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常雨

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[求助] 化合物微谱数据求助 已有1人参与

化合物碳谱如下:
17.2,20.8,21.4,45.8,47.4,49.6,65.6,77.3,83.4,87.3,123.5,131.4,135.5,149.9

[ Last edited by 常雨 on 2014-1-10 at 15:03 ]
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常雨: 金币+15, ★★★★★最佳答案 2014-01-10 16:40:22
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1 .     (-)-methyl dihydrophaseate
    ?????:75%
Chemical & Pharmaceutical Bulletin          1993          41          178-182
Chemical Constituents of Astragali Semen
Baoliang CUI,Motoyuki NAKAMURA,Junei KINJO and Toshihiro NOHARA
Structure      13C NMR   ???????
2 .     dihydrophaseic acid
C15H22O5     ?????:73.3%
Korean Journal of Pharmacognosy          2006          37(4)          290-293
Isolation of Dihydrophaseic Acid from Seed Extract of Nelumbo nucifera
Seo, Jee-Hee; Choi, Yeon-Hee; Yoo, Mi-Young; Hong, Kyung-Sik; Lee, Byung-Hoi; Yon, Gyu-Hwan; Kim, Young-Sup; Kim, Young-Kyoon; Ryu, Shi-Yong
Structure      13C NMR   ???????
3 .     4'-dihydrophaseic acid
    ?????:66.6%
Phytochemistry          2010          71          693-700
Gynostemosides A?CE, megastigmane glycosides from Gynostemma pentaphyllum
Zhen Zhang, Wei Zhang, Yan-Ping Ji, Yun Zhao, Chuan-Gui Wang, Jin-Feng Hu
Structure      13C NMR   ???????
4 .     Monaspilosuslin
C15H24O6     ?????:66.6%
Natural Product Research          2010          24          750-758
A new sesquiterpene isolated from the extracts of the fungus Monascus pilosus-fermented rice
Ming-Jen Cheng; Ming-Der Wu; Ih-Sheng Chen; Gwo-Fang Yuan
Structure      13C NMR   ???????
5 .     trans-4-dihydrophaseic acid
C15H22O5     ?????:66.6%
Chemistry of Natural Compounds          2013          49          486-492
Chemical Constituents from Aphanamixis grandifolia
Qi Zeng, Ji Ye, Jie Ren, Xiang-rong Cheng, Jiang-jiang Qin, Hui-Zi Jin, Wei-Dong Zhang
Structure      13C NMR   ???????
6 .     dihydrophaseic acid
    ?????:66.6%
Natural Products and Bioprospecting          2012          2          150-153
Two new glucosides from the pellicle of the walnut (Juglans regia)
Le Cai, Chuan-Shui Liu, Xiao-Wei Fu, Xiao-Jing Shen, Tian-Peng Yin, Ya-Bin Yang, Zhong-Tao Ding
Structure      13C NMR   ???????
7 .     (-)-methyl dihydrophaseate
C16H24O5     ?????:62.5%
Chinese Traditional and Herbal Drugs          2012          43          1685-1687
Isolation and identification of two sesquiterpenes from flowers of Carthamus tinctorius
LI Xiao-feng; HU Xiao-ru; DAI Zhong; ZHANG Yan; LIANG Hong; LIN Rui-chao
Structure      13C NMR   ???????
8 .     15-Hydroxy phaseic acid
C15H22O6     ?????:60%
Phytochemistry Letters          2012          5          297-300
Terpenoids from the leaves of Podocarpus gracilior
Laura Faiella, Abeer Temraz, Tiziana Siciliano, Nunziatina De Tommasi, Alessandra Braca
Structure      13C NMR   ???????
9 .     1,7,7-trimethyl-2-exo-norbornyl p-nitrobenzoate
    ?????:60%
Journal of the Chinese Chemical Society          1991          38          609-612
Nuclear Magnetic Resonance Studies ??. Carbon-13 Chemical Shifts of Some Methyl-Substituted Norbornyl p-Nitrobenzoates
???V??(Kwang-Ting Liu);??????(Hui-Ju Chen);???P(Pao-Feng Chiu);??????(Shu-Ming Lee)
Structure      13C NMR   ???????
10 .     6-hydroxy-dihydrophaseic acid
C15H22O6     ?????:60%
Phytochemistry          2012          80          137-147
Sesquiterpenes from the roots of Illicium dunnianum
Jian Bai, Hui Chen, Zhen-Feng Fang, Shi-Shan Yu, Wen-Jie Wang, Yang Liu, Shuang-Gang Ma, Yong Li, Jing Qu, Song Xu, Jun-Hong Liu, Fen Zhao, Nan Zhao
Structure      13C NMR   ???????
11 .     7,7-dimethyl-2-exo-norbornyl p-nitrobenzoate
