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Contri

新虫 (初入文坛)

[求助] 催化反应后发现产物种类多,有出现大分子副产物,求教大神解答!!

小学渣第一次接触催化剂制备的研究方向,一个多月了发现基本没什么进展,很是着急…………

现在的情况是:我重复之前前辈的实验,制备出的催化剂在相同温度下,选择性低了40%,GC检测出产物最多有十几个峰,有些滞留时间还很长。。。。
                        昨天改了一下配方,制备催化剂时改用醋酸盐了,高温选择性有所提高,但是低温时选择性还是个渣,产物种类减少了,但还是有5个峰,滞留时间长的产物还是有,这和前辈的比还是个渣呀!!!!!!(前辈的实验能在低温时就可以100%转化和100%选择性,我高温是最高的选择性只有96.5%)
                     
  小学渣请教各位大牛,我的催化剂大概问题是出在哪了。。。。制备的过程都是按照之前前辈的步骤做的。。。。。产物种类多和出现滞留时间长的物质,是不是说明我的催化剂催化强度太大了(我制备的是固体酸催化剂)???跪求大牛赐教!!!!!!!!

[ Last edited by Contri on 2013-11-21 at 10:27 ]
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