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[求助]
急！毕业在即，求助各位高人帮忙解析一下化合物，拜托已有1人参与
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化合物1：YB-1 溶剂：甲醇 13CNMR数据：56.59,57.63,73.83,88.73,112.19,117.30,121.27,135.02,148.53,150.33 化合物2：YB-2 溶剂：甲醇 13CNMR数据：9.29,20.96,21.82,23.73,23.74,37.87,43.15,51.09,56.78,59.39,74.10,106.77,123.07,165.31,175.90 化合物4：YB-4 溶剂：甲醇 13CNMR数据：8.10,13.78,23.03,27.52,30.18,40.29,41.60,51.57,54.88,71.96,80.34,105.97,122.10,164.20,174.75 麻烦各位有微谱数据库或者会拨谱解析的兄弟姐妹们，帮帮忙，毕业在即，小女感激不尽！ |
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小小小糖豆: 金币+20, ★★★★★最佳答案 2015-03-26 09:31:28
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YB-1 1 . (+)-securigtran I C20H22O6 相似度:90% Pharmazie 1998 53 710-715 Studies on Securigera securidacea(L.)Deg.et DORFL.(fabaceae)seeds,an antidiabetic Egyptian folk medicine A.A.ALI,M.H.MOHAMED,M.S.KAMEL,M.A.FOUAD and O.SPRING Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . 桉脂素 相似度:80% China Journal of Chinese Materia Medica 2012 37 2092-2099 Non-anthraquinones constituents from the roots of Knoxia valerianoides ZHAO Feng; WANG Sujuan; WU Xiuli; YU Yang; YUE Zhenggang; LIU Bo; LIN Sheng; ZHU Chenggen; YANG Yongchun; SHI Jiangong Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . 2,3-bis-(α-hydroxy-4-hydroxy-3-methoxybenzyl)-butane-1,4-diol 相似度:80% Chinese Traditional and Herbal Drugs 2015 46 178−186 Chemical constituents from roots of Kadsura longipedunculata CHEN Jia-bao, LIU Jia-bao, CUI Bao-song, LI Shuai Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . guaiacylglycerol 相似度:70% Chinese Pharmaceutical Journal 2010 45 101-103 Water-Soluble Chemical Constituents of Angelica Sinensis(Oliv.) Diels JIANG Wei, WANG Chang-hong, WANG Zheng-tao Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . (±)-1-(4-hydroxymethyl-2,5-dihydrofuran-2-yl)-5-methyl-1H-pyrimidine-2,4-dione C10H12N2O4 相似度:70% Journal of Medicinal Chemistry 2001 44 806-813 Syntheses and Structure−Activity Relationships of Novel Apio and Thioapio Dideoxydidehydronucleosides as Anti-HCMV Agents Lak Shin Jeong, Hea Ok Kim, Hyung Ryong Moon, Joon Hee Hong, Su Jeong Yoo, Won Jun Choi, Moon Woo Chun, and Chong-Kyo Lee Structure 13C NMR Structure & 13C NMR 碳谱模拟图 YB-2 1 . 愈创木-6(7)-烯-4,10-二醇 C15H26O2 相似度:60% Chinese Traditional and Herbal Drugs 2011 42 1477-1480 Chemical constituents of Patrinia scabiosaefolia GAO, Liang, ZHANG, Lin, LIU, Jiang-yun, CAI, Pei-lie, YANG, Shi-lin Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . moreli-3,9-dien-7β-ol-2-one 相似度:53.3% Journal of Natural Products 1992 Vol 55 577 Molecular Rearrangements in the Longipinene Series Luisa U. Román, Juan D. Hernández, Carlos M. Cerda-García-Rojas, Rosa María Domínguez-López, Pedro Joseph-Nathan Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . compound 3 C15H20O3 相似度:53.3% Journal of Natural Products 1992 Vol 55 577 Molecular Rearrangements in the Longipinene Series Luisa U. Román, Juan D. Hernández, Carlos M. Cerda-García-Rojas, Rosa María Domínguez-López, Pedro Joseph-Nathan Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . compound 4a 相似度:53.3% Phytochemistry 1993 32 57-60 Abscisic alcohol glucoside in quince Andrea Lutz, Peter Winterhalter Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . 