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badhuster

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[求助] 毕业在即。微谱求助。。谢谢大家！已有1人参与

(xjc-44)
13C NMR (CDCl3, 101 MHz) δ 15.93, 20.63, 55.83, 62.68, 63.88, 74.29, 80.31, 101.23, 108.17, 108.34, 110.25, 118.64, 119.66, 121.38, 127.44, 127.53, 127.55, 130.43, 131.07, 132.05, 139.08, 139.49, 147.43, 147.71, 147.87, 151.07, 166.47, 167.66.

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分分分，植化的命根

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seuseasoar

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【答案】应助回帖

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badhuster: 金币+10 2015-04-08 21:50:50

1 .    ethyl 4-[1-(1,3-benzodioxol-5-yl)-9H-β-carbolin-3-yl]-2-oxo-6-phenyl-1,2,3,4-tetrahydropyrimidine-5-carboxylate
C31H24N4O5    相似度:58.6%
Tetrahedron       2014       70       5711-5719
Convenient synthesis of 1-aryl-9H-β-carboline-3-carbaldehydes and their transformation into dihydropyrimidinone derivatives by Biginelli reaction
Péter ábrányi-Balogh, András Dancsó, Dávid Frigyes, Balázs Volk, György Keglevich, Mátyás Milen
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
2 .    rhaponticin 6''-O-gallate
C28H28O13    相似度:57.1%
Chemical & Pharmaceutical Bulletin       1984       32       3501-3517
Studies on Rhubarb (Rhei Rhizoma). VI. Isolation and Characterization of Stilbenes
YOSHIKI KASHIWADA,GENICHIRO NONAKA and ITSUO NISHIOKA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
3 .    guaiacylglycerol-β-O-6'-(2-rnethoxy)cinnamyl alcohol ether tetraacetate
相似度:57.1%
Phytochemistry       1996       43       409-412
A lignan and four terpenoids from Brucea javanica that induce differentiation with cultured HL-60 promyelocytic leukemia cells
Lumonadio Luyengi, Nanjoo Suh, Harry H. S. Fong, John M. Pezzuto, A. Douglas Kinghorn
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
4 .    cis-N-[9,10-dimethoxy-2-(3'',4''-methylenedioxyphenyl)-4-oxo-1-phenyl-3,4,6,7-tetrahydro-2H-pyrido[2,1-a]isoquinolin-3-yl]acetamide
C30H28N2O6    相似度:57.1%
Tetrahedron       2012       68       2864-2875
Synthesis of benzoindoloquinolizines via a Cu(I)-mediated C–N bond formation
Rattana Worayuthakarn, Prattya Nealmongkol, Somsak Ruchirawat, Nopporn Thasana
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
5 .    trans-N-[9,10-dimethoxy-2-(3'',4''-methylenedioxyphenyl)-4-oxo-1-phenyl-3,4,6,7-tetrahydro-2H-pyrido[2,1-a]isoquinolin-3-yl]acetamide
C30H28N2O6    相似度:57.1%
Tetrahedron       2012       68       2864-2875
Synthesis of benzoindoloquinolizines via a Cu(I)-mediated C–N bond formation
Rattana Worayuthakarn, Prattya Nealmongkol, Somsak Ruchirawat, Nopporn Thasana
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
6 .    (2R,3R,3aR,11aR)-10-[(1,3-benzodioxol-5-yl)methyl]-2,3-(isopropylidenedioxy)-4-(p-tolylsulfonyl)-3a,4,5,10,11,11a-hexahydrofuro[3,2-b][1,5]benzodiazocine
C30H32N2O7S    相似度:57.1%
European Journal of Organic Chemistry       2010                1754-1762
Palladium-Catalyzed Intramolecular Aryl Amination Reaction: An Expeditious Approach to the Synthesis of Chiral Benzodiazocine Derivatives
Nirmal Das Adhikary and Partha Chattopadhyay
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
7 .    ethyl 4-[1-(1,3-benzodioxol-5-yl)-9H-β-carbolin-3-yl]-6-methyl-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
C26H22N4O5    相似度:57.1%
Tetrahedron       2014       70       5711-5719
