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2011GG

铜虫 (小有名气)

应助: 1 (幼儿园)
金币: 256.4
散金: 85
红花: 2
帖子: 117
在线: 125.9小时
虫号: 2020315
注册: 2012-09-22
专业: 绿色有机化学

[求助] 亲爱的虫友们跪求解谱(碳谱氢谱质谱）急已有2人参与

Q+除一个强度为1.09e7的离子峰834.9，强度为5e5的517.1，,561.3，818.9,832.5的峰外，基本没什么峰。
Q-是441.4(2.8 e7 )
溶剂为甲醇求各路大侠帮忙解谱呀小女无限感激。

Q-.jpg

Q+.jpg

氢谱.jpg

碳谱.jpg

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1楼2014-05-20 23:30:30

已阅回复此楼关注TA 给TA发消息送TA红花 TA的回帖

2011GG

铜虫 (小有名气)

应助: 1 (幼儿园)
金币: 256.4
散金: 85
红花: 2
帖子: 117
在线: 125.9小时
虫号: 2020315
注册: 2012-09-22
专业: 绿色有机化学

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11楼: Originally posted by tonypengt at 2014-05-24 14:37:51
求一下碳谱的微谱看看！...

1 .    8-O-acetylharpagide
相似度:76.4%
Korean Journal of Pharmacognosy       1998       29(2)       75-78
Studies on the Constituents of the Herbs of Ajuga multiflora (I)
Yu, Young-Jun; Do, Jae-Chul; Jung, Keun-Young; Kwon, Soon-Youl; Son, Kun-Ho
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
2 .    8-O-acetylharpagide
相似度:76.4%
Chinese Traditional and Herbal Drugs       2012       43       869-872
Chemical constituents of Lagochilus ilicifolius
QIAN Jing-shi; ZHANG Bin-feng; WANG Wei; LIU Qing; WANG Chang-hong; JIAO Ying; CHOU Gui-xin; XU Hong; WANG Zheng-tao
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
3 .    6-epi-8-O-acetylharpagide
C17H26O11    相似度:70.5%
Phytochemistry       2000       54       807-809
Iridoids from Caryopteris x clandonensis
Sébastien Hannedouche, Edouard Stanislas, Claude Moulis, Isabelle Fourasté
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
4 .    8-O-acetylharpagide
相似度:70.5%
Journal of Natural Products       1993       Vol 56       830
Neocleordane Diterpenoids and Their Artifacts from Teucrium olivarianum
Mohammed A. Al-Yahya, Ilias Muhammad, Humayun H. Mirza, Farouk S. El-Feraly, Andrew T. McPhail
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
5 .    ajureptaside B
C17H28O11    相似度:70.5%
Chemical & Pharmaceutical Bulletin       2011       59(8)       1065-1068
Four New Iridoid Glucosides from Ajuga reptans
Masateru ONO, Chisato FURUSAWA,Takumi OZONO, Keisuke ODA, Shin YASUDA,Masafumi OKAWA, Junei KINJO, Tsuyoshi IKEDA, Hiroyuki MIYASHITA,Hitoshi YOSHIMITSU, and Toshihiro NOHARA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
6 .    8-O-acetylharpagide
相似度:70.5%
Phytochemistry       1989       28       1601-1604
Iridoid glycosides of Aureolaria flava and their sequestration by Euphydryas phaeton butterflies
Gil Belofsky,M.Deane Bowers,Sarah Janzen,Frank Stermitz
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
7 .    caryocanoside A
C17H26O10    相似度:70.5%
Journal of Natural Medicines       2014       68       231-235
Constituents of Caryopteris incana and their antibacterial activity
Kazuko Yoshikawa, Akinori Harada, Kanako Iseki, Toshihiro Hashimoto
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
8 .    6-epi-8-O-Acetylharpagide
C17H26O11    相似度:70.5%
Chemical & Pharmaceutical Bulletin       2007       55       159-222
Naturally Occurring Iridoids. A Review, Part 1
Biswanath DINDA, Sudhan DEBNATH and Yoshihiro HARIGAYA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
9 .    Caryocanoside A
C17H26O10    相似度:70.5%
Journal of Natural Medicines       2014       68       231-235
Constituents of Caryopteris incana and their antibacterial activity
Kazuko Yoshikawa, Akinori Harada, Kanako Iseki, Toshihiro Hashimoto
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
10 .    harpagoside
相似度:68.1%
Phytochemistry       2006       67       1372-1377
Iridoid glycosides from Harpagophytum procumbens D.C. (devil’s claw)
Jin Qi, Ji-Jun Chen, Zhi-Hong Cheng, Jia-Hong Zhou,Bo-Yang Yu, Samuel X. Qiu
