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X-ray crystal structure determination Single crystals suitable for X-ray diffraction were obtained from the slow evaporation of acetonitrile solutions at room temperature. For complex7, a single crystal of suitable size was mounted on a Bruker SMART CCD area-detector diffractometer with graphite monochromated Mo–Ka radiation (k=0.71073 A ˚ ) at 113(2) K. Corrections were made for Lorentz and Polarization factors as well as for absorption (numerical).  15.jpg |
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leilejiayou
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