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xqiuqiuľ³æ (ÕýʽдÊÖ)
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[ÇóÖú]
΢Æ×ÇóÖú£¬·Ç³£¸Ðл£¡ ÒÑÓÐ1È˲ÎÓë
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| 13C NMR (151 MHz, DMSO) ¦Ä 212.04, 183.43, 177.87, 144.49, 144.31, 141.96, 138.05, 134.75, 131.68, 131.27, 130.46, 129.25, 127.84, 127.38, 126.83, 108.90, 74.01, 61.04, 48.46, 43.25, 39.52, 24.35, 18.77, 12.87, 6.93. |
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xqiuqiu: ½ð±Ò+10, ¡ïÓаïÖú 2014-12-19 20:34:51
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1 . 1-Benzylapomorphine HCl C24H24ClNO2 ÏàËÆ¶È:56% Bioorganic & Medicinal Chemistry 2013 21 4143-4150 1-substituted apomorphines as potent dopamine agonists Reet Reinart-Okugbeni, Argo Vonk, Ain Uustare, Zsuzsanna Gyulai, Attila Sipos, Ago Rinken Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 2 . (S)-5-(4-{1-ethyl-1-[4-(3-ethyl-3-hydroxypentyl)-3-methyl phenyl]-propyl}-2-methylphenoxymethyl)-dihydrofuran-2-one ÏàËÆ¶È:55.5% Bioorganic & Medicinal Chemistry 2012 20 4495-4506 Systematic SAR study of the side chain of nonsecosteroidal vitamin D3 analogs Hirotaka Kashiwagi, Yoshiyuki Ono, Masateru Ohta, Kenji Morikami, Tadakatsu Takahashi Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 3 . compound 31 C38H46O4SSi ÏàËÆ¶È:55.5% The Journal of Organic Chemistry 2002 67 7750-7760 Total Synthesis of Rhizoxin D, a Potent Antimitotic Agent from the Fungus Rhizopus chinensis James D. White, Paul R. Blakemore, Neal J. Green, E. Bryan Hauser, Mark A. Holoboski, Linda E. Keown, Christine S. Nylund Kolz, and Barton W. Phillips Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 4 . (-)-3-Benzoyl-1-[(1R,2R,5S)-5-(tert-butyl-diphenylsilanyloxymethyl) bicyclo[3.1.0]hex-3-en-2-yl)-5-methylpyrimidine-2,4(1H,3H)-dione C35H36N2O4Si ÏàËÆ¶È:55.5% Bioorganic & Medicinal Chemistry 2011 19 3945-3955 Synthesis of enantiomerically pure d-and l-bicyclo[3.1.0]hexenyl carbanucleosides and their antiviral evaluation Ah-Young Park, Won Hee Kim, Jin-Ah Kang, Hye Jin Lee, Chong-Kyo Lee, Hyung Ryong Moon Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 5 . (-)-3-Benzoyl-1-[(1R,2R,5S)-5-(tert-butyl-diphenylsilanyloxymethyl) bicyclo[3.1.0]hex-3-en-2-yl]pyrimidine-2,4(1H,3H)-dione C34H34N2O4Si ÏàËÆ¶È:53.8% Bioorganic & Medicinal Chemistry 2011 19 3945-3955 Synthesis of enantiomerically pure d-and l-bicyclo[3.1.0]hexenyl carbanucleosides and their antiviral evaluation Ah-Young Park, Won Hee Kim, Jin-Ah Kang, Hye Jin Lee, Chong-Kyo Lee, Hyung Ryong Moon Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 6 . (2E,4R,5S,6R,7E)-5-(benzyloxy)-8-((tert-butyldiphenylsilyloxy)methyl)-6-ethyl-4-methyldeca-2,7-dienal C37H48O3Si ÏàËÆ¶È:52% Organic Letters 2005 Vol. 7, No. 25 5569-5572 Toward a Total Synthesis of the Novel Polyketide Natural Product Spiculoic Acid A Goverdhan Mehta and Uday Kumar Kundu Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 7 . 1-(2-bromobenzyl)-7-benzyloxy-5,6-dimethoxy-1,2,3,4-tetrahydroisoquinoline C25H26BrNO3 ÏàËÆ¶È:52% Chemical & Pharmaceutical Bulletin 2009 57 368-376 First Total Syntheses of (¡À)-Isopiline, (¡À)-Preocoteine, (¡À)-Oureguattidine and (¡À)-3-Methoxynordomesticine and the Biological Activities of (¡À)-3-Methoxynordomesticine Surachai Nimgirawath, Phansuang Udomputtimekakul, Thongchai Taechowisan, Asawin Wanbanjob and Yuemao Shen Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 8 . 2-acetylbenz oylmethylene-3-[1-methoxy-1-(4-methoxyphenacyl)methyl ene]tropone C28H24O6 ÏàËÆ¶È:52% Heterocycles 2004 62 667-677 Reactions of 4-Methoxy-2-(4-methoxyphenyl)-9-oxocycloheptapyrylium Perchlorate with Active Methylene Compounds Dao-Lin Wang and Kimiaki Imafuku* Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 9 . 4-Phenyl-2-thienyl-4H-benzo[f]chromene-3-carbothioic acid O-ethyl ester C26H20O2S2 ÏàËÆ¶È:52% Tetrahedron 2012 68 1247-1252 Highly convergent one-pot four-component regioselective synthesis of 4H-benzo[f]chromenes via annulation of ¦Â-oxodithioesters Subhasis Samai, Ganesh Chandra Nandi, Maya Shankar Singh Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 10 . 