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In this study, the combination of thiol-ene chemistry and the synthesis of polyurethane aqueous dispersions coatings was used to prepare a series of newly developed UV-curable polyurethane coatings. A novel UV-curable polyurethane coatings system was well established. The results proved the feasibility of the UV-curable polyurethane coatings can be prepared by blending multifunctional thiol- and ene-terminated polyurethane aqueous dispersions. Our reports illustrated the impact of the different preparation methods and technology conditions on solution stability and photopolymerization behavior of the resulting polyurethane coatings. The key factors affecting their performance of their solution stability and photopolymerization behavior were the composition, structure, thiol and ene numbers of resulting polyurethane dispersions. It was found that the resulting polyurethane coatings showed good solution stability, high photopolymerization activity and excellent physical properties by FT-IR, photo-DSC and DMA measurements. On this basis of it, new organic-inorganic nano-composite systems were well constructed by chemically doped by polyhedral oligomeric silsesquioxane (POSS), hollow SiO2 microspheres and carbon nanotubes (CNTs) with polyurethane aqueous dispersions. The results showed that the POSS, hollow SiO2 microspheres and CNTs have good compatibility and synergistic enhancement performance with polyurethane dispersions. Through the in-depth study of their microstructure, thermal, optical and mechanical properties, theoretical and experimental basis for the development of high-performance and functional polyurethane aqueous dispersions coatings were developed. 31 papers were published in journals of Polymer, Chem. Phys. Lett., Appl. Phys. Lett., Appl. Surf. Sci. and J. Appl. Polym. Sci. etc and 7 authorized and 11 pendent patents.


Ó¢ÎÄÖ÷Ìâ´ÊUV-curable; polyurethane; aqueous dispersions coatings; thiol-ene chemistry; preparation

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