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jgtgdzd22银虫 (小有名气)
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Structures were solved with direct methods using SHELXL-97 and refined by full matrix least-squares methods on F2with SHELXL-97. Nonhydrogen atoms were refined with anisotropic thermal parameters. All hydrogen atoms were geometrically fixed and allowed to refine using a riding model. Atomic coordinates, bond angles, bond lengths, and thermal parameters associated with complex 7 have been deposited at the Cambridge Crystallographic Data Center (CCDC code is 754970). The crystal data and structure refinement parameters for complex7are given in Table1.  16.jpg  17.jpg |
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