2,2-Dimethyl-1',5-diphenyl-4,5-dihydro-2H-spiro[furan-3,3'-indolin]-2'-one C25H23NO2 ÏàËÆ¶È:52% Tetrahedron 2012 68 1483-1491 Synthesis of spiro[furan-3,3'-indolin]-2'-ones by PET-catalyzed [3+2] reactions of spiro[indoline-3,2'-oxiran]-2-ones with electron-rich olefins Lihong Wang, Zhanshan Li, Lianhong Lu, Wei Zhang Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 11 . 2-Phenyl-5,7-di(m-tolyl)-4H-chromen-4-one C29H22O2 ÏàËÆ¶È:52% European Journal of Organic Chemistry 2012 1639-1652 Efficient Synthesis of Arylated Flavones by Site-Selective Suzuki¨CMiyaura Cross-Coupling Reactions of the Bis(triflate) of 5,7- and 7,8-Dihydroxyflavone Nadi Eleya, Imran Malik, Sebastian Reimann, Kai Wittler, Martin Hein, Tam¨¢s Patonay, Alexander Villinger, Ralf Ludwig and Peter Langer Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 12 . 2-(4-((1H-1,2,4-triazol-1-yl)methyl)-5-(4-bromophenyl)-1-(2,4-dichlorophenyl)-1H-pyrazol-3-yl)-5-(1-p-tolylcyclopropyl)-1,3,4-thiadiazole C30H22BrCl2N7S ÏàËÆ¶È:52% Bioorganic & Medicinal Chemistry 2010 18 6377-6388 Discovery of 2-(4-((1H-1, 2, 4-triazol-1-yl)methyl)-5-(4-bromophenyl)-1-(2-chlorophenyl)-1H-pyrazol-3-yl)-5-tert-butyl-1, 3, 4-thiadiazole (GCC2680) as a potent, selective and orally efficacious cannabinoid-1 receptor antagonist Jinhwa Lee, Hee Jeong Seo, Suk Ho Lee, Jeongmin Kim, Myung Eun Jung, Sung-Han Lee, Kwang-Seop Song, Junwon Lee, Suk Youn Kang, Min Ju Kim, Mi-Soon Kim, Eun-Jung Son, MinWoo Lee, Ho-Kyun Han Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 13 . dl-(4R,5R)-ethyl 1-(4-bromobenzyl)-2,4,5-triphenyl-4,5-dihydro-1H-imidazole-4-carboxylate C31H27N2O2Br ÏàËÆ¶È:52% Bioorganic & Medicinal Chemistry 2009 17 3093-3103 Structural¨Cactivity relationship study of highly-functionalized imidazolines as potent inhibitors of nuclear transcription factor-¦ÊB mediated IL-6 production Daljinder K. Kahlon, Theresa A. Lansdell, Jason S. Fisk, Jetze J. Tepe Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 14 . ethyl 1,1'-dibenzyl-2,5'-dioxo-1,2-dihydrospiro[indole-3,3'-pyrrolidine]-2'-carboxylate C28H26N2O4 ÏàËÆ¶È:52% European Journal of Organic Chemistry 2011 5303-5310 Diastereoselective Access to Tri- and Pentacyclic Spiro--lactam-oxindole Cores through a Tandem Aza-Michael Initiated Ring Closure Sequence Iyad Allous, S¨¦bastien Comesse, Morgane Sanselme and Adam Daïch Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 15 . (1E,3E,NE)-N-(1-benzyl-2-oxoindolin-3-ylidene)-3-(ethoxycarbonyl)-4-(4-(trifluoromethyl)phenyl)buta-1,3-dien-1-amine C29H23F3N2O4 ÏàËÆ¶È:52% Tetrahedron 2013 69 3593-3607 Nitrogen-containing Lewis bases catalyzed highly regio- and stereoselective reactions of allenyl acetates with isatin-derived oximes Yuan-Liang Yang, Yin Wei, Qin Xu, Min Shi Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 16 . (5S*,6aS*)-6,6a-dihydro-10-phenyl-5-(N-pyrrolidine-2-one)isoindolo[2,1-a]quinoline-11(5H)-one C26H22N2O2 ÏàËÆ¶È:52% Journal of Heterocyclic Chemistry 2013 50 E18-E38 5-Amido- and 5-Amino-Substituted Epoxyisoindolo[2,1-a]tetrahydroquinolines and 10-Carboxylic Acids: Their Synthesis and Reactivity Vladimir P. Zaytsev, Fedor I. Zubkov, Flavien A. A. Toze, Daria N. Orlova, Maria N. Eliseeva, Dmitry G. Grudinin, Eugeniya V. Nikitina and Alexey V. Varlamov Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ 17 . (3S,3'S)-1-methyl-6'-phenyl-3'-propionyl-1'-tosyl-2',3'-dihydro-1'H-spiro[indoline-3,4'-pyridin]-2-one C29H28N2O4S ÏàËÆ¶È:52% Tetrahedron 2014 70 2838-2846 Access to 2¡ä,3¡ä-dihydro-1¡äH-spiro[indoline-3,4¡ä-pyridin]-2-ones via amino acid derived phosphine-catalyzed asymmetric [4+2] annulation with easily available oxindole-derived ¦Á,¦Â-unsaturated imines Original Research Article Xiao-Nan Zhang, Xiang Dong, Yin Wei, Min Shi Structure 13C NMR Structure & 13C NMR ̼Æ×Ä£Äâͼ |

2Â¥2014-12-18 15:27:58
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