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oyf8888

银虫 (小有名气)

[求助] 跪求4个微谱数据,衷心感谢!

溶剂均为氘代氯仿
1.  17.275,17.791,26.018,27.429,29.767,31.337,33.971,41.279,44.967,112.159,138.599,146.181,170.670,208.736,209.176

2.
15.598,20.341,21.950,23.028,25.297,28.628,29.531,42.068,46.728,49.445,55.743,57.026,73.054,211.430

3.  16.304,17.564,32.840,35.451,59.348,75.520,111.188,123.573,139.449,147.334

4.
18.247,22.625,31.269,33.090,63.196,80.825,84.657,110.634,144.883
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lifeliuyan

至尊木虫 (职业作家)

【答案】应助回帖

查询结果:共查到453个化合物(查询结果仅供参考)  
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1 .     compound E
     相似度:100%
Phytochemistry          1989          28          1425-1426
Sesquiterpenes from Eremophila species
Kim A. Dastlik,Peter G. Forster,Emilio L. Ghisalberti,Phillip R. Jefferies
Structure      13C NMR   碳谱模拟图

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2 .     oplopanone
     相似度:100%
Archives of Pharmacal Research          1997          20          363-367
Sesquiterpene components from the flower buds of Magnolia fargesii
Keun Young Jung, Dong Seon Kim, Sei Ryang Oh, Im Seon Lee and Jung Joon Lee, et al.
Structure      13C NMR   碳谱模拟图

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3 .     ent-oplopanone
C15H26O2     相似度:93.3%
Chemical & Pharmaceutical Bulletin          1987          35          124-135
Marine Natural Products. XVII. Nephtheoxydiol, a New Cytotoxic Hydroperoxy-Germacrane Sesquiterpene, and Related Sesquiterpenoids from an Okinawan Soft Coral of Nephthea sp. (Nephtheidae)
ISAO KITAGAWA,ZHENG CUI,BYENG WHA SON,MOTOMASA KOBAYASHI and YOSHIMASA KYOGOKU
Structure      13C NMR   碳谱模拟图

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4 .     oplopanone
C15H26O4     相似度:93.3%
Natural Product Research          2003          17          445-449
A new xanthone from Hedychium gardnerianum
Maria João Carvalho; Luís M. Carvalho; Ana Margarida Ferreira; Artur M. S. Silva
Structure      13C NMR   碳谱模拟图

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5 .     (-)-oplopanone
     相似度:93.3%
China Journal of Chinese Materia Medica          2009          34          990-993
Studies on chemical constituents in fruit of Alpinia oxyphylla
XU Junju, TAN Ninghua, ZENG Guangzhi, HAN Hongjin, HUANG Huoqiang, JI Changjiu, ZHU Meiju, ZHANG Yumei
Structure      13C NMR   碳谱模拟图

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6 .     oplopanone
C15H26O2     相似度:93.3%
China Journal of Chinese Materia Medica          2003          28          342-344
Studies on the Constituents in Rhizome of Homalomena occuta
HU Yongmei, YANG Zhonglin, YE Wencai, CHONG Qihou
Structure      13C NMR   碳谱模拟图

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7 .     Oplopanone
     相似度:93.3%
Phytochemistry          1995          39          603-607
Sesquiterpenes from leaves of Cryptomeria japonica
Wen-Chiung Su, Jim-Min Fang, Yu-Shia Cheng
Structure      13C NMR   碳谱模拟图

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8 .     Oplopanone
     相似度:93.3%
Natural Product Research          2012          26          850-858
A new sesquiterpenoid from the rhizomes of Homalomena sagittifolia
K.C. Wong, Abdul Hamid, I.M.S. Eldeen, M. Zaini Asmawi,S. Baharuddin, H.S. Abdillahi and J. Van Staden
Structure      13C NMR   碳谱模拟图

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9 .     oplopanone
     相似度:93.3%
Phytochemistry          1983          22          1457-1459
Sesquiterpene alcohols and triterpenoids from Liatris microcephala
Werner Herz, Kinzo Watanabe
Structure      13C NMR   碳谱模拟图

