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sunshine_欢木虫 (著名写手)
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[求助]
求大神帮着解谱 已有1人参与
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溶剂是吡啶 碳谱数据： 14.823,16.369,17.1,17.66,20.445,21.353,23.933,24.234,26.716,26.912,29.890,30.86,31.405,33.906,34.344,35.139,36.866,40.097,40.459,42.555,62.087,62.789,69.776,71.665,71.722,75.151,75.299,75.471,76.505,76.727,77.961,78.282,78.483,81.576,84.609,102.401,105.075,105.168,105.877,155.742,165.128 应该是甾体皂苷类 |
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- 附件 2 : H谱.jpg
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2楼2014-03-14 18:49:05
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【答案】应助回帖
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sunshine_欢: 金币+5, ★有帮助 2014-03-17 09:35:24
sunshine_欢: 金币+5, ★有帮助 2014-03-17 09:35:24
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查询结果：共查到3931个化合物(查询结果仅供参考) 1 . anemarrhenasaponin IV C45H74O18 相似度:75.6% Chemical & Pharmaceutical Bulletin 1994 42 2342-2345 New Steroidal Saponins from the Rhizomes of Anemarrhena asphodeloides BUNGE (Liliaceae) Setsuo SAITO,Satoshi NAGASE and Koki ICHINOSE Structure 13C NMR Structure & 13C NMR 碳谱模拟图 2 . aspacochioside C C45H74O17 相似度:75.5% Chinese Chemical Letters 2003 14 717-719 A New Furost-20(22)-ene Oligoglycoside from Asparagus cochinchinensis Yong Chun YANG, Sheng Yang HUANG, Shun Yan MO, Chun YANG, Jian Gong SHI Structure 13C NMR Structure & 13C NMR 碳谱模拟图 3 . Aspacochioside C C45H74O17 相似度:75.5% Journal of Asian Natural Products Research 2004 6 99-105 FUROSTANOL OLIGOGLYCOSIDES FROM ASPARAGUS COCHINCHINENSIS JIAN-GONG SHI,, GUO-QIANG LI, SHENG-YANG HUANG, SHUN-YAN MO,YAN WANG, YONG-CHUN YANG and WEN-YAN H Structure 13C NMR Structure & 13C NMR 碳谱模拟图 4 . Ys-IV 相似度:75.5% Phytochemistry 1989 28 1215-1217 The steroidal glycosides from the caudex of Yucca gloriosa Kimiko Nakano,Tokushi Yamasaki,Yukiko Imamura,Kōtarō Murakami,Yoshihisa Takaishi,Toshiaki Tomimatsu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 5 . 薤白皂苷 F C45H74O18 相似度:75.5% Chinese Journal of Medicinal Chemistry 2005 15 142-147 Study on bioactive steroidal saponins of Allium macrostemon Bunge CHEN Hai-feng, WANGNai-li, YAO Xin-sheng Structure 13C NMR Structure & 13C NMR 碳谱模拟图 6 . schidigera-saponin A2 C44H68O18 相似度:75% Journal of Natural Products 2000 63 332-338 Antiyeast Steroidal Saponins from Yucca schidigera (Mohave Yucca), a New Anti-Food-Deteriorating Agent Masazumi Miyakoshi,Yukiyoshi Tamura, Hitoshi Masuda, Kenji Mizutani,Osamu Tanaka, Takao Ikeda,Kazuhiro Ohtani, Ryoji Kasai,and Kazuo Yamasaki Structure 13C NMR Structure & 13C NMR 碳谱模拟图 7 . (25R,S)-5β-spirostan-3β-ol 3-O-{O-β-D-glucopyranosyl-(1→2)-O-[β-D-xylopyranosyl-(1→3)]-β-D-galactopyranoside} C44H72O17 相似度:75% Chemical & Pharmaceutical Bulletin 1995 43 1162-1166 Structures of Toxic Steroidal Saponins from Narthecium asiaticum MAXIM. Toshihiro INOUE,Yoshihiro MIMAKI,Yutaka SASHIDA and Masato KOBAYASHI Structure 13C NMR Structure & 13C NMR 碳谱模拟图 8 . asparagusin A 相似度:75% Chinese