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[求助]
求助微谱一个 已有1人参与
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氘代甲醇做的，600MHz 碳谱数据如下： 14.44,23.71,26.05,30.20,30.44,30.77,30.06,64.03,62.90,67.94,68.80,70.13,70.31,71.17,71.56,71.83,72.46,72.56,74.65,74.77,100.70,105.34 |
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杨大松
至尊木虫 (文坛精英)
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【答案】应助回帖
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感谢参与，应助指数 +1
zhaozeqing: 金币+20, ★★★很有帮助 2015-01-03 13:31:01
感谢参与，应助指数 +1
zhaozeqing: 金币+20, ★★★很有帮助 2015-01-03 13:31:01
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1 . colebroside A C47H90O14 相似度:81.8% Journal of Asian Natural Products Research 2000 2 177-185 Colebroside A, A New Diglucoside of Fatty Acid Ester of Glycerin from Clerodendrum colebrookianum HUI YANG, BE1 JIANG, AI-JUN HOU, ZHONG-WEN LINa and HAN-DONG SUN Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . β-D-Galactopyranosyl-(1→1)-6-O-palmitate-α-D-mannopyranoside C28H52O12 相似度:77.2% Bioorganic & Medicinal Chemistry 2011 19 4803-4811 Synthesis, gp120 binding and anti-HIV activity of fatty acid esters of 1, 1-linked disaccharides Stewart Bachan, Jacques Fantini, Anjali Joshi, Himanshu Garg, David R. Mootoo Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . heterosigmaglycolipid IV 相似度:72.7% Chemical & Pharmaceutical Bulletin 1992 40 1404-1410 Marine Natural Products. XXIX. Heterosigma-glycolipids I, II, III, and IV, Four Diacylglyceroglycolipids Possessing ω3-Polyunsaturated Fatty Acid Residues, from the Raphidopycean Dinoflagellate Heterosigma akashiwo Motomasa KOBAYASHI,Kozo HAYASHI,Kazuyoshi KAWAZOE and Isao KITAGAWA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . α-D-Galactopyranosyl-(1→1)-6-O-palmitate-α-D-mannopyranoside C28H52O12 相似度:72.7% Bioorganic & Medicinal Chemistry 2011 19 4803-4811 Synthesis, gp120 binding and anti-HIV activity of fatty acid esters of 1, 1-linked disaccharides Stewart Bachan, Jacques Fantini, Anjali Joshi, Himanshu Garg, David R. Mootoo Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . gingerglycolipid B C33H58O14 相似度:70.3% Chemical & Pharmaceutical Bulletin 1992 40 2239-2241 6-GINGESULFONIC ACID, A NEW ANTI-ULCER PRINCIPLE, AND GINGERGLYCOLIPIDS A, B AND C, THREE NEW MONOACYLDIGALACTOSYLGLYCEROLS, FROM ZINGIBERIS RHIZOMA ORIGINATING IN TAIWAN Masayuki YOSHIKAWA,Shoko HATAKEYAMA,Kumiko TANIGUCHI,Hisashi MATUDA and Johji YAMAHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-2-[N-(R)-2-hydroxytetracosanoyl)amino]-1,3,4-pentadecanetriol C45H89NO10 相似度:69.5% Journal of Medicinal Chemistry 1995 38 2176-2187 Structure-Activity Relationship of .alpha.-Galactosylceramides against B16-Bearing Mice Masahiro Morita, Kazuhiro Motoki, Kohji Akimoto, Takenori Natori, Teruyuki Sakai, Eiji Sawa, Kazuo Yamaji, Yasuhiko Koezuka, Eiichi Kobayashi, Hideaki Fukushima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-2-(N-hexacosanoylamino)-1,3,4-icosanetriol C52H103NO10 相似度:69.5% Journal of Medicinal Chemistry 1995 38 2176-2187 Structure-Activity Relationship of .alpha.-Galactosylceramides against B16-Bearing Mice Masahiro Morita, Kazuhiro Motoki, Kohji Akimoto, Takenori Natori, Teruyuki Sakai, Eiji Sawa, Kazuo Yamaji, Yasuhiko Koezuka, Eiichi Kobayashi, Hideaki Fukushima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . compound 13 相似度:68.1% Chemical & Pharmaceutical Bulletin 1992 40 1404-1410 Marine Natural Products. XXIX. Heterosigma-glycolipids I, II, III, and IV, Four Diacylglyceroglycolipids Possessing ω3-Polyunsaturated Fatty Acid Residues, from the Raphidopycean Dinoflagellate Heterosigma akashiwo Motomasa KOBAYASHI,Kozo HAYASHI,Kazuyoshi KAWAZOE and Isao KITAGAWA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . M-5 