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小小小糖豆

银虫 (小有名气)

[求助] 求助微谱!毕业急需! 已有1人参与

名称:YB-3
溶剂:甲醇
13C NMR:8.10,24.96,25.01,25.83,31.86,38.20,53.18,73.58,82.49,107.47,124.27,162.20,175.41

名称:YB-5
溶剂:氯仿
13C NMR:8.48,19.91,22.90,35.84,72.27,78.20,120.17,163.08,175.19

名称:YB-6
溶剂:氯仿
13C NMR:8.43,22.54,24.83,36.29,36.94,41.51,51.43,51.90,103.93,107.04,122.27,148.78,161.28,172.70
谢谢各位的大力相助!
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yangyinhe

至尊木虫 (著名写手)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
小小小糖豆: 金币+15, ★★★很有帮助 2015-03-27 09:35:39
1 .     zedoarolide A
C15H22O5     相似度:86.6%
Chemical & Pharmaceutical Bulletin          2001          49(12)          1558-1566
Medicinal Foodstuffs. XXVIII.1) Inhibitors of Nitric Oxide Production and New Sesquiterpenes, Zedoarofuran, 4-Epicurcumenol,Neocurcumenol, Gajutsulactones A and B, and Zedoarolides A and B, from Zedoariae Rhizoma
Hisashi MATSUDA, Toshio MORIKAWA, Iwao TOGUCHIDA, Kiyofumi NINOMIYA, and Masayuki YOSHIKAWA
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

2 .     zedoarolide B
    相似度:86.6%
Journal of Shenyang Pharmaceutical University          2008          25          188-190
Guaiane sesquiterpenes of Curcuma wenyujin
HU Dan, MA Ning, LOU Yan, QU Ge-xia, QIU Feng
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

3 .     zedoarolide A
C15H22O5     相似度:60%
Chemical & Pharmaceutical Bulletin          2001          49(12)          1558-1566
Medicinal Foodstuffs. XXVIII.1) Inhibitors of Nitric Oxide Production and New Sesquiterpenes, Zedoarofuran, 4-Epicurcumenol,Neocurcumenol, Gajutsulactones A and B, and Zedoarolides A and B, from Zedoariae Rhizoma
Hisashi MATSUDA, Toshio MORIKAWA, Iwao TOGUCHIDA, Kiyofumi NINOMIYA, and Masayuki YOSHIKAWA
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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4 .     zedoalactone A
    相似度:60%
Planta Medica          2005          71          482-484
Anti-Babesial Compounds from Curcuma zedoaria
Ken Kasahara,Shinkichi Nomura, Subeki, Hideyuki Matsuura,Masahiro Yamasaki , Osamu Yamato , Yoshimitsu Maede ,Ken Katakura,Mamoru Suzuki ,Trimurningsih, Chairul ,Teruhiko Yoshihara
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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5 .     Zedoalactone A
C15H22O4     相似度:60%
Phytochemistry          1995          40          1197-1200
Guaiane sesquiterpene lactones from Curcuma aeruginosa
Ichiro Takano, Ichiro Yasuda, Koichi Takeya, Hideji Itokawa
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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6 .     zedoalactone A
    相似度:60%
Chinese Pharmaceutical Journal          2008          43          822-824
Studies on Chemical Constituents in Guiyujin (Report Ⅰ)
GE Yue-wei, GAO Hui-min, WANG Wei-hao, WANG Zhi-min
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

7 .     zedoalactone A
    相似度:60%
Journal of Shenyang Pharmaceutical University          2008          25          188-190
Guaiane sesquiterpenes of Curcuma wenyujin
HU Dan, MA Ning, LOU Yan, QU Ge-xia, QIU Feng
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

8 .     zedoarolide B
C15H22O5     相似度:60%
Heterocycles          2001          55          841-846
Inhibitors of Nitric Oxide Production and New Sesquiterpenes, 4-epi-Curcumenol, Neocurcumenol, Gajutsulactones A and B, and Zedoarolides A and B from Zedoariae Rhizoma
Hisashi Matsuda, Toshio Morikawa, Iwao Toguchida, Kiyofumi Ninomiya, and Masayuki Yoshikawa
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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9 .     zedoalactone A
    相似度:60%
Chinese Traditional and Herbal Drugs          2011          42          1079-1082
Chemical constituents from Paraixeris serotina
XU, Guo-xi
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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10 .     1,3,7,7-Trimethyl-2,11,12-trioxa-5-tricyclo[4.4.1.1 3.0]dodecaen
C13H20O3     相似度:53.8%
Helvetica Chimica Acta          1980          63          2230-2257
Photochemische Reaktionen 115. Mitteilung [1]. Zur Photochemie konjugierter ,γ,δ-Epoxyenone: Der Einfluss eines Hydroxylsubstituenten in -Stellung
Norio Nakamura, Wolfhard Berned Schweizer, Bruno Frei, Hans Richard Wolf, Oskar Jeger
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图
2楼2015-03-26 10:41:46
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

yangyinhe

至尊木虫 (著名写手)