Convenient synthesis of 1-aryl-9H-β-carboline-3-carbaldehydes and their transformation into dihydropyrimidinone derivatives by Biginelli reaction
Péter ábrányi-Balogh, András Dancsó, Dávid Frigyes, Balázs Volk, György Keglevich, Mátyás Milen
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
8 .    methyl 4-[1-(1,3-benzodioxol-5-yl)-9H-β-carbolin-3-yl]-6-(1-methylethyl)-2-oxo-1,2,3,4-tetrahydropyrimidine-5-carboxylate
C27H24N4O5    相似度:57.1%
Tetrahedron       2014       70       5711-5719
Convenient synthesis of 1-aryl-9H-β-carboline-3-carbaldehydes and their transformation into dihydropyrimidinone derivatives by Biginelli reaction
Péter ábrányi-Balogh, András Dancsó, Dávid Frigyes, Balázs Volk, György Keglevich, Mátyás Milen
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
9 .    trans-N-[2-(3'',4''-dimethoxyphenyl)-9,10-dimethoxy-4-oxo-1-phenyl-3,4,6,7-tetrahydro-2H-pyrido[2,1-a]isoquinolin-3-yl]benzamide
C36H34N2O6    相似度:55.1%
Tetrahedron       2012       68       2864-2875
Synthesis of benzoindoloquinolizines via a Cu(I)-mediated C–N bond formation
Rattana Worayuthakarn, Prattya Nealmongkol, Somsak Ruchirawat, Nopporn Thasana
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
10 .    phyllamyricin E
C22H18O7    相似度:53.5%
Journal of Natural Products       1996       59       1061-1065
Six Lignans from Phyllanthus myrtifolius
Shoei-Sheng Lee, Mei-Tsu Lin, Chao-Lin Liu, Yung-Yaw Lin, and Karin C. S. Chen Li
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
11 .    compound 1a
C31H26O11    相似度:53.5%
Chemical & Pharmaceutical Bulletin       1991       39       1466-1472
Studies on Nepalese Crude Drugs. XIV. New Flavonoids from the Root of Scutellaria prostrata JACQ. ex BENTH.
Yuichi KIKUCHI,Yukinori MIYAICHI and Tsuyoshi TOMIMORI
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
12 .    mananthoside A
C27H26O11    相似度:53.5%
Chinese Chemical Letters       2002       13       959-962
Two New Arylnaphthalene Lignan Glycosides from Mananthes patentiflora
Bin CHEN, Yan LIU, Chun FENG, Bo Gang LI, Guo Lin ZHANG
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
13 .    mono-O-acetyldaurinol glucoside
相似度:53.5%
Phytochemistry       1990       29       2659-2661
Two arylnaphthalene lignans from Haplophyllum buxbaumii
Yousef Al-Abed,Salim Sabri,Musa Abu Zarga,Zahir Shah,Atta-Ur-Rahman
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
14 .    (E)-3(5)-[β-(4-hydroxy-3-methoxyphenyl)-ethenyl]-5(3)-phenyl-1H-pyrazole
C18H16N2O2    相似度:53.5%
Bioorganic & Medicinal Chemistry       2009       17       1290-1296
Synthesis and biological evaluation of curcuminoid pyrazoles as new therapeutic agents in inflammatory bowel disease: Effect on matrix metalloproteinases
R.M. Claramunt, L. Bouissane, M.P. Cabildo, M.P. Cornago, J. Elguero, A. Radziwon, C. Medina
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
15 .    compound 11b
C30H28N2O6    相似度:53.5%
Tetrahedron       2012       68       2864-2875
Synthesis of benzoindoloquinolizines via a Cu(I)-mediated C–N bond formation
Rattana Worayuthakarn, Prattya Nealmongkol, Somsak Ruchirawat, Nopporn Thasana
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
16 .    compound 11e
C28H23BrN2O4    相似度:53.5%
Tetrahedron       2012       68       2864-2875
Synthesis of benzoindoloquinolizines via a Cu(I)-mediated C–N bond formation
Rattana Worayuthakarn, Prattya Nealmongkol, Somsak Ruchirawat, Nopporn Thasana
Structure    13C NMR Structure & 13C NMR    碳谱模拟图

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