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化合物1 溶剂：氘代吡啶 c谱：14.92,22.94,25.82,26.68,26.74,29.52,29.61,29.64,29.83,29.87,29.92,29.95,30.01,30.03,30.19,30.24,32.12,32.99,33.31,33.80,34.12,35,71,52.93,61.99,72.43,72.97,76.73,123.07,123.31,123.51,123.80,123.90,130.70,130.81,135.32,135.52,135.71,135.81,149.67,149.89,150.10,150.22,175.20 化合物2 溶剂：cdc13 c谱：13.76,14.15,19.20,22.72,24.70,29.08,29.26,29.39,29.46,29.61,29.67,29.68,29.72,30.58,31.95,33.84,65.60,76.77,77.03,77.28,128.86,130.94,178.84 |
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111111 1 . (2S,3S,4R)-1-O-(6-deoxy-6-(4-ethylphenyltriazol-1-yl)-α-D-galactopyranosyl)-2-hexacosylamino-octadecane-1,3,4-triol C60H108N4O8 相似度:66.6% Bioorganic & Medicinal Chemistry 2012 20 7149-7154 Synthesis of 6″-triazole-substituted α-GalCer analogues as potent iNKT cell stimulating ligands Nora Pauwels, Sandrine Aspeslagh, Dirk Elewaut, Serge Van Calenbergh Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . (2S,3R,4E)-N-(30'-(Linoleoyloxy)triacontanoyl]-1-O-(β-D-glucopyranosyl)-4-icosasphingenine C74H139NO10 相似度:65.2% European Journal of Organic Chemistry 1991 1991 529-535 Synthesis of sphingosine relatives, X. 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