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sunjing2008

银虫 (正式写手)

[求助] 微谱求助! 已有1人参与

氘代试剂为MeOD, C谱数据213.9,206.1,178.4,164.6,153.8,143.4,131.1,118.7,100.6,84.5,75.4,61.0,55.3,52.6,49.6,47.2,44.9,34.3,29.3,27.0,26.9,26.5,18.2,17.5。多谢!!!
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sydong

铁杆木虫 (著名写手)

【答案】应助回帖

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sunjing2008: 金币+20, ★★★★★最佳答案 2014-09-29 11:19:14
氘代甲醇,查不到,其它溶剂查到13个:查询结果:共查到13个化合物(查询结果仅供参考)
1 .     andibenin-B
    相似度:56%
Journal of the Chemical Society, Perkin Transactions 1          1979                   2118-2121
Studies on fungal metabolites. Part 1. The structures of andibenins-A and -C, and andilesins-A, -B, and -C, meroterpenoids from Aspergillus variecolor
Thomas J. Simpson
Structure      13C NMR   碳谱模拟图
2 .     compound 57
    相似度:54.1%
Magnetic Resonance in Chemistry          1989          27          1166-1175
13C NMR data for isopimarane and 8-epi-isopimarane diterpenoids
A. San Feliciano, M. Medarde, F. Tomé, B. Hebrero and E. Caballero
Structure      13C NMR   碳谱模拟图
3 .     glaucocalyxin B
    相似度:54.1%
Chinese Tladitional Patent Medicine          2009          31          763-765
Chemical constituents from Rabdosia japonica var.glaucocalyx
XIANG Zhao-bao, XU Yi-xinl, CHEN Hai-sheng, HUANG Min-zhul
Structure      13C NMR   碳谱模拟图
4 .     yesodine
C25H35NO4     相似度:52%
Heterocycles          1990          31          1081-1088
Studies on Aconitum Species. XIII. Two New Diterpenoid Alkaloids from Aconitum yesonese var. Macroyesoense (Nakai) Tamura. VI.
Koji Wada, Hideo Bando, and Norio Kawahara
Structure      13C NMR   碳谱模拟图
5 .     compound 8
    相似度:50%
Journal of Natural Products          2000          63          226-229
Grindelane Diterpenoids from Stevia subpubescens
Luisa U. Román, Jairo I. Cambrón, Rosa E. del Río, Juan D. Hernández, Carlos M. Cerda-García-Rojas, and Pedro Joseph-Nathan
Structure      13C NMR   碳谱模拟图
6 .     caesalpinilinn
C21H26O5     相似度:50%
Helvetica Chimica Acta          2009          92          121-123
Five New Cassane-Type Diterpenes from Caesalpinia crista
Zheng-Yi Yang, Yin-Hua Yin, Li-Hong Hu
Structure      13C NMR   碳谱模拟图
7 .     gyrosanol A
C20H32O     相似度:50%
Journal of Natural Products          2010          73          1184-1187
Antiviral and Anti-inflammatory Diterpenoids from the Soft Coral Sinularia gyrosa
Shi-Yie Cheng, Cheng-Ta Chuang, Shang-Kwei Wang, Zhi-Hong Wen, Shu-Fen Chiou, Chi-Hsin Hsu, Chang-Feng Dai and Chang-Yih Duh
Structure      13C NMR   碳谱模拟图
8 .     (-)-14-Methoxybutorphanol
C22H31NO2     相似度:50%
Bioorganic & Medicinal Chemistry          2011          19          2808-2816
Synthesis and binding affinity of novel mono- and bivalent morphinan ligands for к,μ and δ opioid receptors
Bin Zhang, Tangzhi Zhang, Anna W. Sromek, Thomas Scrimale, Jean M. Bidlack, John L. Neumeyer
Structure      13C NMR   碳谱模拟图
9 .     preaustinoid A3
C26H32O7     相似度:50%
Zeitschrift für Naturforschung B          2007          62b          1035-1044
Four Additional Meroterpenes Produced by Penicillium sp Found in Association with Melia azedarach. Possible Biosynthetic Intermediates to Austin
Taicia Pacheco Fill, Grace Kelli Pereira, Regina M. Geris dos Santos, and Edson Rodrigues-Fo
Structure      13C NMR   碳谱模拟图
10 .     phanginin N
C21H26O6     相似度:50%
Journal of China Pharmaceutical University          2012          43          209-210
A new cassane furanoditerpenoid from the seeds of Caesalpinia sappan
ZHANG Jing-yu, QU Wei, LIANG Jing-yu*
Structure      13C NMR   碳谱模拟图
11 .     cattienoid B
C22H28O3     相似度:50%
Fitoterapia          2013          91          125-127
Cattienoids A–C, three novel steroids from the mushroom Tomophagus cattienensis
Bui Thi Thu Hien, Le Thi Phuong Hoa, Le Xuan Tham, Dang Ngoc Quang
Structure      13C NMR   碳谱模拟图
12 .     Daphmacromine L
C22H29NO4     相似度:50%
Fitoterapia          2013          89          205-209
Daphmacromines K–O, alkaloids from Daphniphyllum macropodum
Ming-Ming Cao, Lei Wang, Yu Zhang, Hong-Ping He, Yu-Cheng Gu, Qiang Zhang, Yan Li, Chun-Mao Yuan, Shun-Lin Li, Ying-Tong Di, Xiao-Jiang Hao
Structure      13C NMR   碳谱模拟图
13 .     compound 37
C26H38O5     相似度:50%
Tetrahedron          2014          70          3030-3041
Efficient transformation of 7,14-dihydroxy-ent-kaurenes to novel ent-abietanes having cis-fused α-methylene γ-lactones under Mitsunobu reaction conditions and their cytotoxicities
Yutaka Aoyagi, Kei Ozawa, Tatsuya Kobayashi, Tomoyo Hasuda, Ming-Yu Gui, Yong-Ri Jin, Xu-Wen Li, Haruhiko Fukaya, Reiko Yano, Yukio Hitotsuyanagi, Koichi Takeya
Structure      13C NMR   碳谱模拟图
思路决定出路!
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