Chemical Letters 2000 11 793-794 A New Enolate Furostanoside from Asparagus Filicinus Xiao Dong CONG , Wen Cai YE, Chun Tao CHE Structure 13C NMR Structure & 13C NMR 碳谱模拟图 9 . asparagusin A 相似度:75% Chinese Traditional and Herbal Drugs 2012 43 1716-1720 Steroids from tubers of Asparagus filicinus TAO Hua-ming; WANG Li-shu; ZHAO Da-qing; ZHU Quan-hong; YIN Yong-guan; LIU Yong-hong Structure 13C NMR Structure & 13C NMR 碳谱模拟图 10 . Filiasparoside F C43H70O17 相似度:74.4% Steroids 2010 75 734-739 Steroidal saponins and ecdysterone from Asparagus filicinus and their cytotoxic activities Jia-Jun Wu, Ka-Wing Cheng, Xiao-Feng Zuo, Ming-Fu Wang, Ping Li, Lu-Yong Zhang, Hao Wang, Wen-Cai Ye Structure 13C NMR Structure & 13C NMR 碳谱模拟图 11 . aneinarsaponin B C45H74O18 相似度:73.3% Planta Medica 1991 57 460-462 A New Active Steroidal Saponin from Anemarrhena asphodelo ides DongJun-xing, and Han Gong Yu Structure 13C NMR Structure & 13C NMR 碳谱模拟图 12 . Macrostemonoside F C45H74O18 相似度:73.3% Chinese Chemical Letters 1993 4 141-144 STUDIES ON TWO NEW FUROSTANOL GLYCOSIDES FROM ALLIUM MACROSTEMON BUNGE JUN PENG PENG,XUAN WANG AND XIN SHENG YAO Structure 13C NMR Structure & 13C NMR 碳谱模拟图 13 . timosaponin B III 相似度:73.3% Chinese Chemical Letters 2007 18 171-174 Two new saponins from Anemarrhena asphodeloides Bge Ying Peng, Yu Jing Zhang , Zhi Qiang Ma, Wei San Pan, Yu Qing Sun,Shao Jiang Song Structure 13C NMR Structure & 13C NMR 碳谱模拟图 14 . furost-20(22)-ene-3β,26-diol-3-O-β-D-glucopyranosyl(1→2)-β-D-galactopyranoside C45H74O18 相似度:73.3% Acta Pharmaceutica Sinica 1992 27 26-32 STUDIES ON THE ACTIVE CONSTITUENTES OF ANEMARRHENA ASPHODELOIDES BUNGE JX Dong; GY Han Structure 13C NMR Structure & 13C NMR 碳谱模拟图 15 . macrostemonoside F C45H74O18 相似度:73.3% Acta Pharmaceutica Sinica 1993 28 526-531 STUDIES ON TWO NEW FUROSTANOL GLYCOSIDES FROM ALLIUM MACROSTEMON BUNGE JP Peng; X Wang and XS Yao Structure 13C NMR Structure & 13C NMR 碳谱模拟图 16 . anemarsaponin B 相似度:73.3% Acta Pharmaceutica Sinica 1996 31 271-277 STUDIES ON THE FUROSTANOL SAPONINS FROM ANEMARRHENA ASPHODELOIDES BUNGE BP M; JX Dong; BJ Wang and XZ Yan Structure 13C NMR Structure & 13C NMR 碳谱模拟图 17 . pseudoprototimosaponin A III C45H74O18-H2O 相似度:73.3% Journal of Natural Products 1993 Vol 56 345 Isolation of Pseudoprototimosaponin AIII from Rhizomes of Anemarrhena asphodeloides and Its Hypoglycemic Activity in Streptozotocin-Induced Diabetic Mice Noboru Nakashima, Ikuko Kimura, Masayasu Kimura, Hiromichi Matsuura Structure 13C NMR Structure & 13C NMR 碳谱模拟图 18 . anemarsaponin B 相似度:73.3% Korean Journal of Pharmacognosy 1999 30(2) 163-167 Isolation and Quantitative Determination of Anemarsaponin B from the Rhizomes of Anemarrhena asphodeloides Bunge Lee, Joo-Mi; Lee, Seung-Ho; Park, Jeong-Hill; Kang, Shin-Jung; Chang, Seung-Yeup; Lee, Kyong-Soon; Son, Kun-Ho Structure 13C NMR Structure & 13C NMR 碳谱模拟图 19 . timosaponin BII 相似度:73.3% Journal of Shenyang Pharmaceutical University 1996 13 34-40 A Study on the chemical constituents of Anemarrhena asphodeloides Bge. Bian ji, Xu sui su, Huang