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化合物1 13C谱 MeOD 12.76,16.92,18.16,18.90,20.20,21.20,24.06,26.08,26.20,32.09,32.31,33.94,35.21,35.97,37.04,38.51,39.22,42.96,44.07,46.49,47.56,47.92,53.06,53.98,64.53,65.35,71.74,72.91,73.10,73.39,75.37,82.92,85.69,106.14,130.53,134.23 化合物2 13C MeOD 12.764,17.426,18.053,19.417,19.542,22.575,24.998,25.756,26.758,32.491,33.379,33.416,33.682,36.297,37.780,39.603,39.852,42.388,42.885,44.552,45.874,48.629,55.349,65.201,65.496,69.535,72.247,73.436,73.614,75.893,83.650,106.642,127.149,127.561,133.148,137.748 万分感谢！！！ |
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compound 1 1 . 3-O-β-D-fucopyranosylsaikogenin F C36H58O8 相似度:91.6% Chemical & Pharmaceutical Bulletin 1986 34 1158-1167 Chemical Evaluation of Bupleurum Species Collected in Yunnan, China JING-KAI DING,HIROKO FUJINO(nee KIMATA),RYOJI KASAI,NAOKO FUJIMOTO,OSAMU TANAKA,JUN ZHOU,HIROMICHI MATSUURA and TOHRU FUWA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . prosaikogenin F 相似度:91.6% Journal of Chinese Pharmaceutical Sciences 1999 8 105-107 Studies on the Chemical Constituents of the Roots from Bupleurum scorzonerifolium Bat Yaming; Zhao Yuying; Tan Li and Zhang Ruyi Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . prosaikogenin F 相似度:88.8% Chemical & Pharmaceutical Bulletin 1985 33 3349-3355 New Derivatives of Saikosaponins KOJI SHIMIZU,SAKAE AMAGAYA and YUKIO OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . clinoposaponin IX 相似度:83.3% Phytochemistry 1994 36 1485-1488 Oleanane-triterpene saponins from Clinopodium chinense var. Parviflorum Fumie Mori, Toshio Miyase, Akira Ueno Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . Prostratoside J 相似度:83.3% Chinese Traditional and Herbal Drugs 2003 34 388-390 Two new monoglycosides from Polycarpon prostratum DING Zhong-tao; YANG Xue-qiong; BAO Zhi-juan; YE Jing-ru Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . corchorusin B C36H58O9 相似度:80.5% Journal of the Chemical Society, Perkin Transactions 1 1987 629-634 Triterpenoid glycosides of Corchorus acutangulus Lam. Shashi B. Mahato and Bikas C. Pal Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . clinoposaponin XIII C36H58O9 相似度:75% Chemical & Pharmaceutical Bulletin 1997 45 1493-1497 Saikosaponin Homologues from Clinopodium spp. The Structures of Clinoposaponins XII-XX Toshio MIYASE and Yukari MATSUSHIMA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . 3β,16α,23,28,30-pentahydroxyoleana-11,13(18)-diene 3-O-β-D-fucopyranoside C36H58O9 相似度:75% Natural Product Communications 2008 3 155-157 Saikosaponins from Bupleurum chinense and Inhibition ofHBV DNA Replication Activity Feng Yin, Ruixiang Pan, Rongmin Chen and Lihong Hu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . prosaikogenin E-3 相似度:72.2% Chemical & Pharmaceutical Bulletin 1989 37 1293-1296 New Derivatives of Saikosaponin c Mitsuhiko NOSE,Sakae AMAGAYA,Tadahiro TAKEDA and Yukio OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . prosaikogenin G 相似度:72.2% Chemical & Pharmaceutical Bulletin 1985 33 3349-3355 New Derivatives of Saikosaponins KOJI SHIMIZU,SAKAE AMAGAYA and YUKIO OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 compound 2 1 . Saikosaponin b2 相似度:76.3% Archives of Pharmacal Research 1989 12 226-228 Phenolic compounds of the roots of Bupleurum longeradiatum Jae Sue Choi and Won Sick