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10 .     oplopanone
     相似度:93.3%
Chinese Traditional and Herbal Drugs          2009          40          29-32
益智仁化学成分研究
刘楠;于新宇;赵红;赵余庆
Structure      13C NMR   碳谱模拟图

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11 .     Oplopanone
     相似度:93.3%
Chinese Journal of Natural Medicines          2008          6          339-341
Sesquiterpenes from the Stems of Croton caudatus Geisel. var. tomentosus Hook.
WANG Yuan; ZOU Zhong-Mei
Structure      13C NMR   碳谱模拟图

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12 .     Oplopanone
     相似度:93.3%
Archives of Pharmacal Research          2010          33          1317-1323
Scopoletin from the flower buds of Magnolia fargesii inhibits protein glycation, aldose reductase, and cataractogenesis Ex Vivo
Jun Lee, Nan Hee Kim, Joo Won Nam, Yun Mi Lee and Dae Sik Jang, et al.
Structure      13C NMR   碳谱模拟图

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13 .     oplopanone
     相似度:93.3%
Journal of the Chinese Chemical Society          2002          49          427-431
Cytotoxic Components from the Leaves of Schefflera taiwaniana
Yueh-Hsiung Kuo*, Jir-Mehng Lo and Yih-Fwu Chan
Structure      13C NMR   碳谱模拟图

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14 .     oplopanone
     相似度:93.3%
Journal of the Chinese Chemical Society          2005          52          369-374
Terpenoids from the Flower of Cacalia tangutica
Xia Liu, Quan-Xiang Wu and Yan-Ping Shi*
Structure      13C NMR   碳谱模拟图

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15 .     subdigitatone
C15H26O2     相似度:93.3%
Indian Journal of Chemistry          1995          34B          664-665
New sesquiterpene from Artemisia subdigitata
Yu Li, Yanping Shi & Yang Li
Structure      13C NMR   碳谱模拟图
3楼2013-10-14 09:59:49
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查看全部 5 个回答

lifeliuyan

至尊木虫 (职业作家)

【答案】应助回帖

感谢参与,应助指数 +1
查询结果:共查到85个化合物(查询结果仅供参考)  
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1 .     4,5-seco-Guaia-1(10),11-diene-4,5-dioxo
C15H22O2     相似度:100%
Tetrahedron          2011          67          9193-9198
Sesquiterpenoids, alantolactone analogues, and seco-guaiene from the roots of Inula helenium
Hai-Long Jiang, Jia Chen, Xiao-Jie Jin, Jun-Li Yang, Ya Li, Xiao-Jun Yao , Quan-Xiang Wu
Structure      13C NMR   碳谱模拟图

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2 .     mandassidione
C15H22O2     相似度:100%
Phytochemistry          1988          27          3319-3321
Mandassidione and other sesquiterpenic ketones from Cyperus articulatus
B. Nyasse,R. Ghogomu,Tih B.L. Sondengam,M. T. Martin,B. Bodo
Structure      13C NMR   碳谱模拟图

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3 .     cyperusol B1
C15H24O2     相似度:80%
Journal of Natural Products          2004          67          569-576
Structures of New Sesquiterpenes and Hepatoprotective Constituents from the Egyptian Herbal Medicine Cyperus longus
Fengming Xu, Toshio Morikawa, Hisashi Matsuda, Kiyofumi Ninomiya, and Masayuki Yoshikawa
Structure      13C NMR   碳谱模拟图

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4 .     mandassidione
     相似度:80%
China Journal of Chinese Materia Medica          2010          35          315-322
Terpenoids of Heteroplexis micocephala and their bioactivities
FAN Xiaona; LIN Sheng; ZHU Chenggen; HU Jinfeng; LIU Yang; CHEN Xiaoguang; CHEN Naihong; WANG Wenjie; SHI Jiangong
Structure      13C NMR   碳谱模拟图

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5 .     cyperusol B2
C15H24O2     相似度:73.3%
Journal of Natural Products          2004          67          569-576
Structures of New Sesquiterpenes and Hepatoprotective Constituents from the Egyptian Herbal Medicine Cyperus longus
Fengming Xu, Toshio Morikawa, Hisashi Matsuda, Kiyofumi Ninomiya, and Masayuki Yoshikawa
Structure      13C NMR   碳谱模拟图

