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In the case of AS (A), the sintering shrinkage took place at 1300-1400℃, and then the expansion occurred due to the generation of CA6. And in the case of AM(D), the expansion caused by formation of spinel occurred at the temperature between 1200 and 1450℃, which is consistent with the XRD results demonstrating that the spinel peak is presented from 1200℃ as mentioned above, and then it began to show the sintering shrinkage.And at the temperature higher than 1500℃, the expansion caused by CA6 generation occurred.In the case of ASM (B and C), the sintering shrinkage caused by the formation in liquid phase seemed to have bigger effect on the expansions than the spinel formation at the temperature between 1200 and1400℃. It was judged that the thermal linear expansion was associated with in-situ spinel formation at 1400℃, but it was associated with CA6 formation at the temperature higher than 1500℃. |
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RacherSasuke
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2楼2014-09-22 12:39:50
3楼2014-09-22 20:37:42
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真强必胜: 金币+2, 谢谢 2014-09-23 12:46:37
英语留级生: 金币+12, 翻译EPI+1, ★★★★★最佳答案, 非常非常感谢 2014-09-23 14:41:01
真强必胜: 金币+2, 谢谢 2014-09-23 12:46:37
英语留级生: 金币+12, 翻译EPI+1, ★★★★★最佳答案, 非常非常感谢 2014-09-23 14:41:01
| 就AS（A）而言，当温度为1300－1400℃时发生烧结收缩，然后由于产生CA6而发生膨胀。而在AM（D），当温度在1200－1450℃时因形成尖晶石而发生膨胀，这与用X射线衍射得到的结果是一致的，表明在如上所述的从1200℃出现尖晶石峰，然后开始表现为烧结收缩。在温度超过1500℃时，因产生CA6而发生膨胀。就ASM（B和C）而言，液相形成而引起的烧结收缩作用比温度在1200－1400℃之间所形成尖晶石而引起的膨胀作用更大。据判断，在1400℃时线性热膨胀与原位尖晶石的形成相关，但在温度超过1500℃时则与CA6的形成相关。 |
4楼2014-09-22 21:25:58