song, Wang ze xing Structure 13C NMR Structure & 13C NMR 碳谱模拟图 20 . anemarsaponin B-II C45H76O19 相似度:73.3% Journal of Ethnopharmacology 2008 118 271-279 Antiosteoporotic chemical constituents from Er-Xian Decoction, a traditional Chinese herbal formula Luping Qin, Ting Han, Qiaoyan Zhang, Dapeng Cao, Hua Nian, Khalid Rahman, Hanchen Zheng Structure 13C NMR Structure & 13C NMR 碳谱模拟图 21 . anemarnoside B C45H74O19 相似度:73.3% Journal of Asian Natural Products Research 2013 15 891-898 Steroidal saponins from Anemarrhena asphodeloides Qing-Bo Liu, Ying Peng, Ling-Zhi Li, Pin-Yi Gao, Yu Sun, Li-Hong Yu & Shao-Jiang Song Structure 13C NMR Structure & 13C NMR 碳谱模拟图 22 . aspacochioside C45H74O17 相似度:73.3% Archives of Pharmacal Research 2011 34 1587-1591 A New Furostanol Saponin from Asparagus cochinchinensis Yang Shen, Cong-Li Xu, Wei-Dong Xuan, Hui-Liang Li, Run-Hui Liu, Xi-Ke Xu, and Hai-Sheng Chen Structure 13C NMR Structure & 13C NMR 碳谱模拟图 23 . Anemarsaponin B 相似度:73.3% Journal of Medicinal Plants Research 2011 5 1062-1065 Anti-respiratory syncytial virus (RSV) activity of timosaponin A-III from the rhizomes of Anemarrhena asphodeloides Ui Joung Youn, Ji-Eun Jang, Joo-Won Nam, Yoo Jin Lee, Young Min Son, Hyun Ji Shin, Ah-Reum Han, Jun Chang and Eun-Kyoung Seo Structure 13C NMR Structure & 13C NMR 碳谱模拟图 24 . (25S)-26-O-β-D-glucopyranosyl-22-hydroxy-5β-furostane-3β,26-diol 3-O-β-D-glucopyranosyl-(1→2)-O-β-D-galactopyranoside 相似度:73.3% Yakugaku Zasshi 1991 111 306-310 Saponins of Anemarrhenae Rhizoma Seiji NAGUMO, Shinichiro KISHI, Takao INOUE, Masahiro NAGAI Structure 13C NMR Structure & 13C NMR 碳谱模拟图 25 . (25R)-5β-spirostan-3β-yl O-β-D-glucopyranosyl-(1→3)-β-D-galactopyranoside C39H64O13 相似度:73.1% Journal of Natural Products 2009 72 1399-1404 Steroidal Glycosides from Agave utahensis and Their Cytotoxic Activity Akihito Yokosuka,Maki Jitsuno,Satoru Yui, Masatoshi Yamazaki, and Yoshihiro Mimaki Structure 13C NMR Structure & 13C NMR 碳谱模拟图 26 . (25R)-5β-spirostan-3β-ol 3-O-β-D-glucopyranosyl-(1→6)-β-D-glu-copyranoside C39H64O13 相似度:73.1% Planta Medica 2006 72 667-670 Bioactive Steroidal Saponins from Smilax medica Sautour, M.; Miyamoto, T.; Lacaille-Dubois, M.-A. Structure 13C NMR Structure & 13C NMR 碳谱模拟图 27 . Vernocuminoside A C41H66O15 相似度:73.1% Steroids 2009 74 51-61 New vernocuminosides from the stem barks of Vernonia cumingiana Benth Jing Liu, Yunbao Liu, Yikang Si, Shishan Yu, Jing Qu, Song Xu, Youcai Hu, Shuanggang Ma Structure 13C NMR Structure & 13C NMR 碳谱模拟图 28 . 25(S)-5β-spirostan-3β-ol 3-O-R-Larabinopyranosyl-(1→4)-[β-D-glucopyranosyl-(1→2)]-β-Dglucopyranoside 相似度:72.7% Journal of Natural Products 2004 67 194-200 Bioactive Constituents from Asparagus cochinchinensis Hong-Jie Zhang, Kongmany Sydara, Ghee Teng Tan, Cuiying Ma, Bounhoong Southavong, D. Doel Soejarto, John M. Pezzuto, and Harry H. S. Fong Structure 13C NMR Structure & 13C NMR 碳谱模拟图 |
3楼2014-03-14 18:49:13
sunshine_欢
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4楼2014-03-17 09:35:04
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