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6 .     10-epi-Acora-3,11-dien-15-ol
     相似度:66.6%
Flavour and Fragrance Journal          2000          15          61-83
1,7-Cyclogermacra-1(10),4-dien-15-al, a sesquiterpene with a novel skeleton, and other sesquiterpenes from Haitian vetiver oil
Peter Weyerstahl, Helga Marschall, Ute Splittgerber and Dietmar Wolf
Structure      13C NMR   碳谱模拟图

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7 .     Huperzine W
C14H21NO2     相似度:60%
Chinese Chemical Letters          2002          13          331-332
Huperzine W, a Novel 14 Carbons Lycopodium Alkaloid from Huperzia serrata
Chang Heng TAN, Xiao Qiang MA, Guo Fu CHEN, Shan Hao JIANG,Da Yuan ZHU
Structure      13C NMR   碳谱模拟图

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8 .     4 (15)-cadinene-6,10-diol
C23H24O11     相似度:60%
Journal of Asian Natural Products Research          2004          6          199-204
CHEMICAL CONSTITUENTS FROM ALPINIA TONKINENSIS
JIAN ZHANG and LING-YI KONG
Structure      13C NMR   碳谱模拟图

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9 .     (-)-huperzine W
C14H21NO2     相似度:60%
Natural Products and Bioprospecting          2012          2          255-257
One-step synthesis of Lycopodium alkaloid (-)-huperzine W via Suzuki-Miyaura coupling
Tao Xu, Shi-Zhi Jiang, Huai-Rong Luo, Yu-Rong Yang
Structure      13C NMR   碳谱模拟图

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10 .     (1S,6R,7S,10S)-7-isopropyl-10-methyl-4-methylenedecahydronaphthalene-6,10-diol
C15H26O2     相似度:60%
Acta Crystallographica Section E          2007          63          o3579
6β,10β-Cadinene-6,10-diol: a sesquiterpenoid from the rhizome of Acorus calamus L.
Wei-Wei Dong, Kai-Bei Yu, Jian-Min Yue and Run-Hua Lu
Structure      13C NMR   碳谱模拟图
2楼2013-10-14 09:58:54
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lifeliuyan

至尊木虫 (职业作家)

【答案】应助回帖

查询结果:共查到49个化合物(查询结果仅供参考)  
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1 .     (6RS)-(E)-3,7-Dimethyl-2,7-octadiene-1,6-diol
     相似度:100%
Journal of Agricultural and Food Chemistry          1998          46          1966-1970
(S)-3,7-Dimethyl-5-octene-1,7-diol and Related Oxygenated Monoterpenoids from Petals of Rosa damascena Mill.
Holger Knapp, Markus Straubinger, Selenia Fornari, Noriaki Oka, Naoharu Watanabe, and Peter Winterhalter
Structure      13C NMR   碳谱模拟图

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2 .     compound 25
     相似度:90%
Organic Magnetic Resonance          1975          7          426-432
13C-NMR-Spektren von Monoterpenen
F. Bohlmann, R. Zeisberg and E. Klein
Structure      13C NMR   碳谱模拟图

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3 .     (3S)-(E)-2,6-dimethyl-10-methylene-1,6,11-dodecatrien-3-ol
     相似度:60%
Journal of Natural Products          1992          Vol 55          428
New Farnesane Sesquiterpenes from Hebeloma senescens
Maurizio Bocchi, Luigi Garlaschelli, Giovanni Vidari, Giorgio Mellerio
Structure      13C NMR   碳谱模拟图

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4 .     compound 2
C10H14O3     相似度:60%
Chemical & Pharmaceutical Bulletin          2009          57          294-297
Structure of New Monoterpene Glycoside from Sibiraea angustata RCHD. and Its Anti-obestic Effect
Yoshiaki Ito, Satoshi Kamo, Samir Kumar Sadhu, Takashi Ohtsuki, Masami Ishibashi and Yoshihiro Kano
Structure      13C NMR   碳谱模拟图

