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chengmiaojy

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[求助] 微谱求助,谢谢

13C NMR (75 MHz, MeOD) δ 30.52, 56.39, 56.44, 56.77,108.18, 111.63, 113.72, 115.80, 116.44, 123.04, 123.93,125.22, 127.74, 146.94, 148.58, 149.27, 150.25, 152.45, 170.24, 181.99 .
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lifeliuyan

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【答案】应助回帖

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chengmiaojy(豆哥代发): 金币+10, 谢谢 2013-11-11 09:14:41
???????????鵽852????????(???????????ο?)  
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1 .     discretine N-oxide
C20H23NO5     ?????:70%
Journal of Natural Products          2008          71(12)          2057-2059
Antiplasmodial Alkaloids from Desmos rostrata
Ngoc Tuan Nguyen, Van Cuong Pham, Marc Litaudon, Françoise Gu??ritte, Philippe Grellier, Van Tuyen Nguyen, and Van Hung Nguyen
Structure      13C NMR   ???????

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2 .     N-trans-feruloil-3'-O-metoxidopamina
C19H21NO5     ?????:70%
Qu??mica Nova          2013          36          1111-1115
CONSTITUINTES QUÍMICOS DE Solanum buddleifolium Sendtn
Francisco das Chagas L. Pinto, Maria da Conceição M. Torres, Edilberto R. Silveira e Ot??lia Deusd??nia L. Pessoa*,Raimundo Braz-Filho,Maria Lenise da Silva Guedes
Structure      13C NMR   ???????

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3 .     8-hydroxydihydropalmatine
     ?????:66.6%
Journal of Natural Products          2003          66          481-486
Palmatine and Berberine Isolation Artifacts
Radek Marek, Pavlna Sečkov, Dagmar Hulov, Jaromr Marek, Ji Dostl, and Vladimr Sklen
Structure      13C NMR   ???????

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4 .     (E)-3',4'-dimethoxy-2'-(3,4-dimethoxycinnamoyloxy)-acetophenone
C21H22O7     ?????:66.6%
Bioorganic & Medicinal Chemistry          2009          17          7218-7226
Synthesis and antioxidant properties of new chromone derivatives
Ana Gomes, Ondrej Neuwirth, Marisa Freitas, Diana Couto, Daniela Ribeiro, Andrea G.P.R. Figueiredo, Artur M.S. Silva, Raquel S.G.R. Seixas, Diana C.G.A. Pinto, Augusto C. Tom??, Jos?? A.S. Cavaleiro, Eduarda Fernandes, Jos?? L.F.C. Lima
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


5 .     2-O-caffeoyl-3-O-feruloyltartaric acid
     ?????:66.6%
Natural Product Communications          2012          7          1353-1356
Efficient Counter-current Chromatographic Isolation and Structural Identification of Two New Cinnamic Acids from Echinacea purpurea
Ying Lu, JiaYin Li, MiLu Li, Xia Hu, Jun Tan and Zhong Hua Liu
Structure      13C NMR   ???????

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6 .     cilinaphthalide B
C23H22O7     ?????:65.2%
Journal of Natural Products          1999          62          1056-1058
Cytotoxic Lignans of Justicia ciliata
Shiow-Hwa Day, Nien-Yung Chiu, Shen-Jeu Won, and Chun-Nan Lin
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


7 .     (E)-3- (5'-hydroperoxy-2,2'-dihydroxy[1,1'-biphenyl]-4-yl)-2-propenoic acid
     ?????:65%
Chemistry of Natural Compounds          2005          41          17-21
CARBOXYLIC ACIDS FROM Phyllanthus urinaria
Wanxing Wei, Yuanjiang Pan, Yaozu Chen,Cuiwu Lin, Tengyou Wei, and Shukai Zhao
Structure      13C NMR   ???????

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8 .     N-trans-feruLoylmethoxytyramine
C19H21NO5     ?????:65%
Phytochemistry          1998          49          1443-1447
Amides from stems of annona cherimola
Chung-Yi Chen, Fang-Rong Chang, Hsin-Fu Yen, Yang-Chang Wu
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


9 .     N-cis-feruloylmethoxytyramine
C19H21NO5     ?????:65%
Phytochemistry          1998          49          1443-1447
Amides from stems of annona cherimola
Chung-Yi Chen, Fang-Rong Chang, Hsin-Fu Yen, Yang-Chang Wu
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


10 .     N-trans-feruloyl-3-methyldopamine
     ?????:65%
Planta Medica          2011          77          1528-1530
Downregulation of Matrix Metalloproteinase-13 by the Root Extract of Cyathula officinalis Kuan and its Constituents in IL-1??-treated Chondrocytes
Hyun Young Park, Hyun Lim, Hyun Pyo Kim, Yong Soo Kwon
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


11 .     7,8-dihydroxy-3',4',-dimethoxyisoflavone
C17H14O6     ?????:65%
Chemical & Pharmaceutical Bulletin          2009          57          346-360
Synthesis of Various Kinds of Isoflavones, Isoflavanes, and Biphenyl-Ketones and Their 1,1-Diphenyl-2-picrylhydrazyl Radical-Scavenging Activities
Hideyuki Goto, Yoshiyasu Terao and Shuji Akai
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


