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[求助] 求单斜CuO的I/Ic(RIR)值已有1人参与

PDF#48-1548: QM=Star/Calculated; d=Other/Unknown; I=(Unknown)
Tenorite, syn
CuO
Radiation=CuKa1 Lambda=1.5406 Filter=
Calibration= d-Cutoff= I/Ic(RIR)=
Ref= Level-1 PDF

Monoclinic,  C2/c(15) Z=4 mp=
Cell=4.688x3.423x5.132<90x99.506x90> Pearson=
Density(c)=6.505 Density(m)= Mwt= Vol=
Ref= Ibid.

Strong Line: 2.52/X  2.32/X  2.53/4  1.87/3  2.31/2  1.51/2  1.41/2  1.38/1

d(A)    I(f) I(v)  h  k l  n^2  2-Theta Theta  1/(2d) 2pi/d
2.752 13.0 11.0  1  1 0       32.508  16.254  0.1817  2.2831
2.532 37.0 34.0  0  0 2       35.417  17.709  0.1974  2.4812
2.523  100.0 93.0  1  1  -1       35.543  17.772  0.1981  2.4897
2.324 99.0  100.0  1  1 1       38.708  19.354  0.2151  2.7033
2.313 21.0 21.0  2  0 0       38.902  19.451  0.2162  2.7163
1.961 3.0 4.0  1  1  -2       46.259  23.129  0.2550  3.2042
1.867 30.0 38.0  2  0  -2       48.716  24.358  0.2677  3.3642
1.778 1.0 1.0  1  1 2       51.343  25.671  0.2812  3.5337
1.711 7.0 10.0  0  2 0       53.485  26.743  0.2921  3.6705
1.621 1.0 1.0  0  2 1       56.741  28.371  0.3084  3.8760
1.582 10.0 15.0  2  0 2       58.264  29.132  0.3160  3.9710
1.506 20.0 31.0  1  1  -3       61.524  30.762  0.3320  4.1721
1.417 10.0 17.0  0  2 2       65.811  32.906  0.3526  4.4314
1.410 15.0 25.0  3  1  -1       66.220  33.110  0.3546  4.4557
1.405 1.0 2.0  3  1 0       66.447  33.224  0.3557  4.4693
1.379 6.0 10.0  1  1 3       67.903  33.951  0.3625  4.5556
1.375 14.0 24.0  2  2 0       68.123  34.061  0.3636  4.5686
1.361 1.0 2.0  2  2  -1       68.905  34.453  0.3672  4.6146
1.315 1.0 2.0  3  1  -2       71.681  35.841  0.3801  4.7762
1.304 5.0 9.0  3  1 1       72.371  36.186  0.3832  4.8159
1.295 1.0 2.0  2  2 1       72.942  36.471  0.3858  4.8487
1.265 6.0 11.0  0  0 4       74.976  37.488  0.3950  4.9643
1.261 5.0 9.0  2  2  -2       75.243  37.621  0.3962  4.9794
1.201 1.0 2.0  0  2 3       79.731  39.865  0.4161  5.2285
1.196 2.0 4.0  2  0  -4       80.155  40.077  0.4179  5.2517
1.195 1.0 2.0  1  1  -4       80.239  40.119  0.4183  5.2562
1.169 4.0 8.0  3  1  -3       82.359  41.180  0.4274  5.3707
1.161 2.0 4.0  2  2 2       83.063  41.531  0.4304  5.4083
1.156 4.0 8.0  3  1 2       83.566  41.783  0.4325  5.4351
1.123 1.0 2.0  4  0  -2       86.530  43.265  0.4449  5.5906
1.121 1.0 2.0  2  2  -3       86.772  43.386  0.4459  5.6031
1.109 1.0 2.0  1  1 4       87.965  43.983  0.4508  5.6646
1.108 1.0 2.0  1  3 0       88.051  44.026  0.4511  5.6690
1.091 3.0 6.0  1  3  -1       89.787  44.894  0.4581  5.7572
1.073 1.0 2.0  1  3 1       91.726  45.863  0.4659  5.8541
1.040 1.0 2.0  2  0 4       95.562  47.781  0.4807  6.0409
1.017 2.0 5.0  2  2 3       98.388  49.194  0.4913  6.1743
1.007 2.0 5.0  3  1 3       99.681  49.840  0.4961  6.2340
0.991 1.0 2.0  4  0 2    101.932  50.966  0.5042  6.3361
0.981 2.0 5.0  1  1  -5    103.353  51.677  0.5092  6.3994
0.980 2.0 5.0  2  2  -4    103.561  51.781  0.5100  6.4086
0.958 2.0 5.0  4  2 0    107.045  53.523  0.5219  6.5590
0.943 1.0 2.0  1  3  -3    109.515  54.757  0.5301  6.6620
0.939 3.0 7.0  4  2  -2    110.166  55.083  0.5323  6.6886
0.933 1.0 3.0  4  0  -4    111.187  55.593  0.5356  6.7299
0.921 2.0 5.0  1  1 5    113.485  56.742  0.5428  6.8210
0.918 2.0 5.0  4  2 1    114.056  57.028  0.5446  6.8432
0.909 1.0 3.0  1  3 3    115.739  57.870  0.5497  6.9077
0.904 1.0 3.0  5  1  -1    116.833  58.417  0.5530  6.9488
0.888 1.0 3.0  2  2 4    120.216  60.108  0.5628  7.0719
0.887 6.0 16.0  3  3 1    120.504  60.252  0.5636  7.0821

