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| 13C NMR (75 MHz, MeOD) δ16.79,16.83,19.09,30.73,62.02,62.59,65.05,65.38,65.71,67.10,67.14,68.17,71.00,71.50,72.96,75.01,75.46,75.57,76.83,77.18,77.44,77.85,77.90,78.14,78.82, 79.04,79.53,102.11,109.15,109.99,112.13,112.17,146.54,146.62,146.73,147.57. 谢谢！ |
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沫沫、Alone: 金币+20, ★★★很有帮助 2014-09-12 20:36:39
感谢参与，应助指数 +1
沫沫、Alone: 金币+20, ★★★很有帮助 2014-09-12 20:36:39
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1 . polygalasaponin XIX C64H102O32 相似度:63.8% Chemical & Pharmaceutical Bulletin 1995 43 966-970 Studies on the Constituents of Polygala japonica HOUTT. II. Structures of Polygalasaponins XI-XIX Dongming ZHANG,Toshio MIYASE,Masanori KUROYANAGI,Kaoru UMEHARA and Akira UENO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . compound 3 相似度:61.1% Journal of Natural Products 2007 70 1680-1682 Saponins from the Roots of Nylandtia spinosa Cheikh Diome,Anne-Claire Mitaine-Offer,Tomofumi Miyamoto, Clément Delaude, Jean-François Mirjolet, Olivier Duchamp, and Marie-Aleth Lacaille-Dubois Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . cycloviracin B1 C83H152O33 相似度:56.7% The Journal of Antibiotics 1992 45 1472-1480 NEW ANTIVIRAL ANTIBIOTICS, CYCLOVIRACINS B1 AND B2 II. STRUCTURE DETERMINATION MITSUAKI TSUNAKAWA, CHIKAKO KOTAKE, TETSURO YAMASAKI, TOSHIO MORIYAMA, MASATAKA KONISHI, TOSHIKAZU OKI Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . Methyl Quamoside A C37H64O27 相似度:56.7% Chemical & Pharmaceutical Bulletin 2013 61 952-961 Three Acylated Glycosidic Acid Methyl Esters and Two Acylated Methyl Glycosides Generated from the Convolvulin Fraction of Seeds of Quamoclit pennata by Treatment with Indium(III) Chloride in Methanol Kousuke Akiyama, Tomoko Mineno, Masafumi Okawa, Junei Kinjo, Hiroyuki Miyashita, Hitoshi Yoshimitsu, Toshihiro Nohara, Masateru Ono Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . compound 1 C69H110O37 相似度:56.4% Journal of Natural Products 2007 70 1680-1682 Saponins from the Roots of Nylandtia spinosa Cheikh Diome,Anne-Claire Mitaine-Offer,Tomofumi Miyamoto, Clément Delaude, Jean-François Mirjolet, Olivier Duchamp, and Marie-Aleth Lacaille-Dubois Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . stansin 5 C50H86O21 相似度:55.5% Journal of Natural Products 2004 67 1552-1556 Isolation and Characterization of Five New Tetrasaccharide Glycosides from the Roots of Ipomoea stans and Their Cytotoxic Activity Ismael Len, Ral G. Enrquez, Dino Gnecco, Mara L. Villarreal,Daniel Alonso Corts, William F. Reynolds, and Margaret Yu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . tyrianthin 6 C49H84O21 相似度:55.5% Journal of Natural Products 2007 70 557-562 Resin Glycosides from the Roots of Ipomoea tyrianthina and Their Biological Activity Gumersindo Mirón-López,Maribel Herrera-Ruiz, Samuel Estrada-Soto, Francisco Aguirre-Crespo,Lorena Vázquez-Navarrete,and Ismael León-Rivera Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . tragopogonsaponin R methyl ester C64H96O27 相似度:55.5% Chemical & Pharmaceutical Bulletin 1991 39 388-396 Novel Acylated Saponins from Tragopogon porrifolius L. Isolation and the Structures of Tragopogonsaponins A-R Tsutomu WARASHINA,Toshio MIYASE and Akira