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[求助] 微谱求助 已有1人参与

最近分的一化合物   由于解谱技术着实太差  不知化合物类型  望好心人给微谱一下  谢谢
163.3, 153.1, 148.9, 146.1, 144.3, 141.1, 140.4, 132.3, 131.0, 128.4, 21.7, 21.1
这是13C-NMR谱数据  溶剂为氘代吡啶
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笑多会怀孕

铁杆木虫 (著名写手)

【答案】应助回帖

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感谢参与,应助指数 +1
辣笔v小新: 金币+1, 鼓励应助交流 2014-04-01 22:59:02
京羚: 金币+5, 有帮助 2014-04-02 15:46:17
.     7,8-Dimethylalloxazine
    相似度:100%
Archives of Pharmacal Research          2004          27          604-609
A new indolinepeptide fromPaecilomyces sp. J300
Hak Cheol Kwon, Kyung Ran Kim, Sang Deuk Zee, Sae Yun Cho and Kang Ro Lee
Structure      13C NMR   碳谱模拟图
2 .     2-(Pyridin-3-yl)-2,3,4,5,6,7-hexahydro-1,2-benzisothiazol-3-one 1,1-dioxide perchlorate
C12H13O7SN2Cl     相似度:66.6%
Zeitschrift für Naturforschung B          2009          64          669-675
Sultam and Sultim Structures, Part 5. Weak Hydrogen Bonds in Molecular Networks of 2-Hetaryl-3-oxosultams in Comparison with 2-Aryl-3-oxosultams
A. Eilfeld, J. Hunger, J. Sieler, and B. Schulze
Structure      13C NMR   碳谱模拟图
3 .     1-[2-(2,4-dimethylphenyl)-2-oxoethyl]pyridinium bromide
C15H16BrNO     相似度:66.6%
Tetrahedron          2013          69          5016-5021
Effect of solvent nature on the regioselectivity of the reactions of pyridinium ylides with E-1,2-di(alkylsulfonyl)-1,2-dichloroethene. From the reaction of 1,3-dipolar cycloaddition to the reaction of nucleophilic addition–elimination (AdN–E1,5)
Natalia E. Dontsova, Vladimir N. Nesterov, Anatoliy M. Shestopalov
Structure      13C NMR   碳谱模拟图
4 .     2,5-dimethyl-p-(4'-trimethylsilylphenyl)phenylboronic acid
    相似度:61.5%
European Journal of Organic Chemistry          2010                   5672-5680
Synthesis and Structural Analysis of Substituted Tripod-Shaped Tri- and Tetra(p-phenylene)s
Jesús Hierrezuelo, Elena Guillén, J. Manuel López-Romero, Rodrigo Rico, M. Rosa López-Ramírez, J. Carlos Otero and Chengzhi Cai
Structure      13C NMR   碳谱模拟图
5 .     (E)-2-(4-fluorostyryl)-3,5,6-trimethylpyrazine
C15H15FN2     相似度:61.5%
Chemical Biology & Drug Design          2012          79          731-739
Ligustrazine Derivatives. Part 4: Design, Synthesis, and Biological Evaluation of Novel Ligustrazine-based Stilbene Derivatives as Potential Cardiovascular Agents
Lijuan Deng, Xiuli Guo, Li Zhai, Yuning Song, Hongfei Chen, Peng Zhan, Jingde Wu and Xinyong Liu
Structure      13C NMR   碳谱模拟图
6 .     3-(2-furanyl)-6-(3,5-dinitrophenyl)-1,2,4-triazolo[3,4-b]-1,3,4-thiadiazole
C13H6N6O5S     相似度:58.3%
Molecules          2002          7          681-689
Synthesis and Biological Activity of 3-(2-Furanyl)-6-Aryl-1, 2, 4-Triazolo[3, 4-b]-1, 3, 4 –Thiadiazoles
Li-Xue Zhang, An-Jiang Zhang, Xian-Xing Chen, Xin-Xiang Lei, Xiang-Yun Nan, Dong-Yong Chen and Zi-Yi Zhang
Structure      13C NMR   碳谱模拟图
7 .     3-methyl-2-(4-chlorophenyl)-6-phenyl-1,2,4-triazin-5(2H)-one
C16H12ClN3O     相似度:58.3%
Journal of Heterocyclic Chemistry          2008          45          975-979
Studies with 2-arylhydrazononitriles: Further investigations on reactivity of 2-arylhydrazononitriles towards hydroxylamine
Sayed M. Riyadh,Hamad M. Al-Matar and Mohamed H. Elnagdi
Structure      13C NMR   碳谱模拟图
8 .     N,N-bis(4-methylphenacyl)-p-toluidine
C25H25NO2     相似度:58.3%
Journal of Heterocyclic Chemistry          2007          44          133-136
Synthesis of novel 3,5,7-triaryl-5,6-dihydro-4h-1,2,5-triazepines
Gurusamy Ravindran,Shanmugam Muthusubramanian,Sanguvan Selvaraj and Subbu Perumal
Structure      13C NMR   碳谱模拟图
9 .     ethyl 3-chloroquinoxaline-2-carboxylate
    相似度:58.3%
Journal of Heterocyclic Chemistry          2007          44          1139-1143
Pyrazolo[4',3':5,6]pyrano[2,3-b]quinoxalin-4(1H)-one: Synthesis and characterization of a novel tetracyclic ring system
Gernot A. Eller,Barbara Datterl and Wolfgang Holzer
Structure      13C NMR   碳谱模拟图
10 .     3,5-dichlorobenzo[h][1,6]naphthyridine
C12H6N2Cl2     相似度:58.3%
Journal of Heterocyclic Chemistry          2003          40          255-259
Synthesis of novel benzo[h] [1,6]naphthyridines via a rearrangement of hexahydro-5H-pyrrolo [2,1-c] [1,4]benzodiazepines
Antoine Hinschberger,Frédéric Fabis,Jana Sopkova-De Oliveira Santos and Sylvain Rault
Structure      13C NMR   碳谱模拟图
11 .     8-benzoyl-3,7-dimethyl-6H-pyrazolo[5,1-c][1,2,4]triazin-4-one
C14H12N4O2     相似度:58.3%
Journal of Heterocyclic Chemistry          2001          38          711-716
Synthesis of some novel 3,7-dimethyl-4H-pyrazolo[5,1-c][1,2,4]triazin-4-ones
Ahmed A. El-Barbary, Mahmoud A. El-Badawi and Yasser M. Loksha
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