相似度:68.1% Chemical & Pharmaceutical Bulletin 1982 30 3544-3547 Marine Natural Products. X. Pharmacologically Active Glycolipids from the Okinawan Marine Sponge Phyllospongia foliascens (PALLAS) HIROYUKI KIKUCHI,YASUMASA TSUKITANI,TOSHITAKA MANDA,TAKASHI FUJII,HAJIME NAKANISHI,MOTOMASA KOBAYASHI and ISAO KITAGAWA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . DGDG 相似度:68.1% Natural Product Research 2006 20 766-774 Diacylglycerolipids isolated from a thermophile cyanobacterium from the Euganean hot springs Gabriele Marcolongo; Francesca De Appolonia; Alfonso Venzo; Christopher P. Berrie; Tommaso Carofiglio; Cristina Ceschi Berrini Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . 1-O-palmitoyl-3-O-[α-D-galactopyranosyl(1→6)-β-D-galactopyranosyl]-sn-glycerol C31H58O14 相似度:68.1% Natural Product Sciences 2004 10 341-343 A Monoacyldigalactosyl Glycerol from the Green Alga Enteromorpha prolifera Kim, Ju-Sun; Shim, Sang-Hee; Lee, Sang-Hyun; Chae, Sung-Wook; Han, Sang-Jun; Kang, Sam-Sik; Lee, Yeon-Sil; Jung, Sang-Hoon; Shin, Kuk-Hyun Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . (2S)-1-O-(9Z,12Z)-octadecadienoyl-2-O-(7Z,10Z)-hexa-decadienoyl-3-O-(β-D-galactopyranosyl(1-6)-β-D-galactopyranosyl)-sn-glycerol 相似度:68.1% Phytochemistry 1995 40 1433-1437 Anti-tumour-promoting glyceroglycolipids from the green alga, Chlorella vulgaris Takashi Morimoto, Akito Nagatsu, Nobutoshi Murakami, Jinsaku Sakakibara, Harukuni Tokuda, Hoyoku Nishino, Akio Iwashima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . DGDG 相似度:68.1% Phytochemistry 1995 40 1433-1437 Anti-tumour-promoting glyceroglycolipids from the green alga, Chlorella vulgaris Takashi Morimoto, Akito Nagatsu, Nobutoshi Murakami, Jinsaku Sakakibara, Harukuni Tokuda, Hoyoku Nishino, Akio Iwashima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . compound 4a+5a 相似度:68.1% Russian Chemical Bulletin 2003 52 1868-1872 New lipids from the soft corals of the Andaman Islands A.S. Dmitrenok, P. Radhika, V. Anjaneyulu, C. Subrahmanyam and P.V. Subba Rao, et al. Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 2-O-(α-D-galactopyranosyl)-1-O-(8''-hexacosanoyloxy)-D-arabino-1,2,3,4-octadecanetetrol C50H98O10 相似度:68.1% Tetrahedron 2013 69 7438-7447 Design and synthesis of new KRN7000 analogues Original Research Article Man Sun, Yuhang Wang, Xin-Shan Ye Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . 2-hydroxy-3-(octadecyloxy)-propyl-α-D-fucopyranoside C27H54O7 相似度:68.1% Indian Journal of Chemistry Section B 2000 39B 121-124 A new lipid glycoside from two sinularia species of Andaman and Nicobar islands V Anjaneyulu, P V Subba Rao, P Radhika Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . (2S,3R,4R)-2-[(2'R,3'R,4'R)-2',3',4'-(trihydroxy)hex-acosanoyloxy]-3,4-(dihydroxy)octadecyl α-D-galactopyranoside C50H98O12 相似度:68% Tetrahedron 2013 69 9710-9725 Synthesis and biological activity of hydroxylated analogs of RCAI-80 Original Research Article Masao Shiozaki, Takuya Tashiro, Hiroyuki Koshino, Tomokuni Shigeura, Hiroshi Watarai, Masaru Taniguchi, Kenji Mori Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . gingerglycolipid C C33H60O14 相似度:66.6% Chemical & Pharmaceutical Bulletin 1992 40 2239-2241 6-GINGESULFONIC ACID, A NEW ANTI-ULCER PRINCIPLE, AND GINGERGLYCOLIPIDS A, B AND C, THREE NEW MONOACYLDIGALACTOSYLGLYCEROLS, FROM ZINGIBERIS RHIZOMA ORIGINATING IN TAIWAN Masayuki YOSHIKAWA,Shoko HATAKEYAMA,Kumiko TANIGUCHI,Hisashi MATUDA and Johji YAMAHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . Agelasphin-7a C46H90NO10 相似度:66.6% Tetrahedron Letters 1993 34 5591-5592 Agelasphins, novel α-galactosylceramides from the marine sponge Agelas mauritianus Takenori Natori, Yasuhiko Koezuka, Tatsuo