9β,10β-Epoxytrichodiene 相似度:53.3% Phytochemistry 1993 32 93-104 Potential inhibitors of trichothecene biosynthesis in Fusarium culmorum: Epoxidation of a trichodiene derivative Andrew R. Hesketh, Linden gledhill, Barrie W. Bycroft, Paul M. Dewick, John Gilbert Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . (-)-10α-Hydroxy-1αH-guaia-4,6-dien-3-one 相似度:53.3% Organic Letters 2005 Vol. 7, No. 15 3291-3294 Total Syntheses of Four Stereoisomers of 4α-Hydroxy-1β,7β-peroxy-10aH-guaia-5-ene Gonzalo Blay, Begoña Garcia, Eva Molina, and José R. Pedro Structure 13C NMR Structure & 13C NMR 碳谱模拟图 YB-3 1 . Serralactone C C15H22O5 相似度:100% Helvetica Chimica Acta 2009 92 1298-1303 Four New Eudesmane Sesquiterpenoid Lactones from Chloranthus serratus Fei Teng, Hui-Min Zhong, Chang-Xiang Chen, Hai-Yang Liu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . Chloraeudolide C15H22O5 相似度:73.3% Journal of Natural Products 2011 74 16-20 Sesquiterpenes from Chloranthus japonicus Qiu-Hong Wang, Hai-Xue Kuang, Bing-You Yang, Yong-Gang Xia, Jun-Song Wang, and Ling-Yi Kong Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . 1β,4α 11α-trihydroxyeudesmane C15H28O3 相似度:66.6% Chinese Chemical Letters 2000 11 1009-1012 New Sesquiterpenoids from Hedychium yunnanense gagnep Xiu Hua LIU, Dong Bao ZHAO, Chong Ren YANG, Han Qing WANG Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . Disciferitriol C15H29O3 相似度:66.6% Journal of Asian Natural Products Research 2007 9 277-283 Sesquiterpenoids from Hedychium yunnanense and Porana discifera, and the structural revision of two sesquiterpenoids from Laggera pterodonta W.-M. ZHU, Q. ZHAO, S.-L. LI and X.-J. HAO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . disciferitriol C15H28O3 相似度:66.6% Chemistry of Natural Compounds 2014 50 732-734 Chemical Components of the Fibrous Root of Ophiopogon japonicus Tian Feng, Shen Lan, Wang ChenJie, Feng Yi, Zheng XiangWei Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . 1β,4α,13-trihydroxy-eudesm-11(12)-ene C15H26O3 相似度:60% Chemical & Pharmaceutical Bulletin 2006 54(5) 676-678 A New Eudesmane Derivative and a New Fatty Acid Ester from Sambucus williamsii Xujuan YANG,Mansau WONG,Naili WANG,Albert Sun-Chi CHAN,and Xinsheng YAO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . hedytriol C15H28O3 相似度:60% Journal of Asian Natural Products Research 2007 9 277-283 Sesquiterpenoids from Hedychium yunnanense and Porana discifera, and the structural revision of two sesquiterpenoids from Laggera pterodonta W.-M. ZHU, Q. ZHAO, S.-L. LI and X.-J. HAO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . 1β-hydroxyilicic acid C15H24O4 相似度:60% Natural Product Research 2003 17 99-102 A New Eudesmane Type Sesquiterpene from Inula Viscosa Musa H. Abu Zarga; Salim S. Sabri; Emad M. Hamed; Monther A. Khanfar; Klaus-Peter Zeller; Atta-Ur-Rahman Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . 1β,4β-dihydroxy-5α,8β-(H)-eudesm-7 相似度:60% Acta Botanica Yunnanica 2010 32 83-86 A New Phenolic Glycoside from Chloranthusmul tistachys (Chloranthaceae) RAN Xin-Hui, N I Wei, WEI Gang, CHEN Chang-Xiang, LIU Hai-Yang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . istanbulin B 相似度:60% Journal of Chinese Medicinal Materials 2005 28 292-293 草珊瑚化学成分研究 曾爱华, 罗永明 Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
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