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书名Functionalized Inorganic Fluorides 作者ALAIN TRESSAUD Research Director CNRS (Emeritus), ICMCB–CNRS, Bordeaux University, France 语言英语 页数617 出版社wiley ISBN: 978-0-470-74050-7 (Cloth 目录 1 Sol-Gel Synthesis of Nano-Scaled Metal Fluorides – Mechanism and Properties 1 Erhard Kemnitz, Gudrun Scholz and Stephan Ru¨diger 1.1 Introduction 1 1.1.1 Sol-Gel Syntheses of Oxides – An Intensively Studied and Widely Used Process 1 1.1.2 Sol-Gel Syntheses of Metal Fluorides – Overview of Methods 2 1.2 Fluorolytic Sol-Gel Synthesis 4 1.2.1 Mechanism and Properties 5 1.2.2 Insight into Mechanism by Analytical Methods 8 1.2.3 Exploring Properties 27 1.2.4 Possible Fields of Application 29 References 35 2 Microwave-Assisted Route Towards Fluorinated Nanomaterials 39 Damien Dambournet, Alain Demourgues and Alain Tressaud 2.1 Introduction 39 2.2 Introduction to Microwave Synthesis 40 2.2.1 A Brief History 40 2.2.2 Mechanisms to Generate Heat 40 2.2.3 Advantages of Microwave Synthesis 41 2.2.4 Examples of Microwave Experiments 41 2.3 Preparation of Nanosized Metal Fluorides 42 2.3.1 Aluminium-based Fluoride Materials 42 2.3.2 Microwave-assisted Synthesis of Transition Metal Oxy-Hydroxy-Fluorides 2.4 Concluding Remarks 64 Acknowledgements 64 References 65 3 High Surface Area Metal Fluorides as Catalysts 69 Erhard Kemnitz and Stephan Ru¨diger 3.1 Introduction 69 3.2 High Surface Area Aluminium Fluoride as Catalyst 71 3.3 Host-Guest Metal Fluoride Systems 74 3.4 Hydroxy(oxo)fluorides as Bi-acidic Catalysts 78 3.5 Oxidation Catalysis 84 3.6 Metal Fluoride Supported Noble Metal Catalysts 88 3.6.1 Hydrodechlorination of Monochlorodifluoromethane 90 3.6.2 Hydrodechlorination of Dichloroacetic Acid (DCA) 94 3.6.3 Suzuki Coupling 95 References 97 4 Investigation of Surface Acidity using a Range of Probe Molecules 101 Alexandre Vimont, Marco Daturi and John M. Winfield 4.1 Introduction 101 4.1.1 Setting the Scene: Metal Fluorides versus Metal Oxides 102 4.1.2 Some Examples of the Application of FTIR Spectroscopy to the Study of Surface Acidity in Metal Oxides 103 4.1.3 A Preview 107 4.2 Characterization of Acidity on a Surface: Contrasts with Molecular Fluorides 108 4.2.1 Molecular Brønsted and Molecular Lewis Acids 108 4.2.2 A Possible Benchmark for Solid Metal Fluoride, Lewis Acids: Aluminium Chlorofluoride 109 4.3 Experimental Methodology 110 4.3.1 FTIR Spectroscopy 110 4.3.2 Characteristic Reactions and the Detection of Adsorbed Species by a Radiotracer Method 112 4.4 Experimental Studies of Surface Acidity 117 4.4.1 Using FTIR Spectroscopy 118 4.4.2 Using HCl as a Probe with Detection via [36Cl]-Labelling 123 4.4.3 Metal Fluoride Surfaces that Contain Surface Hydroxyl Groups: Aluminium Hydroxy Fluorides with the Hexagonal Tungsten Bronze Structure 129 4.4.4 Possible Geometries for HCl Adsorbed at Metal Fluoride Surfaces: Relation to Oxide and Oxyfluoride Surfaces 135 4.5 Conclusions 136 References 137  QQ图片20140109171113.jpg [ Last edited by 雷光月 on 2014-1-9 at 18:40 ] |
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