-heptyl-N-methoxy-N-methylbenzamide C16H25NO2 相似度:69.2% European Journal of Organic Chemistry 2010 4991-5003 Weinreb Amide Based Building Blocks for Convenient Access to Analogues of Phenstatin Balasubramaniam Sivaraman and Indrapal Singh Aidhen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 12 . Coriander lactone C37H70O2 相似度:69.2% Organic and Medicinal Chemistry Letters 2012 2 1-4 Two new aliphatic lactones from the fruits of Coriandrum sativum L. Kamran J Naquvi, Mohammed Ali and Javed Ahmad Structure 13C NMR Structure & 13C NMR 碳谱模拟图 13 . 2-(2-Benzyloxyethoxy)ethyl decanoate 相似度:69.2% Steroids 2013 78 435-453 New propanoyloxy derivatives of 5β-cholan-24-oic acid as drug absorption modifiers Lenka Coufalová, Lech Mrózek, Lucie Rárová, Lukáš Plaček, Radka Opatřilová, Jiří Dohnal, Katarína Král’ová, Oldřich Paleta, Vladimír Král, Pavel Drašar, Josef Jampílek Structure 13C NMR Structure & 13C NMR 碳谱模拟图 14 . Coriander lactone C37H70O2 相似度:69.2% Organic and Medicinal Chemistry Letters 2011 1 1-4 Two new aliphatic lactones from the fruits of Coriandrum sativum L. Kamran J Naquvi, Mohammed Ali and Javed Ahmad Structure 13C NMR Structure & 13C NMR 碳谱模拟图 15 . linoleic acid 相似度:69.2% Journal of Applied Phycology 2008 20 713-720 Algicidal activity of polyunsaturated fatty acids derived from Ulva fasciata and U.pertusa (Ulvaceae, Chlorophyta) on phytoplankton Mochammad Amin Alamsjah, Shotaro Hirao, Fumito Ishibashi, Tatsuya Oda, Yuji Fujita Structure 13C NMR Structure & 13C NMR 碳谱模拟图 16 . 2-(1',2'-O-Di-n-hexanoyl-sn-3'-glyceryl)-2-thio-1,3,2-dithiaphospholane C20H40NO7PS 相似度:69.2% The Journal of Organic Chemistry 1994 59 4821-4831 Design, Synthesis, and Evaluation of Phospholipid Analogs as Inhibitors of the Bacterial Phospholipase C from Bacillus cereus Stephen F. Martin, Yue-Ling Wong, Allan S. Wagman Structure 13C NMR Structure & 13C NMR 碳谱模拟图 17 . tripalmitin 相似度:69.2% Chinese Joumal of Experimental Traditional Medical Fomulae 2013 19 136-139 Chemical Constituents from the Ethyl Acetate Extract Parts of Qinzhu Siwu Tang YUAN Hai-mei, PENG Teng, HUANG Dao-qiu, LI Xiao-nian, LI Bo-qun, LING Zhi-qun, YANG Jing, HE Gang-min, LI Yu-chuan Structure 13C NMR Structure & 13C NMR 碳谱模拟图 18 . 1-cerotoylglycerol 相似度:69.2% Chinese Pharmaceutical Journal 2014 49 1393-1396 Chemical Constituents of Roots of Salvia plebeia LIU Li, DAI Yi-qun, XIE Guo-yong, LI Ming-liang, FENG Qi-tong, QIN Min-jian Structure 13C NMR Structure & 13C NMR 碳谱模拟图 19 . glycerol 1,3-di-(9E-octadecenoate) 2-hexadecanoate C55H102O6 相似度:69.2% Acta Botanica Yunnanica 2007 29 367-370 Palaeophytochemical Constituents from the Pliocene-fossil Wood of Tsuga dumosa (Pinaceae) ZHAO You-Xing, LI Cheng-Sen, LUO Xiao-Dong, ZHOU Lu, YI Tie-Mei, ZHOU Jun Structure 13C NMR Structure & 13C NMR 碳谱模拟图 20 . methyl undeca-4E,6Z-dienoate C12H10O2 相似度:69.2% Chemistry of Natural Compounds 1999 35 358-360 Insect pheromones and their analogs LIX. A new method for the synthesis of components of the sex pheromones of insects of the genusMalacosoma O. S. Kukovinets, V. G. Kasradze, E. V. Salimova, V. N. Odinokov, F. Z. Galin, P. I. Fedorov Structure 13C NMR