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| Hydrothermal synthesis of Ni-Fe layered double hydroxide with high crystallinity using homogeneous precipitation method |
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zyc102(杈杈代发): 金币+5, Thanks 2013-11-09 18:27:08
zyc102(杈杈代发): 金币+5, Thanks 2013-11-09 18:27:08
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Accession number: 20134416911165 Title: Hydrothermal synthesis of Ni-Fe layered double hydroxide with high crystallinity using homogeneous precipitation method Authors: Zhang, Ying Chao1 Author affiliation: 1 Beijing Solar Energy Research Institute Co. Ltd, Beijing 100012, China Corresponding author: Zhang, Y. C. (zyc102@126.com) Source title: Advanced Materials Research Abbreviated source title: Adv. Mater. Res. Volume: 821-822 Monograph title: Advances in Textile Engineering and Materials III Issue date: 2013 Publication year: 2013 Pages: 1313-1316 Language: English ISSN: 10226680 ISBN-13: 9783037858844 Document type: Conference article (CA) Conference name: 3rd International Conference on Textile Engineering and Materials, ICTEM2013 Conference date: August 24, 2013 - August 25, 2013 Conference location: Dalian, China Conference code: 100396 Publisher: Trans Tech Publications Ltd, Kreuzstrasse 10, Zurich-Durnten, CH-8635, Switzerland Abstract: Ni-Fe layered double hydroxide containing carbonate anion (CO3 2-) has been successfully synthesized by a process of homogeneous precipitation involving urea hydrolysis under hydrothermal conditions. Factors that influence the composition and the crystallinity degree of NiFe-LDH, such as the molar fraction of urea/NO3 - in solution, the total metal ion concentration in solution and the aging time, have been investigated in detail. Structure and morphology of the sample were characterized by X-ray powder diffraction (XRD), Fourier transform infrared (FT-IR) spectra and scanning electron microscope (SEM). The results indicate NiFe-LDH with high purity present well-crystalline, uniform crystallite size. © (2013) Trans Tech Publications, Switzerland. Number of references: 4 Main heading: Hydrothermal synthesis Controlled terms: Metal ions - Nickel - Precipitation (chemical) - Scanning electron microscopy - Textiles - Urea - X ray powder diffraction Uncontrolled terms: Crystallinity degree - Fourier transform infrared - Homogeneous Precipitation - Homogeneous precipitation method - Hydrothermal conditions - Layered double hydroxides - Metal ion concentration - Structure and morphology Classification code: 819 Synthetic and Natural Fibers; Textile Technology - 804.1 Organic Compounds - 802.3 Chemical Operations - 931.3 Atomic and Molecular Physics - 802.2 Chemical Reactions - 548.1 Nickel - 533 Ore Treatment and Metal Refining - 741.1 Light/Optics DOI: 10.4028/www.scientific.net/AMR.821-822.1313 Database: Compendex Compilation and indexing terms, © 2013 Elsevier Inc. |
2楼2013-11-08 16:08:07