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[求助]
亲爱的虫友们 跪求解谱(碳谱 氢谱 质谱） 急 已有2人参与
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Q+除一个强度为1.09e7的离子峰834.9，强度为5e5的517.1，,561.3，818.9,832.5的峰外，基本没什么峰。 Q-是441.4(2.8 e7 ) 溶剂为甲醇 求各路大侠帮忙解谱呀 小女无限感激。  Q-.jpg  Q+.jpg  氢谱.jpg  碳谱.jpg |
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1 . 8-O-acetylharpagide 相似度:76.4% Korean Journal of Pharmacognosy 1998 29(2) 75-78 Studies on the Constituents of the Herbs of Ajuga multiflora (I) Yu, Young-Jun; Do, Jae-Chul; Jung, Keun-Young; Kwon, Soon-Youl; Son, Kun-Ho Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . 8-O-acetylharpagide 相似度:76.4% Chinese Traditional and Herbal Drugs 2012 43 869-872 Chemical constituents of Lagochilus ilicifolius QIAN Jing-shi; ZHANG Bin-feng; WANG Wei; LIU Qing; WANG Chang-hong; JIAO Ying; CHOU Gui-xin; XU Hong; WANG Zheng-tao Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . 6-epi-8-O-acetylharpagide C17H26O11 相似度:70.5% Phytochemistry 2000 54 807-809 Iridoids from Caryopteris x clandonensis Sébastien Hannedouche, Edouard Stanislas, Claude Moulis, Isabelle Fourasté Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . 8-O-acetylharpagide 相似度:70.5% Journal of Natural Products 1993 Vol 56 830 Neocleordane Diterpenoids and Their Artifacts from Teucrium olivarianum Mohammed A. Al-Yahya, Ilias Muhammad, Humayun H. Mirza, Farouk S. El-Feraly, Andrew T. McPhail Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . ajureptaside B C17H28O11 相似度:70.5% Chemical & Pharmaceutical Bulletin 2011 59(8) 1065-1068 Four New Iridoid Glucosides from Ajuga reptans Masateru ONO, Chisato FURUSAWA,Takumi OZONO, Keisuke ODA, Shin YASUDA,Masafumi OKAWA, Junei KINJO, Tsuyoshi IKEDA, Hiroyuki MIYASHITA,Hitoshi YOSHIMITSU, and Toshihiro NOHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . 8-O-acetylharpagide 相似度:70.5% Phytochemistry 1989 28 1601-1604 Iridoid glycosides of Aureolaria flava and their sequestration by Euphydryas phaeton butterflies Gil Belofsky,M.Deane Bowers,Sarah Janzen,Frank Stermitz Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . caryocanoside A C17H26O10 相似度:70.5% Journal of Natural Medicines 2014 68 231-235 Constituents of Caryopteris incana and their antibacterial activity Kazuko Yoshikawa, Akinori Harada, Kanako Iseki, Toshihiro Hashimoto Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . 6-epi-8-O-Acetylharpagide C17H26O11 相似度:70.5% Chemical & Pharmaceutical Bulletin 2007 55 159-222 Naturally Occurring Iridoids. A Review, Part 1 Biswanath DINDA, Sudhan DEBNATH and Yoshihiro HARIGAYA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . Caryocanoside A C17H26O10 相似度:70.5% Journal of Natural Medicines 2014 68 231-235 Constituents of Caryopteris incana and their antibacterial activity Kazuko Yoshikawa, Akinori Harada, Kanako Iseki, Toshihiro Hashimoto Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . harpagoside 相似度:68.1% Phytochemistry 2006 67 1372-1377 Iridoid glycosides from Harpagophytum procumbens D.C. (devil’s claw) Jin Qi, Ji-Jun Chen, Zhi-Hong Cheng, Jia-Hong Zhou,Bo-Yang Yu, Samuel X. Qiu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 11 . 