Structure & 13C NMR 碳谱模拟图 21 . Altheahexacosanyl lactone C26H48O2 相似度:68.7% Natural Product Research 2010 24 1358-1364 Phytochemical investigation of the seeds of Althea officinalis L. Sunita Rani; Suroor A. Khan; M. Ali Structure 13C NMR Structure & 13C NMR 碳谱模拟图 22 . N-(E-1,3-dihydroxyhexadec-4-en-2-yl)heptacosanamide C43H85NO3 相似度:68.7% Chinese Journal of Spectroscopy Laboratory 2005 22 1138-1141 The Secondary M etabol ites from Halimeda Xishaensi XIAO Xiao-Mei, XU Shi-Hai, YANG Kai Structure 13C NMR Structure & 13C NMR 碳谱模拟图 23 . 1-O-hexadecanoyl-2-O-(9-octadecenoyl)-3-O-(9,12-octadecadienoyl) glycerol 相似度:66.6% Acta Pharmaceutica Sinica 2002 Vol 37 271-274 CHEMICAL CONSTITUENTS FROM MARINE FUNGUS PENICILLIUM THOMII JIANG Ting; TIAN Li; GUO Ai hua; FU Hong zheng; PEI Yue hu; LIN Wen han Structure 13C NMR Structure & 13C NMR 碳谱模拟图 24 . (8Z,11Z)-Pentadeca-8,11-dien-2-ol C15H28O 相似度:66.6% Organic & Biomolecular Chemistry 2008 6 4333-4339 Isolation, structure elucidation and total synthesis of a cytotoxic dienone from Echinacea pallida Stefania Morandi, Federica Pellati, Claudia Ori, Barbara Adinolfi, Paola Nieri, Stefania Benvenuti and Fabio Prati Structure 13C NMR Structure & 13C NMR 碳谱模拟图 25 . (1SR,4SR)-1-(2-benzoylhydrazinyl)-N-cyclohexyl-4-methylcyclohexane carboxamide C21H31N3O2 相似度:66.6% Tetrahedron 2013 69 3480-3485 An efficient and diastereoselective synthesis of hydrazino amides via a novel one-pot three-component reaction Sorour Ramezanpour, Saeed Balalaie, Frank Rominger, Hamid Reza Bijanzadeh Structure 13C NMR Structure & 13C NMR 碳谱模拟图 26 . (1SR,4SR)-N-cyclohexyl-4-methyl-1-(2-(thiophene-2-carbonyl)hydrazinyl)cyclohexane carboxamide C19H29N3O2S 相似度:66.6% Tetrahedron 2013 69 3480-3485 An efficient and diastereoselective synthesis of hydrazino amides via a novel one-pot three-component reaction Sorour Ramezanpour, Saeed Balalaie, Frank Rominger, Hamid Reza Bijanzadeh Structure 13C NMR Structure & 13C NMR 碳谱模拟图 27 . compound 27 C16H20O3F2 相似度:64.2% Zeitschrift für Naturforschung B 2004 59 77-94 Synthesis of Highly Flexible Difluorinated Cyclopropanoid Nucleoside Analogues R. Csuk and L. Eversmann Structure 13C NMR Structure & 13C NMR 碳谱模拟图 28 . 4-(2-octyloxyethyl)phenol C16H26O2 相似度:64.2% Food Chemistry 2011 129 1169-1178 Preparation and antioxidant activity of tyrosyl and homovanillyl ethers A. Madrona, G. Pereira-Caro, L. Bravo, R. Mateos, J.L. Espartero Structure 13C NMR Structure & 13C NMR 碳谱模拟图 29 . (±)-1,1,1-trichloro-4-phenylbutan-2-yl hexanoate C16H21Cl3O2 相似度:64.2% Journal of the American Chemical Society 2009 131 7552-7553 A Tetrachloro Polyketide Hexahydro-1H-isoindolone, Muironolide A, from the Marine Sponge Phorbas sp. Natural Products at the Nanomole Scale Doralyn S. Dalisay, Brandon I. Morinaka, Colin K. Skepper and Tadeusz F. Molinski Structure 13C NMR Structure & 13C NMR 碳谱模拟图 30 . pulchranin A C14H29N3O 相似度:64.2% Tetrahedron Letters 2013 54 1247-1250 Pulchranin A, isolated from the Far-Eastern marine sponge, Monanchora pulchra: the first marine non-peptide inhibitor of TRPV-1 channels Alla G. Guzii, Tatyana N. Makarieva, Yuliya V. Korolkova, Yaroslav