【答案】应助回帖

1 .     compound 3g
    相似度:55.5%
Indian Journal of Chemistry Section B          2005          44B          1505-1508
A convenient synthesis of γ-methyl α-(alkylidene)-γ-butyrolactones
Shet,Jyoti B; Amonkar,Chandan P; Nadkarni,Vishnu S; Tilve,Santosh G
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

2 .     3-(2-butoxy)-2-methyl-3-(1H-tetrazol-5-yl)propionic acid
C9H16N4O3     相似度:55.5%
Journal of Heterocyclic Chemistry          2013          50          868-873
An Efficient Two-Step Synthesis of New 5-Substituted-1H-tetrazoles of Biological Interest
Nilo Zanatta, Fabio M. da Silva, Andreia M. P. W. da Silva, Estefania da C. Aquino, Helio G. Bonacorso and Marcos A. P. Martins
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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3 .     gentiopicral
C10H10O4     相似度:50%
Planta Medica          1983          49          208-210
Studies on Iridoid-related Compounds III: Gentiopicral, the Aglucone of Gentiopicroside
Kyoko Ishiguro, Masae Yamaki and Shuzo Takagi
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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4 .     gentiogenal
    相似度:50%
Planta Medica          1983          49          211-215
Gentiogenal, a Conversion Product of Gentiopicrin (Gentiopicroside)
W. G. van der Sluis, J. M. van der Nat, A. L. Spek, V. Ikeshiro and R. P. Labadie
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

5 .     1,2-dihydroxymintlactone
    相似度:50%
Chinese Journal of Natural Medicines          2013          11          71-73
A new menthane-type monoterpene from Pleurotus eryngii
LIU Liang-Yan, LI Zheng-Hui, LIU Ji-Kai
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

6 .     (5S,7R)-7-hydroxy-5,8,8-trimethylnonanamide
C12H25NO2     相似度:50%
Chemical Communications          2013          49          3341-3344
Zinc stabilization of prefibrillar oligomers of human islet amyloid polypeptide
Jeffrey R. Brender, Janarthanan Krishnamoorthy, Grazia M. L. Messina, Aniruddha Deb, Subramanian Vivekanandan, Carmelo La Rosa, James E. Penner-Hahn and Ayyalusamy Ramamoorthy
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

7 .     (2S,4R,6R)-6-(Cyanomethyl)-4-hydroxy-5,5-dimethyltetrahydro-2H-pyran-2-carboxamide
C10H16N2O3     相似度:50%
European Journal of Organic Chemistry          2012                   1217-1222
An Ammonia-Triggered Stereocontrolled Conversion of a -Lactone to the Central Tetrahydropyran of Pederin, Psymberin, and Onnamides D–F
William J. Buffham, Nigel A. Swain, Sarah L. Kostiuk, Théo P. Gonçalves and David C. Harrowven
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

8 .     1-N-Succinimido-6-O-acetyl-1,2,3,4-tetradeoxy-2β-iodo-α-D/L-hexopyra-noside
    相似度:50%
European Journal of Organic Chemistry          1998          1998          481-492
Enantiopure D-, L- (and 2-epi-) Purpurosamine C-Type Glycosyl Donors from Racemic Acrolein Dimer − Biocatalytic Resolution
Silke Erbeck, Xifu Liang, Richard Krieger and Horst Prinzbach
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

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9 .     aspinolide A
C10H16O3     相似度:50%
European Journal of Organic Chemistry          1997          1997          87-95
Secondary Metabolites by Chemical Screening, 34. – Aspinolides and Aspinonene/Aspyrone Co-Metabolites, New Pentaketides Produced by Aspergillus ochraceus
Jens Fuchser and Axel Zeeck
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图

--------------------------------------------------------------------------------

10 .     gentiolactone
    相似度:50%
Natural Product Research and Development          2012          24          42-46
Chemical constituents of Swertia cincta
GENG Jia-ling; GENG Chang-an; CHEN Ji-jun
Structure      13C NMR    Structure & 13C NMR     碳谱模拟图
3楼2015-03-26 10:44:08
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