8-O-acetylharpagide 相似度:64.7% Journal of Natural Products 2002 65 789-793 The Antiplasmodial Activity of Isolates from Ajuga remota Kimani A. M. Kuria, Hezekiah Chepkwony, Cindy Govaerts, Eugene Roets, Roger Busson, Peter de Witte, Istvan Zupko, Georges Hoornaert, Ludo Quirynen, Louis Maes, Leen Janssens, Jos Hoogmartens, and Gert Laekeman Structure 13C NMR Structure & 13C NMR 碳谱模拟图 12 . clandonoside hydrate C15H24O11 相似度:64.7% Phytochemistry 1999 51 767-769 Iridoid keto-glycosides from Caryopteris × Clandonensis Sebastien Hannedouche, Ingrid Jacquemond-Collet, Nicolas Fabre, Edouard Stanislas, Claude Moulis Structure 13C NMR Structure & 13C NMR 碳谱模拟图 13 . 8-acetyl harpagide 相似度:64.7% Natural Product Research and Development 2000 12(3) 45-47 CHEMICAL STUDIES OF AJUGA LUPULINA VAR.MAJOR Li Bo; Zheng Chuanchi; Lin Zhongwen; Sun Handong Structure 13C NMR Structure & 13C NMR 碳谱模拟图 14 . Barlerin 相似度:63.1% Phytochemistry 1994 36 967-970 Iridoid glycosides from Phlomis younghusbandii roots Ryoji Kasai, Masako Katagiri, Kazuhiro Ohtani, Kazuo Yamasaki, Yang Chong-Ren, Osamu Tanaka Structure 13C NMR Structure & 13C NMR 碳谱模拟图 15 . ajureptaside A C18H30O13 相似度:61.1% Chemical & Pharmaceutical Bulletin 2011 59(8) 1065-1068 Four New Iridoid Glucosides from Ajuga reptans Masateru ONO, Chisato FURUSAWA,Takumi OZONO, Keisuke ODA, Shin YASUDA,Masafumi OKAWA, Junei KINJO, Tsuyoshi IKEDA, Hiroyuki MIYASHITA,Hitoshi YOSHIMITSU, and Toshihiro NOHARA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 16 . 3'-O-β-glucopyranosyl-stilbericoside C20H30O15 相似度:60% Phytochemistry 2002 60 769-771 Iridoid glucosides from Thunbergia laurifolia Tripetch Kanchanapoom, Ryoji Kasai, Kazuo Yamasaki Structure 13C NMR Structure & 13C NMR 碳谱模拟图 17 . 3'-O-β-Glucopyranosylstilbericoside C20H30O15 相似度:60% Chemical & Pharmaceutical Bulletin 2007 55 159-222 Naturally Occurring Iridoids. A Review, Part 1 Biswanath DINDA, Sudhan DEBNATH and Yoshihiro HARIGAYA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 18 . harpagoside 相似度:59.0% Phytochemistry 1989 28 2701-2704 Iridoids from Scrophularia ningpoensis Tetsuya Kajimoto,Mitsuharu Hidaka,Kayoko Shoyama,Toshihiro Nohara Structure 13C NMR Structure & 13C NMR 碳谱模拟图 19 . 8-acetylharpagide 相似度:58.8% Phytochemistry 2006 67 830-837 Flavonol and iridoid glycosides of Ajuga remota aerial parts Lawrence O. Arot Manguro, Samuel Otieno Wagai, Peter Lemmen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 20 . 5,9-epi-7,8-didehydropenstemoside C17H24O11 相似度:58.8% Journal of Natural Products 2004 67 1584-1587 Iridoid Glycosides from Eremostachys glabra Abbas Delazar, Maureen Byres, Simon Gibbons, Yashodharan Kumarasamy,Masoud Modarresi, Lutfun Nahar, Mohammad Shoeb, and Satyajit D. Sarker Structure 13C NMR Structure & 13C NMR 碳谱模拟图 21 . lamalbid 相似度:58.8% Chemical & Pharmaceutical Bulletin 1986 34 876-880 Iridoid Glucosides from Lamium amplexicaule SHIGERU KOBAYASHI,AKIRA MIMA,MASARU KIHARA and YASUHIRO IMAKURA Structure 13C NMR Structure & 13C NMR 碳谱模拟图 22 . 6-Keto-8-acetylharpagide C17H24O11 相似度:58.8% Journal of Asian Natural Products Research 2007 9 617-629 Further flavonol and iridoid glycosides from Ajuga remota aerial parts LAWRENCE ONYANGO AROT MANGURO, JOSEPH ACHOLA OGUR, DENNIS MAGIO OKORA, SAMUEL OTIENO WAGAI and PETER LEMMEN Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
19楼2014-05-25 19:35:34
lazierboy
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2楼2014-05-21 01:22:18
3楼2014-05-21 08:21:22
lazierboy
专家顾问 (正式写手)
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专家经验: +97 - 应助: 99 (初中生)
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4楼2014-05-21 14:54:39