A. Andreev, Irina V. Mosharova, Ksenya M. Tabakmaher, Vladimir A. Denisenko, Pavel S. Dmitrenok, Ekaterina K. Ogurtsova, Alexandr S. Antonov, Hyi-Seung Lee, Eugene V. Grishin Structure 13C NMR Structure & 13C NMR 碳谱模拟图 31 . (4Z,6E,8Z)-tetradeca-4,6,8-trien-1-ol C14H24O 相似度:64.2% Tetrahedron 2013 69 3872-3877 Z-Stereoselective semi-reduction of alkynes: modification of the Boland protocol Yasser M.A. Mohamed, Trond Vidar Hansen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 32 . isopropyl 4-octylbenzoate C18H28O2 相似度:64.2% Tetrahedron 2013 69 9580-9585 Iron-catalyzed cross-coupling of aryltrimethylammonium triflates and alkyl Grignard reagents Original Research Article Wang-Jun Guo, Zhong-Xia Wang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 33 . Methyl (5Z)-5-Hexacosenoate 相似度:64.2% Journal of the American Chemical Society 1988 110 8117-8124 Biosynthetic studies of marine lipids. 17. The course of chain elongation and desaturation in long-chain fatty acids of marine sponges Soonkap. Hahn, Ivan L. Stoilov, T. B. Tam. Ha, Daniel. Raederstorff, George A. Doss, Hui Ting. Li, Carl. Djerassi Structure 13C NMR Structure & 13C NMR 碳谱模拟图 34 . 硬脂酸苯甲酯 相似度:64.2% Chinese Journal of Organic Chemistry 2013 33 190-194 Cesium Chloride Catalysized the Reaction of Sodium (Potassium) Carboxylates with Alkyl Bromides (Chlorides) Liu Wenqi, Qi Jianyong, Chen Jinyang, Li Ningbo, Qui Renhua, Xu Xinhua Structure 13C NMR Structure & 13C NMR 碳谱模拟图 35 . (5Z,8Z)-tetradecadienoic acid 相似度:64.2% Chemistry of Natural Compounds 2015 51 26−30 Synthesis of the ω6 (5Z,8Z)-Tetradecadienoic and (7Z,10Z)-Hexadecadienoic Polyene Fatty Acids A. B. Golovanov, K. D. Ganina, N. V. Groza, S. V. Eremin, G. I. Myagkova Structure 13C NMR Structure & 13C NMR 碳谱模拟图 36 . heptadeca-4-ene-acetate C18H34O2 相似度:62.5% Indian Journal of Chemistry Section B 2009 48B 1038-1040 Isolation and characterization of novel esters from aerial parts of Tiliacora acuminata Selvaraj,S Joseph; Alphonse,I; Britto,S John Structure 13C NMR Structure & 13C NMR 碳谱模拟图 37 . (1SR,4SR)-ethyl 4-(cyclohexylcarbamoyl)-4-(2-(thiophene-2-carbonyl)hydrazinyl)piperidine-1-carboxylate C20H30N4O4S 相似度:62.5% Tetrahedron 2013 69 3480-3485 An efficient and diastereoselective synthesis of hydrazino amides via a novel one-pot three-component reaction Sorour Ramezanpour, Saeed Balalaie, Frank Rominger, Hamid Reza Bijanzadeh Structure 13C NMR Structure & 13C NMR 碳谱模拟图 38 . (5Z,7E,9Z)-methyl pentadeca-5,7,9-trienoate C16H26O2 相似度:62.5% Tetrahedron 2013 69 3872-3877 Z-Stereoselective semi-reduction of alkynes: modification of the Boland protocol Yasser M.A. Mohamed, Trond Vidar Hansen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 39 . compound 12f 相似度:62.5% European Journal of Organic Chemistry 2001 2001 1293-1308 Pyrrolidine N-Oxides by Stereoselective Addition of Grignard and Lithium Compounds to 4,5-Dideoxy-2,3-O-isopropylidene-D-erythro-4-pentenose N-Benzyl Nitrone and Subsequent Cope−House Cyclization Andreas M. Palmer and Volker Jäger Structure 13C NMR Structure & 13C NMR 碳谱模拟图 40 . 