    ?????:57.1%
Journal of the Chinese Chemical Society          1991          38          609-612
Nuclear Magnetic Resonance Studies ??. Carbon-13 Chemical Shifts of Some Methyl-Substituted Norbornyl p-Nitrobenzoates
???V??(Kwang-Ting Liu);??????(Hui-Ju Chen);???P(Pao-Feng Chiu);??????(Shu-Ming Lee)
Structure      13C NMR   ???????
12 .     7,7-dimethyl-2-endo-norbornyl p-nitrobenzoate
    ?????:57.1%
Journal of the Chinese Chemical Society          1991          38          609-612
Nuclear Magnetic Resonance Studies ??. Carbon-13 Chemical Shifts of Some Methyl-Substituted Norbornyl p-Nitrobenzoates
???V??(Kwang-Ting Liu);??????(Hui-Ju Chen);???P(Pao-Feng Chiu);??????(Shu-Ming Lee)
Structure      13C NMR   ???????
13 .     ??OH-S-2900-imide
    ?????:57.1%
Journal of Agricultural and Food Chemistry          2006          54          4333-4342
Metabolism of N-[(R)-1-(2,4-Dichlorophenyl)ethyl]-2-cyano-3,3-dimethylbutanamide (Delaus, S-2900) and Its Isomer, N-[(S)-1-(2,4-Dichlorophenyl)ethyl]-2-cyano-3,3-dimethylbutanamide (S-2900S), in Rats. 1. Identification of Metabolites in Feces and Urine
Yoshitaka Tomigahara, Naohiko Isobe, Hideo Kaneko, and Iwao Nakatsuka
Structure      13C NMR   ???????
14 .     5-PhOH-??OH-S-2900-imide
    ?????:57.1%
Journal of Agricultural and Food Chemistry          2006          54          4333-4342
Metabolism of N-[(R)-1-(2,4-Dichlorophenyl)ethyl]-2-cyano-3,3-dimethylbutanamide (Delaus, S-2900) and Its Isomer, N-[(S)-1-(2,4-Dichlorophenyl)ethyl]-2-cyano-3,3-dimethylbutanamide (S-2900S), in Rats. 1. Identification of Metabolites in Feces and Urine
Yoshitaka Tomigahara, Naohiko Isobe, Hideo Kaneko, and Iwao Nakatsuka
Structure      13C NMR   ???????
15 .     compound 3
C15H18O3     ?????:53.3%
Tetrahedron Letters          2003          44          6759-6761
A novel neolignan, mansoxetane, and two new sesquiterpenes, mansonones R and S, from Mansonia gagei
Pattara Tiew, Hiromitsu Takayama, Mariko Kitajima, Norio Aimi, Udom Kokpol, Warinthorn Chavasiri
Structure      13C NMR   ???????
16 .     (E)-4-(3a,5-dihydroxy-3,6a-dimethylhexahydro-2H-3,5-methanocyclopentafuran-4-yl)-3-methylbut-3-enoic acid
C16H24O5     ?????:53.3%
Phytochemistry          2012          80          89-98
Electrolytic reduction of abscisic acid methyl ester and its free acid
Nobuhiro Hirai, Kumiko Iwami, Mari Horiuchi, Kenji Kano, Yasushi Todoroki, Hajime Ohigashi
Structure      13C NMR   ???????
17 .     6-[(E)-2-(3-Methoxyphenyl)ethenyl]-2,3,4,5-tetrahydropyridine
C14H17NO     ?????:50%
Journal of Natural Products          2009          72          312-315
Piperidine and Tetrahydropyridine Alkaloids from Lobelia siphilitica and Hippobroma longiflora
Julie R. Kesting, Inge-Lise Tolderlund, Anders F. Pedersen, Matthias Witt, Jerzy W. Jaroszewski, and Dan Staerk
Structure      13C NMR   ???????
18 .     ascleposide A(2a)
C13H22O4     ?????:50%
Chemical & Pharmaceutical Bulletin          2000          48(12)          1908-1911
5, 11-Epoxymegastigmanes from the Leaves of Asclepias fruticosa
Fumiko ABE and Tatsuo YAMAUCHI
Structure      13C NMR   ???????
19 .     2-[(1'e)-3'-methoxy-3',7'-dimethylocta-1',6'-dienyl]benzene-1,4-diol
    ?????:50%
Journal of Natural Products          2002          65          1328-1331
New Meroterpenoids from the Ascidian Aplidium conicum
Leda Garrido, Eva Zub??a, Mar??a J. Ortega, and Javier Salv??
Structure      13C NMR   ???????
20 .     cucubalol
C13H22O4     ?????:50%
Planta Medica          2002          68          91-94
New Norsesquiterpenoids from Cucubalus baccifer
Yong-Xian Cheng,Jun Zhou,Shi-Ming Deng,Ning-Hua Tan
Structure      13C NMR   ???????
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