Higa Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . (2S,3S,4R)-1-O-(α-D-Galactosyl)-6-oxa-2-tetracosanoy lamino-1,3,4-nonanetriol C38H75NO10 相似度:66.6% Bioorganic & Medicinal Chemistry 2012 20 2850-2859 Synthesis and biological evaluation of truncated α-galactosylceramide derivatives focusing on cytokine induction profile Tetsuya Toba, Kenji Murata, Junko Futamura, Kyoko Nakanishi, Bitoku Takahashi, Naohiro Takemoto, Minako Tomino, Takashi Nakatsuka, Seiichi Imajo, Megumi Goto, Takashi Yamamura, Sachiko Miyake, Hirokazu Annoura Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . (2S,3S,4R)-1-O-(α-D-Galactosyl)-6-oxa-2-tetracosanoy lamino-1,3,4-octadecanetriol C47H93NO10 相似度:66.6% Bioorganic & Medicinal Chemistry 2012 20 2850-2859 Synthesis and biological evaluation of truncated α-galactosylceramide derivatives focusing on cytokine induction profile Tetsuya Toba, Kenji Murata, Junko Futamura, Kyoko Nakanishi, Bitoku Takahashi, Naohiro Takemoto, Minako Tomino, Takashi Nakatsuka, Seiichi Imajo, Megumi Goto, Takashi Yamamura, Sachiko Miyake, Hirokazu Annoura Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-2-[N-(R)-2-hydroxytetracosanoyl)amino]-1,3,4-octadecanetriol C48H95NO10 相似度:66.6% Journal of Medicinal Chemistry 1995 38 2176-2187 Structure-Activity Relationship of .alpha.-Galactosylceramides against B16-Bearing Mice Masahiro Morita, Kazuhiro Motoki, Kohji Akimoto, Takenori Natori, Teruyuki Sakai, Eiji Sawa, Kazuo Yamaji, Yasuhiko Koezuka, Eiichi Kobayashi, Hideaki Fukushima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-2-(N-hexacosanoylamino)-1,3,4-octadecanetriol C50H99NO10 相似度:66.6% Journal of Medicinal Chemistry 1995 38 2176-2187 Structure-Activity Relationship of .alpha.-Galactosylceramides against B16-Bearing Mice Masahiro Morita, Kazuhiro Motoki, Kohji Akimoto, Takenori Natori, Teruyuki Sakai, Eiji Sawa, Kazuo Yamaji, Yasuhiko Koezuka, Eiichi Kobayashi, Hideaki Fukushima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . (2S,3S,4R)-1-O-(α-D-galactopyranosyl)-2-(N-hexacosanoylamino)-1,3,4-nonadecanetriol C51H101NO10 相似度:66.6% Journal of Medicinal Chemistry 1995 38 2176-2187 Structure-Activity Relationship of .alpha.-Galactosylceramides against B16-Bearing Mice Masahiro Morita, Kazuhiro Motoki, Kohji Akimoto, Takenori Natori, Teruyuki Sakai, Eiji Sawa, Kazuo Yamaji, Yasuhiko Koezuka, Eiichi Kobayashi, Hideaki Fukushima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . vesparioside 相似度:66.6% European Journal of Organic Chemistry 2005 2005 368-373 Vesparioside from the Marine Sponge Spheciospongia vesparia, the First Diglycosylceramide with a Pentose Sugar Residue Valeria Costantino, Ernesto Fattorusso, Concetta Imperatore and Alfonso Mangoni Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . 1-O-(α-D-galactopyranosyl)-2-O-(8'-octyl)-D-ribo-1,2,3,4-octadecanetetrol C32H64O9 相似度:65.3% Tetrahedron 2013 69 7438-7447 Design and synthesis of new KRN7000 analogues Original Research Article Man Sun, Yuhang Wang, Xin-Shan Ye Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 27 . 6-O-stearoylraffinose 相似度:65.3% European Food Research and Technology 2013 237 237-244 Synthesis and characterization of raffinose fatty acid monoesters under ultrasonic irradiation Yuyun Lu, Rian Yan, Xiang Ma, Yong Wang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 28 . 8-p-Methoxyphenoxyloctyl 2-acetamido-2-deoxy-6-O-(β-D-galactopyranosyl)-β-D-glucopyranoside 相似度:65.2% Bioorganic & Medicinal Chemistry 1996 4 683-692 Towards oligosaccharide libraries: A study of the random galactosylation of unprotected N-acetylglucosamine Yili Ding, Jill Labbe, Osamu Kanie, Ole Hindsgaul Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
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