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| Proton nuclear magnetic resonance ( 1 H-NMR) spectra were measured on a Mercury-Plus 300 spectrometer (CDCl3 or DMSO-d6as solvent and tetramethylsilane (TMS) as the internal standard). Mass spectra (MS) were measured on a Thermo MAT95XP-HRMS spectrometer. Elemental analyses (EA) were performed with an Elementar Vario EL elemental analyzer. Fluorescence spectra were measured on a Shimadzu RF-5301pc spectrometer with a slit width of 1.5 nm for both excitation and emission. |
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2楼2014-11-10 16:19:32