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[求助]
溶剂为氘带甲醇 已有1人参与
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| 13C-NMR从小到大排列为：23.4,30.9,42.5,63.0,69.1,71.9,75.3,75.4,77.8,78.4,99.4,99.7,115.9,144.6 |
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杨大松
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【答案】应助回帖
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夏柘的天空: 金币+15, ★★★★★最佳答案 2014-12-30 17:33:29
感谢参与，应助指数 +1
夏柘的天空: 金币+15, ★★★★★最佳答案 2014-12-30 17:33:29
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1 . (2E)-2,6-Dimethylocta-2,7-dien-1,6-diol-6-O-β-D-glucopyranoside 相似度:75% Helvetica Chimica Acta 1993 76 2563-2569 Anatolioside E: A New Acyclic Monoterpene Glycoside from Viburnum orientale Ihsan Çaliş, Ayşen Yürüker, Heinz Rüegger, Anthony D. Wright and Otto Sticher Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . (3S)-8-hydroxylinaloyl β-D-glucopyranoside C16H28O7 相似度:68.7% Carbohydrate Research 1997 301 123-143 First total synthesis of two new diglycosides, neohancosides A and B, from Cynanchum hancockianum Yaeko Konda, Tsuneyuki Toida, Eisuke Kaji, Kazuyoshi Takeda, Yoshihiro Harigaya Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 9-hydroxylinaloyl glucoside C16H28O7 相似度:66.6% Phytochemistry 1989 28 3369-3372 Terpenic glycosides from Pluchea indica Taketo Uchiyama,Toshio Miyase,Akira Ueno,Khan Usmanghani Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . linalyl β-D-glucopyranoside 相似度:62.5% Phytochemistry 1994 37 543-546 A phenylpropanoid glucoside from Perilla frutescens Tomoyuki Fujita, Atsunori Funayoshi, Mitsuru Nakayama Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . (3S)-3-O-(β-D-Glucopyranosyl)-3,7-dimethylocta-1,5-dien-3-ol C16H28O6 相似度:62.5% Bulletin of the Korean Chemical Society 2003 24 1475-1477 A New Monoterpene Glucoside from Portulaca oleracea Youngwan Seo, Jongheon Shin, Hyo Jun Cha, You-Ah Kim, Jong-Woong Ahn, Burm-Jong Lee, Dong Seok Lee Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . (3S)-3-O-(β-D-Glucopyranosyl)-3,7-dimethylocta-1,5-dien-3,7-diol C16H28O7 相似度:62.5% Bulletin of the Korean Chemical Society 2003 24 1475-1477 A New Monoterpene Glucoside from Portulaca oleracea Youngwan Seo, Jongheon Shin, Hyo Jun Cha, You-Ah Kim, Jong-Woong Ahn, Burm-Jong Lee, Dong Seok Lee Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . (3S)-linaloyl β-D-glucopyranoside C16H28O6 相似度:62.5% Carbohydrate Research 1997 301 123-143 First total synthesis of two new diglycosides, neohancosides A and B, from Cynanchum hancockianum Yaeko Konda, Tsuneyuki Toida, Eisuke Kaji, Kazuyoshi Takeda, Yoshihiro Harigaya Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . Cnidioside C 相似度:62.5% Shoyakugaku Zasshi 1993 47 74-78 Studies on the Constituents of Cnidii Monnieri Fructus YAHARA SHOJI, SUGIMURA CHIZUKO, NOHARA TOSHIHIRO, NIIHO YUJIRO, NAKAJIMA YOSHIJIRO, ITO HIROSHI Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . (3S,6E)-8-hydroxylinalool 3-O-β-D-glucopyranoside C16H28O7 相似度:62.5% Chinese Journal of Medicinal Chemistry 2013 23 480-485 Isolation and identification of constituents from Leonurus japonicus Ⅱ ZHANG Yi, DENG Shen, LI Xiao-xia, CHEN Yue, HAN Li-feng, WANG