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5 .     compound 10f
C10H10N4O2     相似度:60%
Journal of Heterocyclic Chemistry          2000          37          1041-1048
Reactivity studies of ethyl(Z)-N-(2-amino-1,2-dicyanovinyl) formimidate with carbonyl compounds in the presence of base
M. Joséalves, M. Alice Carvalho, M. Fernanda, J. R. P. Proença and Brian L. Booth
Structure      13C NMR   碳谱模拟图

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6 .     (2Z)-2,6-dimethylhepta-2,6-diene-1,5-diol
     相似度:60%
Russian Journal of Organic Chemistry          2011          47          1287-1292
Synthesis of 6-hydroxycarvone derivatives and their oxidative decyclization with lead tetraacetate
R. F. Valeev, R. F. Bikzhanov, N. K. Selezneva, F. A. Gimalova and M. S. Miftakhov
Structure      13C NMR   碳谱模拟图

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7 .     (7RS)-(2E)-3,7-Dimethyl-2-octene-1,8-diol
     相似度:60%
Journal of Agricultural and Food Chemistry          1998          46          1966-1970
(S)-3,7-Dimethyl-5-octene-1,7-diol and Related Oxygenated Monoterpenoids from Petals of Rosa damascena Mill.
Holger Knapp, Markus Straubinger, Selenia Fornari, Noriaki Oka, Naoharu Watanabe, and Peter Winterhalter
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------


8 .     (7RS)-(2Z)-3,7-Dimethyl-2-octene-1,8-diol
     相似度:60%
Journal of Agricultural and Food Chemistry          1998          46          1966-1970
(S)-3,7-Dimethyl-5-octene-1,7-diol and Related Oxygenated Monoterpenoids from Petals of Rosa damascena Mill.
Holger Knapp, Markus Straubinger, Selenia Fornari, Noriaki Oka, Naoharu Watanabe, and Peter Winterhalter
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------


9 .     5-(3-Furyl)-2-methyl-1-pentene-3-ol
     相似度:60%
European Journal of Organic Chemistry          1992          1992          279-281
Terpenes and Terpene Derivatives, XXVIII. New Monoterpene Derivatives from the Essential Oil of Artemisia salsoloides
Peter Weyerstahl, Hans-Christian Wahlburg, Vijay K. Kaul and Stanislaw Lochynski
Structure      13C NMR   碳谱模拟图

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10 .     Tolbutamide
     相似度:60%
Applied Microbiology and Biotechnology          2006          72          486-491
Biotransformation of tolbutamide to 4′-hydroxytolbutamide by the fungus Cunninghamella blakesleeana
Haihua Huang, Xiuwei Yang, Qiang Li, Lu Sun, Dafang Zhong
Structure      13C NMR   碳谱模拟图
4楼2013-10-14 10:00:35
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lifeliuyan

至尊木虫 (职业作家)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ...
oyf8888: 金币+60, ★★★很有帮助, 非常感谢!祝您一切顺利! 2013-10-14 10:08:54
查询结果:共查到25个化合物(查询结果仅供参考)  
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1 .     5,6-epoxy-5-isopropyl-6-methyl-hepy-3-in-2-on
C11H16O2     相似度:60%
Helvetica Chimica Acta          1977          60          743-767
Photochemische Reaktionen. 93. Mitteilung. Zur Photochemie konjugierter Epoxy-inone: Die UV.-Bestrahlung von 5,6-Epoxy-5-isopropyl-6-methyl-hept-3-in-2-on
Herbert Eichenberger, Hans Richard Wolf and Oskar Jeger
Structure      13C NMR   碳谱模拟图

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2 .     (Z)-6-hydroxymethyl-2-methylocta-1,6-diene-3,8-diol
C10H18O3     相似度:60%
Australian Journal of Chemistry          1989          42          1983-1993
Tropical Marine-Algae. VI. New Monoterpenes From Several Collections of Chondrococcus hornemannii (Rhodophyta, Gigartinales, Rizophyllidaceae)
JC Coll and AD Wright
Structure      13C NMR   碳谱模拟图