Woo Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . prosaikogenin D C36H58O8 相似度:75% Chemical & Pharmaceutical Bulletin 1985 33 3349-3355 New Derivatives of Saikosaponins KOJI SHIMIZU,SAKAE AMAGAYA and YUKIO OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . cauloside B C35H56O9 相似度:72.2% Journal of Agricultural and Food Chemistry 2001 49 5969-5974 Characterization of the Triterpene Saponins of the Roots and Rhizomes of Blue Cohosh (Caulophyllum Thalictroides) Jin-Woo Jhoo, Shengmin Sang, Kan He, Xiaofang Cheng, Nanqun Zhu, Ruth E. Stark, Qun Yi Zheng, Robert T. Rosen, and Chi-Tang Ho Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . leontoside A 相似度:66.6% Planta Medica 1993 59 461-464 A New Bidesmosidic Triterpenoidal Saponin from the Roots of Symphytum officinale Viqar Uddin Ahmad , Faryal Vali Mohammad, Mushtaq Noorwala', and Bilge Sener Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . polygalasaponin XXV C36H56O10 相似度:66.6% Chemical & Pharmaceutical Bulletin 1996 44 173-179 Studies on the Constituents of Polygala japonica HOUTT. III. Structures of Polygalasaponins XX-XXVII Dongming ZHANG,Toshio MIYASE,Masanori KUROYANAGI,Kaoru UMEHARA and Akira UENO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . compound 4b 相似度:66.6% Chemical & Pharmaceutical Bulletin 1994 42 1874-1878 Five New Triterpene Glycosides from Russell Lupine Junei KINJO,Fumiko KISHIDA,Kazutaka WATANABE,Fumio HASHIMOTO and Toshihiro NOHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . prosaikogenin A 相似度:66.6% Phytochemistry 1996 42 1673-1675 Triterpenoid saponins from Bupleurum smithii var. parvifolium Yu-ying Zhao, He-sheng Luo, Bin Wang, Li-bin Ma, Guang-zhong Tu, Ru-yi Zhang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . Kudinoside C35H52O8 相似度:66.6% Phytochemistry 1996 41 871-877 Triterpenes and triterpenoid glycosides from the leaves of Ilex kudincha Ming-An Ouyang, Chong-Ren Yang, Zi-Li Chen, Han-Qing Wang Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . 23-hydroxylongispinogenin 3-O-β-D-glucopyranoside C36H60O9 相似度:66.6% Natural Product Communications 2012 7 705-708 Two Antiproliferative Saponins of Tarenna grevei from the Madagascar Dry Forest Liva Harinantenaina, Peggy J. Brodie, Martin W. Callmander, L. Jérémie Razafitsalama, Vincent E. Rasamison, Etienne Rakotobe and David G. I. Kingston Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . 3β,16α,23,28,30-pentahydroxyoleana-11,13(18)-diene 3-O-β-D-fucopyranoside C36H58O9 相似度:66.6% Natural Product Communications 2008 3 155-157 Saikosaponins from Bupleurum chinense and Inhibition ofHBV DNA Replication Activity Feng Yin, Ruixiang Pan, Rongmin Chen and Lihong Hu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 11 . cauloside A C35H56O8 相似度:66.6% Journal of Agricultural and Food Chemistry 2001 49 5969-5974 Characterization of the Triterpene Saponins of the Roots and Rhizomes of Blue Cohosh (Caulophyllum Thalictroides) Jin-Woo Jhoo, Shengmin Sang, Kan He, Xiaofang Cheng, Nanqun Zhu, Ruth E. Stark, Qun Yi Zheng, Robert T. Rosen, and Chi-Tang Ho Structure 13C NMR Structure & 13C NMR 碳谱模拟图 12 . Pleurosaponin F C36H60O9 相似度:66.6% Chemical & Pharmaceutical Bulletin 2012 60 1011-1018 Triterpene Saponins from Pleurospermum kamtschaticum and Their Biological Activity Il Kyun Lee, Sang Un Choi, Kang Ro Lee Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
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