Tao Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . (2E,6S)-6-hydroxy-2-hydroxymethyl-6-methyl-2,7-octadienoic acid 6-O-β-D-quinovopyranoside C16H26O8 相似度:60% Journal of Natural Products 2009 72 632-639 Cytotoxic Oleanane Triterpene Saponins from Albizia chinensis Rui Liu,Shuanggang Ma,Shishan Yu,Yuehu Pei, Sen Zhang,Xiaoguang Chen, and Jianjun Zhang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . monoterpene glycoside 相似度:60% Journal of Natural Products 2008 71(1) 41-46 Cytotoxic Triterpenoid Saponins Acylated with Monoterpenic Acid from Pithecellobium lucidum Shuang Gang Ma, You Cai Hu, Shi Shan Yu, Yi Zhang, Xiao Guang Chen, Jing Liu, and Yu Xi Liu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . 6-epiaucubin 相似度:60% Planta Medica 1982 46 33-37 Iridoids in Equatorial and Tropical Flora Part Isolation of Amareloside Armando Bianco, Pietro Passacantilli, Marcello Nicoletti and Roberto Alves de Lima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 6-epi-aucubin 相似度:60% Phytochemistry 1995 40 491-494 Iridoids in roots of Pedicularis chinensis Yang Li, Wang Changzeng, Jia Zhongjian Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . decarbomethoxyloganin 相似度:60% Phytochemistry 1994 35 1485-1487 Iridoids of Rauwolfia grandiflora Armandodoriano Bianco, Angelo de Luca, Raffaele Antonio Mazzei, Marcello Nicoletti, Pietro Passacantilli, Roberto Alves De Lima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 6-epiaucubin C15H22O9 相似度:60% Tetrahedron 1982 38 359-362 Iridoids in equatorial and tropical flora—III : Isolation and partial synthesis of 6-epiaucubin a new glucosidic iridoid Original Research Article A. Bianco, P. Passacantilli, M. Nicoletti, R. Alves De Lima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . 1-hydroxylinaloyl-6-O-β-D-glucopyranoside 相似度:58.8% Turkish Journal of Chemistry 2003 27 703-711 Phenolic, Megastigmane, Nucleotide, Acetophenon and Monoterpene Glycosides from Phlomis samia and P. carica FUNDA NURAY YALÇIN, TAYFUN ERSÖZ, PINAR AKBAY, İHSAN ÇALIŞ, ALİ ARSLAN DÖNMEZ, OTTO STICHER Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . epi-vogeloside 相似度:58.8% Journal of Chinese Medicinal Materials 2012 35 1789-1792 Chemical Constituents of Dipsacus asper YANG Zi-gang, DING Kun, XU Gang, SHEN Yong, MENG Zhen-gui, YANG Sheng-chao Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . epi-vogeloside 相似度:58.8% China Journal of Chinese Materia Medica 2011 36 1613-1619 Chemical constitutents from pre-formulation of Lonicerae Japonicae Flos in Shuanghuanglian lyophilized powder for injection WANG, Nan, YANG, Xiuwei Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . creoside II C14H26O7 相似度:57.1% Chemical & Pharmaceutical Bulletin 2008 56(4) 536-540 Bioactive Constituents from Chinese Natural Medicines. XXVIII.1) Chemical Structures of Acyclic Alcohol Glycosides from the Roots of Rhodiola crenulata Seikou NAKAMURA, Xuezheng LI, Hisashi MATSUDA, and Masayuki YOSHIKAWA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . hexane-1,5-diol 1-O-β-D-glucopyranoside C21H24O7 相似度:57.1% Phytochemistry 2003 609-616 Aromatic compound glucosides, alkyl glucoside and glucide from the fruit of anise Eiko Fujimatu, Toru Ishikawa, Junichi Kitajima Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
2楼2014-12-26 14:57:48