神经酰胺 II 相似度:62.5% Chinese Journal of Analytical Chemistry 2001 29 1311-1314 Chemical Constituents of the Tunicate Styela Plicata from the Dayawan Bay Wang Chaojie Structure 13C NMR Structure & 13C NMR 碳谱模拟图 41 . 黄葵内酯 相似度:62.5% Journal of Chinese Medicinal Materials 2008 31 1508-1510 Studies on Chemical Constituents from Zephyranthes candida WU Zhi-ping, CHEN Yu, WANG Ming, DONG Yun-fa, XIA Bing, FENG Xu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 42 . methyl linoleate C19H34O2 相似度:62.5% Journal of Chinese Medicinal Materials 2011 34 223-225 Studies on the Chemical Constituents of Laportea bulbifera ZHU Zhu, MA Lin, ZHU Hai-yan, YANG Xiao-sheng, HAO Xiao-jiang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 43 . LXLS 相似度:62.5% Russian Journal of Bioorganic Chemistry 2006 32 478-484 Identification and Structural Analysis of a Glycophospholipid Component from the Venom of Ant Paraponera clavata K. A. Pluzhnikov, D. N. Bocharov, N. V. Kononova, S. V. Sukhanov, T. A. Balashova, A. S. Arseniev, and E. V. Grishin Structure 13C NMR Structure & 13C NMR 碳谱模拟图 44 . methyl linoleate C19H34O2 相似度:62.5% Chinese Journal of Marine Drugs 2013 32 7-12 南海沉积环境来源真菌Eurotiumsp.SCSIO F452的次生代谢产物研 王发左, 黄智, 史雪凤, 陈玉婵, 田新朋, 李洁, 章卫民, 张偲 Structure 13C NMR Structure & 13C NMR 碳谱模拟图 45 . 7-methoxyeicos-4(E)-enoic acid 相似度:61.5% Journal of Natural Products 1999 62 1696-1699 Serinol-Derived Malyngamides from an Australian Cyanobacterium Feng Wan and Karen L. Erickson Structure 13C NMR Structure & 13C NMR 碳谱模拟图 46 . O-[2'-hydroxy-3'-(2"-heptenyloxy)]-propyl undecanoate C21H40O4 相似度:61.5% Planta Medica 1998 64 225-228 Hypotensive Constituents from the Pods of Moringa oleifera Shaheen Faizi, Bina Shaheen Siddiqui, Rubeena Saleem, KhaIid Aftab, Farhana Shaheen,and Anawr-ul-Hassan GiIani Structure 13C NMR Structure & 13C NMR 碳谱模拟图 47 . compound 6 C26H50O8 相似度:61.5% Chemistry of Natural Compounds 2001 37 124-126 SYNTHESIS OF D-MANNITE ESTERS OF ALIPHATIC AND AROMATIC ACIDS A. F. Artamonov, F. S. Nigmatullina,M. T. Aldabergenova, and B. Zh. Dzhiembaev Structure 13C NMR Structure & 13C NMR 碳谱模拟图 48 . (1-heptyl)diphenylphosphine oxide C19H25OP 相似度:61.5% Journal of Natural Products 1987 Vol 50 75 Synthesis and Biological Activity of Analogs of Fecapentaene-12 S. V. Govindan, David G. I. Kingston, A. A. L. Gunatilaka, Roger L. van Tassell, Tracy D. Wilkins, P. P. de Wit, M. van der Steeg, A. van der Gen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 49 . 2-(p-hydroxyphenyl)Ethylstearate 相似度:61.5% Phytochemistry 1992 31 195-197 A eudesmanolide and other constituents from Inula graveolens Seviˇl O¨ksu¨z, Gu¨laçti Topçu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 50 . Bis(2-methylheptyl)phthalate 相似度:61.5% Korean Journal of Pharmacognosy 2007 38(4) 382-386 Isolation of Melanogenesis Inhibitors from Cinnamomi Cortex Jung, Hee-Wook; Choi, Ji-Young; Lee, Jong-Gu; Choi, Eun-Hyang; Oh, Joon-Seok; Kim, Dong-Chun; Kim, Jeong-Ah; Park, Seong-Hee; Son, Jong-Keun; Lee, Seung-Ho Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
3楼2015-04-07 19:50:52
hycome
木虫 (正式写手)
- 应助: 0 (幼儿园)
- 金币: 3035.6
- 散金: 5
- 帖子: 327
- 在线: 271.1小时
- 虫号: 50805
- 注册: 2004-07-14
- 专业: 生物化工与食品化工
5楼2015-04-07 21:13:05
100