UENO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . operculin V C70H124O25 相似度:55.5% Chemical & Pharmaceutical Bulletin 1990 38 2986-2991 Resin Glycosides. IX. : Operculins I, II, V, VII and VIII, New Ether-Soluble Resin Glycosides of Rhizoma Jalapae Braziliensis(the Roots of Ipomoea operculata) Masateru ONO,Masatoshi NISHI,Toshio KAWASAKI and Kazumoto MIYAHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . serratumoside A C36H48O19 相似度:55.5% Chinese Chemical Letters 2000 11 323-326 A New Phenylpropanoid Glycoside: Serratumoside A from Clerodendrum serratum Hui YANG, Ai Jun HOU, Shuang Xi MEI, Li Yan PENG, Han Dong SUN Structure 13C NMR Structure & 13C NMR 碳谱模拟图 11 . 3β-O-β-D-glucopyranosyl-(1→3)-α-L-rhamopyranosyl-(1→4)-α-L-rhamopyranosyl-(1→6)-β-D-galactopyranosyl-(1→4)-β-D-glucopyranosylolean-12-en-28-oic acid-β-D-glucopyranosyl ester(sugar moiety) C66H108O31 相似度:55.5% Journal of Natural Products 1997 60 1070-1074 Triterpenoid Saponins from Trevesia sundaica Nunziatina De Tommasi, Cosimo Pizza, Aurora Bellino, and Pietro Venturella Structure 13C NMR Structure & 13C NMR 碳谱模拟图 12 . compound 16 C35H61O30N 相似度:55.5% Tetrahedron Letters 2003 44 1839-1842 An efficient synthesis of a hexasaccharide—the repeating unit of the exopolysaccharide from Cryptococcus neoformans serovar A Jianjun Zhang, Fanzuo Kong Structure 13C NMR Structure & 13C NMR 碳谱模拟图 13 . fattiviracin FV-4 C68H124O28 相似度:55.5% The Journal of Antibiotics 2000 53 1420-1423 Structures of Fattiviracin Family, Antiviral Antibiotics EL-SAYED E. HABIB,KAZUMI YOKOMIZO,KEIKO MURATA and MASARU UYEDA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 14 . fattiviracin FV-10 C74H136O28 相似度:55.5% The Journal of Antibiotics 2000 53 1420-1423 Structures of Fattiviracin Family, Antiviral Antibiotics EL-SAYED E. HABIB,KAZUMI YOKOMIZO,KEIKO MURATA and MASARU UYEDA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 15 . propargyl β-D-glucopyranosyl-(1→4)-α-L-rhamnopyranosyl-(1→4)-β-D-glucopyranosyl-(1→4)-2-O-(α-L-rhamnopyranosyl)-β-D-glucopyranoside C33H54O24 相似度:55.5% European Journal of Organic Chemistry 2008 2008 5770-5777 Synthesis of Oligosaccharides Related to a Biodynamic Saponin from Calamus Insignis as Their Propargyl Glycosides Somnath Dasgupta and Balaram Mukhopadhyay Structure 13C NMR Structure & 13C NMR 碳谱模拟图 16 . Mitrarioside B C32H54O13 相似度:55.5% European Journal of Organic Chemistry 1992 1992 665-668 Mitrariosides, Five Bitter Labdane Glycosides from Mitraria coccinea (Gesneriaceae) Luz Clarena Cárdenas, Jaime Rodríguez, Ricardo Riguera and Maria Cristina Chamy Structure 13C NMR Structure & 13C NMR 碳谱模拟图 17 . atractyloside F 相似度:54.0% Chemical & Pharmaceutical Bulletin 1989 37 2995-3000 Studies on the Constiutents of Atractylodes lancea Shoji YAHARA,Tomoko HIGASHI,Kazue IWAKI,Toshihiro NOHARA,Nobuhiro MARUBAYASHI,Ikuhiko UEDA,Hiroshi KOHDA,Katsumi GOTO,Hiromasa IZUMI,Mariko NUNO,Shigeki KATSUKI,Susumu ISODA and Motoyoshi SATAKE Structure 13C NMR Structure & 13C NMR 碳谱模拟图 18 . cycloviracin B2 C83H150O33 相似度:54.0% The Journal of Antibiotics 1992 45 1472-1480 NEW ANTIVIRAL ANTIBIOTICS, CYCLOVIRACINS B1 AND B2 II. STRUCTURE DETERMINATION MITSUAKI TSUNAKAWA, CHIKAKO KOTAKE, TETSURO YAMASAKI, TOSHIO MORIYAMA, MASATAKA KONISHI, TOSHIKAZU OKI Structure 