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3 .     compound 8a
     相似度:55.5%
Zeitschrift für Naturforschung B          2007          62          1174-1182
Triethylborane: An "Old" Reagent with New Functions. 1,2-Hydroboration
B. Wrackmeyer, E. Khan, S. Bayer, and K. Shahid
Structure      13C NMR   碳谱模拟图

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4 .     compound
C8H14O     相似度:55.5%
Journal of the American Chemical Society          2004          126          14720-14721
Total Synthesis of Kendomycin:  A Macro−C−Glycosidation Approach
Yu Yuan, Hongbin Men, and Chulbom Lee
Structure      13C NMR   碳谱模拟图

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5 .     compound 21'
C9H18O3     相似度:55.5%
Tetrahedron          2012          68          8994-9003
Enantiodivergent synthesis of (+)- and (−-isolaurepan
Gonzalo Pazos, Manuel Pérez, Zoila Gándara, Generosa Gómez, Yagamare Fall
Structure      13C NMR   碳谱模拟图

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6 .     4-nonyn-1-ol
     相似度:55.5%
Journal of Chemical Ecology          2010          36          923-932
Identification of the Sex Pheromone of a Protected Species, the Spanish Moon Moth Graellsia isabellae
Jocelyn G. Millar, J. Steven McElfresh, Carmen Romero, Marta Vila, Neus Marí-Mena, Carlos Lopez-Vaamonde
Structure      13C NMR   碳谱模拟图

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7 .     4-Isopropyl-2,7-dimethyl-3-oxa-1.4.7-octatrien
C12H20O     相似度:54.5%
Helvetica Chimica Acta          1981          64          198-214
Photochemische Reaktionen. 117. Mitteilung [1] Zur Photochemie von 5,6-Epoxydienen und konjugierten 5,6-Epoxytrienen
Alex Peter Alder, Hans Richard Wolf, Oskar Jeger
Structure      13C NMR   碳谱模拟图

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8 .     7-dodecyn-1-ol
     相似度:54.5%
Journal of Chemical Ecology          2006          32          1085-1099
Isolation, Identification, Synthesis, and Field Evaluation of the Sex Pheromone of the Brazilian Population of Spodoptera frugiperda
Luciane G. Batista-Pereira, Kathrin Stein, André F. de Paula, Jardel A. Moreira, Ivan Cruz, Maria de Lourdes C. Figueiredo, José Perri Jr., Arlene G. Corrêa
Structure      13C NMR   碳谱模拟图

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9 .     masutakic acid A
C10H16O4     相似度:50%
Chemical & Pharmaceutical Bulletin          2001          49(3)          327-329
A Benzofuran Glycoside and an Acetylenic Acid from the Fungus Laetiporus sulphureus var. miniatus
Kazuko YOSHIKAWA, Shinya BANDO,Shigenobu ARIHARA,Eiko MATSUMURA,and Satoshi KATAYAMA
Structure      13C NMR   碳谱模拟图

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10 .     (2R,3R,4R)-5-Chrysanthemen-1,4-diol
C10H18O2     相似度:50%
Journal of Natural Products          2004          67          37-41
Polyoxygenated Eudesmanes and trans-Chrysanthemanes from the Aerial Parts of Santolina insularis
Ernesto Fattorusso, Federico U. Santelia, Giovanni Appendino, Mauro Ballero, and Orazio Taglialatela-Scafati
Structure      13C NMR   碳谱模拟图

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11 .     jatamanin F
C10H16O4     相似度:50%
Journal of Natural Products          2010          73          632-638
Iridoids and Lignans from Valeriana jatamansi
Sheng Lin, Tao Chen, Xiao-Hua Liu, Yun-Heng Shen, Hui-Liang Li, Lei Shan, Run-Hui Liu, Xi-Ke Xu, Wei-Dong Zhang and Hui Wang
Structure      13C NMR   碳谱模拟图

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12 .     2-butyl-5-ethynyltetrahydrofuran(Minor isomer)
C10H16O     相似度:50%
Organic Letters          2007          Vol. 9, No. 10          1975-1978
Ene-yne Tetrahydrofurans from the Sponge Xestospongia muta. Exploiting a Weak CD Effect for Assignment of Configuration
Brandon I. Morinaka, Colin K. Skepper, and Tadeusz F. Molinski
Structure      13C NMR   碳谱模拟图