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
11 .    8-O-acetylharpagide
相似度:64.7%
Journal of Natural Products       2002       65       789-793
The Antiplasmodial Activity of Isolates from Ajuga remota
Kimani A. M. Kuria, Hezekiah Chepkwony, Cindy Govaerts, Eugene Roets, Roger Busson, Peter de Witte, Istvan Zupko, Georges Hoornaert, Ludo Quirynen, Louis Maes, Leen Janssens, Jos Hoogmartens, and Gert Laekeman
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
12 .    clandonoside hydrate
C15H24O11    相似度:64.7%
Phytochemistry       1999       51       767-769
Iridoid keto-glycosides from Caryopteris × Clandonensis
Sebastien Hannedouche, Ingrid Jacquemond-Collet, Nicolas Fabre, Edouard Stanislas, Claude Moulis
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
13 .    8-acetyl harpagide
相似度:64.7%
Natural Product Research and Development       2000       12(3)       45-47
CHEMICAL STUDIES OF AJUGA LUPULINA VAR.MAJOR
Li Bo; Zheng Chuanchi; Lin Zhongwen; Sun Handong
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
14 .    Barlerin
相似度:63.1%
Phytochemistry       1994       36       967-970
Iridoid glycosides from Phlomis younghusbandii roots
Ryoji Kasai, Masako Katagiri, Kazuhiro Ohtani, Kazuo Yamasaki, Yang Chong-Ren, Osamu Tanaka
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
15 .    ajureptaside A
C18H30O13    相似度:61.1%
Chemical & Pharmaceutical Bulletin       2011       59(8)       1065-1068
Four New Iridoid Glucosides from Ajuga reptans
Masateru ONO, Chisato FURUSAWA,Takumi OZONO, Keisuke ODA, Shin YASUDA,Masafumi OKAWA, Junei KINJO, Tsuyoshi IKEDA, Hiroyuki MIYASHITA,Hitoshi YOSHIMITSU, and Toshihiro NOHARA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
16 .    3'-O-β-glucopyranosyl-stilbericoside
C20H30O15    相似度:60%
Phytochemistry       2002       60       769-771
Iridoid glucosides from Thunbergia laurifolia
Tripetch Kanchanapoom, Ryoji Kasai, Kazuo Yamasaki
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
17 .    3'-O-β-Glucopyranosylstilbericoside
C20H30O15    相似度:60%
Chemical & Pharmaceutical Bulletin       2007       55       159-222
Naturally Occurring Iridoids. A Review, Part 1
Biswanath DINDA, Sudhan DEBNATH and Yoshihiro HARIGAYA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
18 .    harpagoside
相似度:59.0%
Phytochemistry       1989       28       2701-2704
Iridoids from Scrophularia ningpoensis
Tetsuya Kajimoto,Mitsuharu Hidaka,Kayoko Shoyama,Toshihiro Nohara
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
19 .    8-acetylharpagide
相似度:58.8%
Phytochemistry       2006       67       830-837
Flavonol and iridoid glycosides of Ajuga remota aerial parts
Lawrence O. Arot Manguro, Samuel Otieno Wagai, Peter Lemmen
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
20 .    5,9-epi-7,8-didehydropenstemoside
C17H24O11    相似度:58.8%
Journal of Natural Products       2004       67       1584-1587
Iridoid Glycosides from Eremostachys glabra
Abbas Delazar, Maureen Byres, Simon Gibbons, Yashodharan Kumarasamy,Masoud Modarresi, Lutfun Nahar, Mohammad Shoeb, and Satyajit D. Sarker
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
21 .    lamalbid
相似度:58.8%
Chemical & Pharmaceutical Bulletin       1986       34       876-880
Iridoid Glucosides from Lamium amplexicaule
SHIGERU KOBAYASHI,AKIRA MIMA,MASARU KIHARA and YASUHIRO IMAKURA
Structure    13C NMR Structure & 13C NMR    碳谱模拟图
22 .    6-Keto-8-acetylharpagide
C17H24O11    相似度:58.8%
Journal of Asian Natural Products Research       2007       9       617-629
Further flavonol and iridoid glycosides from Ajuga remota aerial parts
LAWRENCE ONYANGO AROT MANGURO, JOSEPH ACHOLA OGUR, DENNIS MAGIO OKORA, SAMUEL OTIENO WAGAI and PETER LEMMEN
Structure    13C NMR Structure & 13C NMR    碳谱模拟图