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【求助】帮忙分析下孔数据
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AREA-VOLUME-PORE SIZE SUMMARY SURFACE AREA DATA Multipoint BET.............................................. 2.527E+02 m²/g Langmuir Surface Area....................................... 4.326E+03 m²/g BJH Method Cumulative Adsorption Surface Area............... 2.624E+02 m²/g BJH Method Cumulative Desorption Surface Area............... 3.032E+02 m²/g DH Method Cumulative Adsorption Surface Area................ 2.646E+02 m²/g DH Method Cumulative Desorption Surface Area................ 3.067E+02 m²/g t-Method External Surface Area.............................. 2.527E+02 m²/g t-Method Micro Pore Surface Area............................ 0.000E+00 m²/g DR Method Micro Pore Area................................... 7.362E+02 m²/g PORE VOLUME DATA Total Pore Volume for pores with Diameter less than 5043.8 Å at P/Po = 0.99622........................ 6.043E-01 cc/g BJH Method Cumulative Adsorption Pore Volume................ 6.026E-01 cc/g BJH Method Cumulative Desorption Pore Volume................ 6.200E-01 cc/g BJH Interpolated Cumulative Adsorption Pore Volume for pores in the range of 5000.0 to 0.0 Å Diamater.................... 6.026E-01 cc/g BJH Interpolated Cumulative Desorption Pore Volume for pores in the range of 5000.0 to 0.0 Å Diamater.................... 6.200E-01 cc/g DH Method Cumulative Adsorption Pore Volume................. 5.966E-01 cc/g DH Method Cumulative Desorption Pore Volume................. 6.149E-01 cc/g t-Method Micro Pore Volume.................................. 0.000E+00 cc/g DR Method Micro Pore Volume................................. 2.600E-01 cc/g PORE SIZE DATA Average Pore Diameter....................................... 9.565E+01 Å BJH Method Adsorption Pore Diameter (Mode).................. 7.743E+01 Å BJH Method Desorption Pore Diameter (Mode).................. 9.557E+01 Å DH Method Adsorption Pore Diameter (Mode).................. 7.743E+01 Å DH Method Desorption Pore Diameter (Mode).................. 9.557E+01 Å DR Method Micro Pore Width .............................. 7.013E+01 Å 请问比表面和孔径孔容到底应该看哪个啊? |
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willard
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nxl5096224(金币+1,VIP+0):多谢应助!
nxl5096224(金币+1,VIP+0):多谢应助!
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感觉数据很奇怪,t-Method Micro Pore Volume.................................. 0.000E+00 cc/g?? 为什么比表面积还很大啊? 比表面积BET和Langmuir怎么差别这么大? 有没有等温线的数据? 孔容可以用这个: Total Pore Volume for pores with Diameter less than 5043.8 Å at P/Po = 0.99622........................ 6.043E-01 cc/g [ Last edited by willard on 2008-6-5 at 22:13 ] |
2楼2008-06-05 22:08:53
dj_king
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nxl5096224(金币+1,VIP+0):多谢关注!
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是做的一种介孔(mesoporous)材料吧,不像是活性炭。 Multipoint BET.............................................. 2.527E+02 m²/g t-Method External Surface Area.............................. 2.527E+02 m²/g t-Method Micro Pore Surface Area............................ 0.000E+00 m²/g BJH Interpolated Cumulative Adsorption Pore Volume for pores in the range of 5000.0 to 0.0 Å Diamater.................... 6.026E-01 cc/g BJH Interpolated Cumulative Desorption Pore Volume for pores in the range of 5000.0 to 0.0 Å Diamater.................... 6.200E-01 cc/g Average Pore Diameter....................................... 9.565E+01 Å 最好看图。 [ Last edited by dj_king on 2008-6-5 at 22:38 ] |

3楼2008-06-05 22:16:24










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