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13 .     2Z,4E-decadienoic methyl ester
     相似度:50%
Phytochemistry          1988          27          207-212
Diterpenes from the latex of Euphorbia broteri
Julio Gonzàlez Urones,Pilar Basabe Barcala,Ma Josè Sexmero Cuadrado,Isidro Sànchez Marcos
Structure      13C NMR   碳谱模拟图

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14 .     2,2,8,8-tetrahexyl-3,6,9-trioxaundecane-1,11-diol
     相似度:50%
Journal of Heterocyclic Chemistry          2001          38          1259-1264
Synthesis of new proton-ionizable crown ether compounds containing substituted lh-pyridin-4-one subcyclic units
Peter Huszthy, Julia Kertesz, Jerald S. Bradshaw, Reed M. Izatt and J. Ty Redd
Structure      13C NMR   碳谱模拟图

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15 .     (S)-1-((3R,5R,S)-5-Methyl-5-(2-((triisopropylsilyl) oxy)ethyl)-1,2-dioxolan-3-yl)ethane-1,2-diol
C17H36O5Si     相似度:50%
Tetrahedron          2012          68          3717-3724
Exploratory studies toward the synthesis of the peroxylactone unit of plakortolides
Bogdan Barnych, Jean-Michel Vatèle
Structure      13C NMR   碳谱模拟图

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16 .     1-(2'-(1''-hydroxy-1''-methylethyl)thien-3'-ylmethyl)-3,3,4,4-tetramethylsuccinimide
C16H23NO3S     相似度:50%
Heterocycles          2001          54          275-282
Azepine and [1,3]Oxazepine Fused Ring Construction through a Cationic Cyclization: an N-acyliminium Ion Trapping of an Oxygen Atom or Olefin
Aïcha Mamouni, Adam Daïch, Stefan Marchalin, and Bernard Decroix
Structure      13C NMR   碳谱模拟图

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17 .     2-(2-methoxyethoxy)-5-methyl-5-hexen-2-yl hydroperoxide
     相似度:50%
Heterocycles          2000          53          1293-1304
Synthesis of 3-Hydroperoxy (or Hydroxy)-substituted 1,2-Dioxanes and 1,2-Dioxepanes by the Ozonolysis of Unsaturated Hydroperoxy Acetals
Takahiro Tokuyasu, Toyonari Ito, Araki Masuyama, and Masatomo Nojima*
Structure      13C NMR   碳谱模拟图

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18 .     5-isopropenyl-2-methyltetrahydrofuran-2-acetaldehyde
C10H16O2     相似度:50%
Russian Journal of Organic Chemistry          2002          38          1594-1605
Transformations of 6,7-Epoxy Derivatives of Citral and Citronellal in Various Acidic Media
O. I. Yarovaya, O. V. Salomatina, D. V. Korchagina, M. P. Polovinka and V. A. Barkhash
Structure      13C NMR   碳谱模拟图

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19 .     N,5-bis(tert-butyldimethylsilyloxy)pentanamide
C17H39NO3Si2     相似度:50%
European Journal of Organic Chemistry          2011                   2293-2300
Glucosinolate Synthesis: a Hydroxamic Acid Approach
Deimante Cerniauskaite, Jolanta Rousseau, Algirdas Sackus, Patrick Rollin and Arnaud Tatibouët
Structure      13C NMR   碳谱模拟图

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20 .     9-tetradecyn-1-ol
     相似度:50%
Journal of Chemical Ecology          2006          32          1085-1099
Isolation, Identification, Synthesis, and Field Evaluation of the Sex Pheromone of the Brazilian Population of Spodoptera frugiperda
Luciane G. Batista-Pereira, Kathrin Stein, André F. de Paula, Jardel A. Moreira, Ivan Cruz, Maria de Lourdes C. Figueiredo, José Perri Jr., Arlene G. Corrêa
Structure      13C NMR   碳谱模拟图
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