12 .     8,8'-bis-(dirhydroconifery l)-diferuloylate
C40H42O12     ?????:65%
Chinese Traditional and Herbal Drugs          2010          41          867-870
????????????о?(??)
??????;?????;?????;??????
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


13 .     N-trans-feruloylmethoxytyramine
     ?????:65%
Archives of Pharmacal Research          2005          28          1224-1227
Cytotoxic constituents from the whole plant of corydalis pallida
Hyang Rim Kim, Hye -Young Min, Yeon Hee Jeong, Sang Kook Lee and Nam Sook Lee, et al.
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


14 .     N-(2,3-Dimethoxyphenylethyl)-2-(3,4-dimethoxyphenyl)acetamide
     ?????:65%
Bioorganic & Medicinal Chemistry          1996          4          781-791
Coralyne and related compounds as mammalian topoisomerase I and topoisomerase II poisons
Darshan Makhey, Barbara Gatto, Chiang Yu, Angela Liu, Leroy F. Liu, Edmond J. LaVoie
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


15 .     5-(3,4-dimethoxybenzylidene)-2-(4-hydroxyphe-nylamino)thiazol-4(5H)-one
C18H16N2O4S     ?????:65%
Bioorganic & Medicinal Chemistry          2010          18          5090-5102
Synthesis of 5-arylidene-2-amino-4-azolones and evaluation of their anticancer activity
Ivanna Subtel??na, Dmytro Atamanyuk, Ewa Szyma??ska, Katarzyna Kieć-Kononowicz, Borys Zimenkovsky, Olexandr Vasylenko, Andrzej Gzella, Roman Lesyk
Structure      13C NMR   ???????

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16 .     N-trans-feruloylmethoxytyramine
     ?????:65%
Journal of the Chinese Chemical Society          1998          45          103-110
Chemical Constituents of Neolitsea parvigemma and Neolitsea Konishii
????B(Keh-Shaw Chen);?????s(Fang-Rong Chang);?Z???(Yi-Chen Chia);?????p(Tian-Shung Wu);??????(Yang-Chang Wu)
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


17 .     N-trans-feruloyl-3'-methoxytyramin
     ?????:65%
Food Science and Biotechnology          2011          20          555-560
Isolation and Identification of Cinnamic Acid Amides as Antioxidants from Allium fistulosum L. and Their Free Radical Scavenging Activity
Gee-Woo Seo, Jeong-Yong Cho, Jae-Hak Moon, and Keun-Hyung Park
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


18 .     (+)-tembetarine perchlorate
C20H25NO4     ?????:65%
Natural Medicines          2004          58          303-306
Quaternary Isoquinoline Alkaloids from Monodora junodii and M. grandidieri
Nishiyama Yumi,Murayama Chiaki, et al.
Structure      13C NMR   ???????

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19 .     3-???-4-????????????
    ?????:65%
China Journal of Chinese Materia Medica          2012          37          2092-2099
Non-anthraquinones constituents from the roots of Knoxia valerianoides
ZHAO Feng; WANG Sujuan; WU Xiuli; YU Yang; YUE Zhenggang; LIU Bo; LIN Sheng; ZHU Chenggen; YANG Yongchun; SHI Jiangong
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


20 .     8-trichloromethyl-7,8-dihydropalmatine
     ?????:63.6%
Journal of Natural Products          2003          66          481-486
Palmatine and Berberine Isolation Artifacts
Radek Marek, Pavlna Sečkov, Dagmar Hulov, Jaromr Marek, Ji Dostl, and Vladimr Sklen
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


21 .     isokaerophyllin
     ?????:61.9%
Phytochemistry          2003                   1375-1379
Immunosuppressive flavones and lignans from Bupleurum scorzonerifolium
Wen-Liang Chang, Li-Wen Chiu, Jenn-Haung Lai, Hang-Ching Lin
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


22 .     8-hydroxydihydropalmatine
     ?????:61.9%
Journal of Natural Products          2003          66          481-486
Palmatine and Berberine Isolation Artifacts
Radek Marek, Pavlna Sečkov, Dagmar Hulov, Jaromr Marek, Ji Dostl, and Vladimr Sklen
Structure      13C NMR   ???????

--------------------------------------------------------------------------------


23 .     13-methyl-palmatrubine
C21H22NO4     ?????:61.9%
Journal of Asian Natural Products Research          2008          10          1117-1121
Two new protoberberine quaternary alkaloids from Corydalis yanhusuo
Xing-Ye Cheng, Yue Shi, Shun-Liang Zheng, Wen Jin and Hong Sun
Structure      13C NMR   ???????

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24 .     7,8-dihydro-8-hydroxypalmatine
     ?????:61.9%
Phytochemistry          1999          50          279-281
A 7,8-dihydro-8-hydroxypalmatine from Enantia chlorantha
Pascal Wafo, Barthelemy Nyasse, Catherine Fontaine
Structure      13C NMR   ???????
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