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The original Handbook of Surface and Interface Analysis: Methods for Problem-Solving was based on the authors¡¯ firm belief that characterization and analysis of surfaces should be conducted in the context of problem solving and not be based on the capabilities of any individual technique. Now, a decade later, trends in science and technology appear to have validated their assertions.
Major instrumental assets are generally funded and maintained as central facilities to help potential users make informed decisions about their appropriate use in solving analytical problem(s). Building on the popular first edition, this long-awaited second edition was motivated by the increasingly common industry view that it is more cost-effective to contract out analytical services than to maintain in-house facilities. Guided by that trend, this book focuses on developing strategic thinking for those who decide which facilities to access and where to subcontract analytical work. It covers most of the major tactical issues that are relevant at the location in which data are being produced.
New Information in this Second Edition Includes:
Electron-optical imaging techniques and associated analytical methods
Techniques based on synchrotron sources
Convenient and versatile scanning probe group methods
Scanning tunneling microscopy, biocompatible materials, and nano-structured materials
Assessing benefits and limitations of different methodologies, this volume provides the essential physical basis and common modes of operation for groups of techniques. Exploring methods for characterization and analysis of particular types of materials and/or their relevant applications¡ªthe text synergizes traditional and novel ideas to help readers develop a versatile and rational approach to surface and interface analysis.
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Auger Electron Spectroscopy
(AES), and Ion Scattering Spectroscopy (ISS) .......................................................... 19
Vaneica Y. Young and Gar B. Hofl und
Chapter 4 Ion Beam Techniques: Time-of-Flight Secondary Ion Mass Spectrometry
(ToF-SIMS) ................................................................................................................65
Birgit Hagenhoff, Reinhard Kersting, and Derk Rading
Chapter 5 Surface and Interface Analysis by Scanning Probe Microscopy ...............................97
Sverre Myhra
Chapter 6 Transmission Electron Microscopy: Instrumentation, Imaging Modes,
and Analytical Attachments ..................................................................................... 139
John M. Titchmarsh
Chapter 7 Synchrotron-Based Techniques ................................................................................ 193
Andrea R. Gerson, David J. Cookson, and Kevin C. Prince
Chapter 8 Quantifi cation of Surface and Near-Surface Composition by AES and XPS ..........223
Sven Tougaard
Chapter 9 Structural and Analytical Methods for Surfaces and Interfaces:
Transmission Electron Microscopy ..........................................................................245
John M. Titchmarsh
Chapter 10 In-Depth Analysis/Profi ling ..................................................................................... 281
François Reniers and Craig R. Tewell
Chapter 11 Characterization of Nanostructured Materials ......................................................... 319
Matthias Werner, Alison Crossley, and Colin Johnston
Chapter 12 Problem-Solving Methods in Tribology with Surface-Specifi c Techniques ............ 351
Christophe Donnet and Jean-Michel Martin
Chapter 13 Problem-Solving Methods in Metallurgy with Surface Analysis ............................ 389
R. K. Wild
Chapter 14 Composites ............................................................................................................... 421
Peter M. A. Sherwood
Chapter 15 Minerals, Ceramics, and Glasses ............................................................................. 457
Roger St. C. Smart and Zhaoming Zhang
Chapter 16 Catalyst Characterization ......................................................................................... 501
Wolfgang E. S. Unger and Thomas Gross
Chapter 17 Surface Analysis of Biomaterials ............................................................................. 529
Marek Jasieniak, Daniel Graham, Peter Kingshott, Lara J. Gamble,
and Hans J. Griesser
Chapter 18 Adhesion Science and Technology ...........................................................................565
John F. Watts
Chapter 19 Electron Spectroscopy in Corrosion Science ...........................................................603
James E. Castle
Index .............................................................................................................................................. 635
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