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1楼 2014-09-26 16:20:56

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

jiaran

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【答案】应助回帖

同一种物质的另一个卡片上有，I/Ic(RIR)=2.5。
无意间看到的啊，楼主可能不需要了吧。。

PDF#45-0937: QM=Star(+); d=Diffractometer; I=Diffractometer
Tenorite, syn
Cu O (Black)
Radiation=CuKa1 Lambda=1.540598 Filter=Graph
Calibration=Internal(Si) d-Cutoff=15.0 I/Ic(RIR)=2.5
Ref= Martin, K., McCarthy, G., North Dakota State Univ., Fargo, ND, USA.
ICDD Grant-in-Aid (1991)
Monoclinic - Powder Diffraction,  C2/c (15) Z=4 mp=
Cell=4.6853x3.4257x5.1303<99.549> Pearson=mC8 (Cu O)
Density(c)=6.506 Density(m)=6.450 Mwt=79.55 Vol=81.20 F(30)=89.7(.0070,48)
Ref= J. Solid State Chem., 89 184 (1990)

Strong Line: 2.53/X 2.32/9 2.31/3 1.87/2 1.51/2 1.41/1 1.38/1 1.58/1 2.75/1 1.42/1
NOTE:  Sample obtained from Fisher Scientific.
Sample annealed for 72 hours at 900 C.
Average relative standard deviation in intensity of the ten strongest reflections for three specimen mounts = 4.8% Validated by calculated pattern.
To replace 00-041-0254.
Deleted by 002 and -111 reflections are not split; WFM 10/95.
See ICSD 67850 (PDF 01-080-0076).

d(A)    I(f) I(v) h  k  l  n^2  2-Theta Theta  1/(2d) 2pi/d
2.753 8.0 7.0  -1  1  0       32.496  16.248  0.1816  2.2823
2.527  100.0  100.0  -1  1  1       35.495  17.747  0.1979  2.4864
2.527  100.0  100.0 0  0  2       35.495  17.747  0.1979  2.4864
2.323 91.0 99.0 1  1  1       38.730  19.365  0.2152  2.7048
2.310 28.0 31.0 2  0  0       38.957  19.479  0.2165  2.7200
1.961 2.0 3.0  -1  1  2       46.248  23.124  0.2549  3.2034
1.867 20.0 27.0  -2  0  2       48.725  24.363  0.2678  3.3649
1.776 1.0 1.0 1  1  2       51.379  25.690  0.2814  3.5360
1.712 6.0 9.0 0  2  0       53.451  26.726  0.2919  3.6684
1.580 9.0 14.0 2  0  2       58.335  29.168  0.3164  3.9754
1.505 15.0 25.0  -1  1  3       61.533  30.767  0.3320  4.1727
1.418 8.0 14.0 0  2  2       65.785  32.892  0.3525  4.4298
1.409 11.0 20.0  -3  1  1       66.248  33.124  0.3547  4.4574
1.378 9.0 16.0 1  1  3       67.943  33.972  0.3627  4.5580
1.375 11.0 20.0  -2  2  0       68.089  34.045  0.3634  4.5666
1.303 5.0 10.0 3  1  1       72.427  36.214  0.3835  4.8191
1.264 5.0 10.0 0  0  4       75.029  37.515  0.3953  4.9673
1.262 6.0 12.0  -2  2  2       75.225  37.612  0.3962  4.9784
1.196 2.0 4.0  -2  0  4       80.180  40.090  0.4180  5.2531
1.169 3.0 6.0  -3  1  3       82.375  41.188  0.4275  5.3716
1.161 2.0 4.0 2  2  2       83.103  41.551  0.4306  5.4105
1.155 2.0 4.0 4  0  0       83.649  41.825  0.4329  5.4395
1.123 1.0 2.0  -4  0  2       86.567  43.283  0.4450  5.5925
1.092 2.0 5.0  -1  3  1       89.721  44.861  0.4579  5.7538
1.074 1.0 2.0 1  3  1       91.649  45.824  0.4655  5.8503
1.039 1.0 2.0 2  0  4       95.672  47.836  0.4811  6.0462
1.017 1.0 2.0 0  2  4       98.406  49.203  0.4914  6.1751
1.006 2.0 5.0 3  1  3       99.814  49.907  0.4966  6.2401
0.981 2.0 5.0  -1  1  5    103.389  51.695  0.5094  6.4010
0.980 2.0 5.0  -2  2  4    103.523  51.761  0.5098  6.4068
0.957 1.0 3.0  -4  2  0    107.086  53.543  0.5221  6.5607
0.943 1.0 3.0  -1  3  3    109.419  54.710  0.5298  6.6580
0.939 2.0 5.0  -4  2  2    110.164  55.082  0.5323  6.6885
0.933 1.0 3.0  -4  0  4    111.208  55.604  0.5356  6.7308
0.920 2.0 5.0 1  1  5    113.571  56.785  0.5431  6.8244
0.918 2.0 6.0  -3  3  1    113.972  56.986  0.5443  6.8400
0.909 1.0 3.0 1  3  3    115.678  57.839  0.5495  6.9054
0.903 1.0 3.0  -5  1  1    116.939  58.470  0.5533  6.9527

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