13C NMR Structure & 13C NMR 碳谱模拟图 19 . xeranthin C39H49NO23 相似度:53.8% Phytochemistry 1990 29 1903-1911 Structure elucidation of an acylated cyanogenic triglycoside,and further cyanogenic constituents from Xeranthemum cylindraceum Philipp Schwind,Victor Wray,Adolf Nahrstedt Structure 13C NMR Structure & 13C NMR 碳谱模拟图 20 . quamoclinic acids D C50H88O30 相似度:53.6% Chemical & Pharmaceutical Bulletin 2010 58 666-672 Components of Ether-Insoluble Resin Glycoside (Convolvulin) from Seeds of Quamoclit pennata Masateru Ono, Yoko Takagi-Taki, Fumiko Honda-Yamada, Naoki Noda and Kazumoto Miyahara Structure 13C NMR Structure & 13C NMR 碳谱模拟图 21 . fucatoside C C33H42O19 相似度:52.7% Journal of Natural Products 2009 72 1424-1428 Phenylethanoid Glycosides from Lantana fucata with in Vitro Anti-inflammatory Activity Lisieux de Santana Juliao,Anna Lisa Piccinelli, Stefania Marzocco, Suzana Guimaraes Leitao,Cinzia Lotti,Giuseppina Autore,and Luca Rastrelli Structure 13C NMR Structure & 13C NMR 碳谱模拟图 22 . persicaoside B C35H48O14 相似度:52.7% Phytochemistry 2008 69 473-478 Polar secondary metabolites of Ferula persica roots Mehrdad Iranshahi, Mehdi Mojarab, Hamid Sadeghian,Mohammad Yahya Hanafi-Bojd, Bernd Schneider Structure 13C NMR Structure & 13C NMR 碳谱模拟图 23 . stansin 4 C49H84O21 相似度:52.7% Journal of Natural Products 2004 67 1552-1556 Isolation and Characterization of Five New Tetrasaccharide Glycosides from the Roots of Ipomoea stans and Their Cytotoxic Activity Ismael Len, Ral G. Enrquez, Dino Gnecco, Mara L. Villarreal,Daniel Alonso Corts, William F. Reynolds, and Margaret Yu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 24 . transsylvanoside J C59H96O27 相似度:52.7% Planta Medica 1997 63 51-54 Hederagenin Glycosides from the Flowers of Cephalaria transsylvanica Suheyla Krmizigul and Malcolm E. Rose Structure 13C NMR Structure & 13C NMR 碳谱模拟图 25 . tragopogonsaponin P methyl ester C63H94O26 相似度:52.7% Chemical & Pharmaceutical Bulletin 1991 39 388-396 Novel Acylated Saponins from Tragopogon porrifolius L. Isolation and the Structures of Tragopogonsaponins A-R Tsutomu WARASHINA,Toshio MIYASE and Akira UENO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 26 . pharbitic acid C C26H47O13 相似度:52.7% Chemical & Pharmaceutical Bulletin 1990 38 1892-1897 Resin Glycosides. VII. : Reinvestigation of the Component Organic and Glycosidic Acids of Pharbitin, the Crude Ether-Insoluble Resin Glycoside ("Convolvulin"  of Pharbitidis Semen (Seeds of Pharbitis nil)Masateru ONO,Naoki NODA,Toshio KAWASAKI and Kazumoto MIYAHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 27 . R-1b C60H96O27 相似度:52.7% Chemical & Pharmaceutical Bulletin 1985 33 4701-4706 Triterpenoid Glycosides from the Roots of Tetrapanax papyriferum K. KOCH. III. Structures of Four New Saponins SEIICHI TAKABE,TADAHIRO TAKEDA,YINGJIE CHEN and YUKIO OGIHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 28 . 3-O-β-gentiobiosyl-platycodigenin 相似度:52.7% Chemical & Pharmaceutical Bulletin 1978 26 671-673 Structures of Prosapogenins from Roots of Platycodon grandiflorum determined by Carbon-13 and Hydrogen-1 Nuclear Magnetic Resonance Spectroscopy HIROSHI ISHII,KAZUO TORI,TAKEHIKO TOZYO and YOHKO YOSHIMURA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
2楼2014-09-12 19:15:29
