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[资源] Distillation Design and Control Using AspenTM Simulation--Second Edition高清版

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Table of Contents
Preface       xi
1       Fundamentals of Vapor-Liquid Phase Equilibrium (VLE)       1
1.1       Vapor Pressure       1
1.2       Binary VLE Phase Diagrams       3
1.3       Physical Property Methods       7
1.4       Relative Volatility       7
1.5       Bubblepoint Calculations       9
1.6       Ternary Diagrams       10
1.7       VLE Nonideality       12
1.8       Residue Curves for Ternary Systems       18
1.9       Conclusion       26
2       Analysis of Distillation Columns       27
2.1       Design Degrees of Freedom       27
2.2       Binary McCabe-Thiele Method       28
2.3       Approximate Multicomponent Methods       38
2.4       Analysis of Ternary Systems Using DISTIL       41
2.5       Conclusion       44
3       Setting up a Steady-State Simulation       45
3.1       Configuring a New Simulation       45
3.2       Specifying Chemical Components and Physical Properties       53
3.3       Specifying Stream Properties       58
3.4       Specifying Equipment Parameters       60
3.5       Running the Simulation       64
3.6       Using "Design Spec/Vary" Function       66
3.7       Finding the Optimum Feed Tray and Minimum Conditions       80
3.8       Column Sizing       81
3.9       Conclusion       84
4       Distillation Economic Optimization       85
4.1       Heuristic Optimization       85
4.2       Economic Basis       87
4.3       Results       89
4.4       Operating Optimization       91
4.5       Conclusion       97
5       More Complex Distillation Systems       98
5.1       Methyl Acetate/Methanol/Water System       98
5.2       Ethanol Dehydration       112
5.3       Heat-Integrated Columns       122
5.4       Conclusion       129
6       Steady-State Calculations for Control Structure Selection       130
6.1       Summary of Methods       131
6.2       Binary Propane/Isobutane System       133
6.3       Ternary BTX System       137
6.4       Multicomponent Hydrocarbon System       141
6.5       Ternary Azeotropic System       145
6.6       Conclusion       150
7       Converting From Steady State to Dynamic Simulation       151
7.1       Equipment Sizing       151
7.2       Exporting to Aspen Dynamics       153
7.3       Opening the Dynamic Simulation in Aspen Dynamics       156
7.4       Installing Basic Controllers       158
7.5       Installing Temperature and Composition Controllers       166
7.6       Performance Evaluation       179
7.7       Comparison with Economic Optimum Design       184
7.8       Conclusion       187
8       Control of More Complex Columns       188
8.1       Methyl Acetate Column       188
8.2       Columns with Partial Condensers       190
8.3       Control of Heat-Integrated Distillation Columns       209
8.4       Control of Azeotropic Columns/Decanter System       222
8.5       Conclusion       231
9       Reactive Distillation       232
9.1       Introduction       232
9.2       Types of Reactive Distillation Systems       234
9.3       TAME Process Basics       238
9.4       TAME Reaction Kinetics and VLE       241
9.5       Plantwide Control Structure       246
9.6       Conclusion       250
10       Control of Sidestream Columns       251
10.1       Liquid Sidestream Column       252
10.2       Vapor Sidestream Column       257
10.3       Liquid Sidestream Column with Stripper       264
10.4       Vapor Sidestream Column with Rectifier       271
10.5       Sidestream Purge Column       281
10.6       Conclusion       290
11       Control of Petroleum Fractionators       291
11.1       Petroleum Fractions       292
11.2       Characterization of Crude Oil       296
11.3       Steady-State Design of PREFLASH Column       304
11.4       Control of PREFLASH Column       311
11.5       Steady-State Design of Pipestill       316
11.6       Control of Pipestill       333
11.7       Conclusion       342
Index       343