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2、 13C NMR (CDCl3) δ 14.28,15.79,17.35,20.95,22.86,29.86,30.88,31.83,41.68,42.62,56.03,74.11,109.18,112.45,132.26,143.91 |
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liujia1713: 金币+10, ★★★很有帮助, 非常感谢！ 2013-10-12 09:50:19
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liujia1713: 金币+10, ★★★很有帮助, 非常感谢！ 2013-10-12 09:50:19
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????????????? ??????????? ????С??????????????????????????(,)??????磺 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 ?????? ?????? (???????????????趨) ?????? %(?????>=50%) ???????????鵽316????????(???????????ο?) 1 . compund 2b ?????:64.7% Phytochemistry 1988 27 3871-3874 Bisabolones and other constituents of Mikania shushunensis Alicia B. Gutierrez,Werner Herz Structure 13C NMR ??????? 2 . 2-Methoxy-calamenene-14-ol ?????:62.5% Phytochemistry 2009 70 69-74 Phytotoxicity of constituents of glandular trichomes and the leaf surface of camphorweed, Heterotheca subaxillaris Masanori Morimoto , Charles L. Cantrell, Lynn Libous-Bailey , Stephen O. Duke Structure 13C NMR ??????? 3 . (+)-(1S,4R)-7- methoxycalamenene C16H24O ?????:62.5% Phytochemistry 1993 32 117-122 Sesquiterpenes of cadinane type from cultured cells of the liverwort, Heteroscyphus planus Kensuke Nabeta, Kinya Katayama, Shunji Nakagawara, Kenji Katoh Structure 13C NMR ??????? 4 . (+)-(1S,4R)-7-hydroxycalamenene ?????:62.5% Phytochemistry 1993 32 117-122 Sesquiterpenes of cadinane type from cultured cells of the liverwort, Heteroscyphus planus Kensuke Nabeta, Kinya Katayama, Shunji Nakagawara, Kenji Katoh Structure 13C NMR ??????? 5 . 7-hydroxycalamenene C15H22O ?????:62.5% Phytochemistry 1990 29 2329-2331 Sesquiterpenes from Heritiera ornithocephala Richard C. Cambie,Allick R. Lal,Farediah Ahmad Structure 13C NMR ??????? 6 . trans-1-Isopropyl-4-methyl-6-methoxy-1,2,3,4-tetra-hydronaphthalene ?????:62.5% Tetrahedron Letters 2003 44 7641-7644 Stereoselective synthesis of tetralins using cationic cyclisations Ruth Appelbe, Mike Casey, Aideen Dunne, Enrica Pascarella Structure 13C NMR ??????? 7 . (+)-(1S,4R)-trans-methoxycalamenene ?????:62.5% Journal of the Chinese Chemical Society 1999 46 191-195 Isocalamenenes from the Liverwort Bazzania tridens ?????(Ran-Chien Chang);?????(Chia-Li Wu) Structure 13C NMR ??????? 8 . (+)-(1S,4R)-trans-7-hydroxycalamenene ?????:62.5% Journal of the Chinese Chemical Society 1999 46 191-195 Isocalamenenes from the Liverwort Bazzania tridens ?????(Ran-Chien Chang);?????(Chia-Li Wu) Structure 13C NMR ??????? 9 . 4??-hydroxy-5??-ethoxy-epi-cubenol C17H32O3 ?????:58.8% Journal of Natural Products 2002 65 25-28 Five New Cadinane-Type Sesquiterpenes from the Heartwood of Chamaecyparis obtusa var. formosana Yueh-Hsiung Kuo, Chia-Hsien Chen,Shih-Chang Chien, and Yun-Lian Lin Structure 13C NMR ??????? 10 . ent-labd-8??-ol-14-ene ?????:58.8% Phytochemistry 1988 27 2265-2268 Lignans and diterpenes of three Aristolochia species Lucia M.X. Lopes,Vanderlan da S. Bolzani Structure 13C NMR ??????? 11 . 14,15-bisnorlabd-8(17)-ene-6,13-di-one ?????:58.8% Tetrahedron 2006 62 8489-8497 Photodegradation of some 14,15-bisnorlabdene-13-ones, derived from larixol. Synthesis of drimanic dienes with functional groups at C-6 Pavel F. Vlad, Alexandru G. Ciocarlan, Mihai N. Coltsa, Calin Deleanu, Oana Costan, Yurii A. Simonov, Victor Ch. Kravtsov, Janusz Lipkowski, Tadeusz Lis, Aede de Groot Structure 13C NMR ??????? 12 . (1??,4??,5??,10??)-1,4-epoxymuurolan-5-ol C15H26O2, ?????:56.2% Helvetica Chimica Acta 2007 Vol. 90 1514 New Cadinane-Type Sesquiterpenes from the Roots of Taiwania cryptomerioides Hayata Chiou-Fung Chyu, Mei-Ru Ke, Yuan-Shiun Chang, Shih-Chang Chien, and Yueh-Hsiung Kuo Structure 13C NMR ??????? 13 . panaxene ?????:56.2% Phytochemistry 2005 66 2708-2713 Three sesquiterpene hydrocarbons from the roots of Panax ginseng C.A. Meyer (Araliaceae) Rita Richter, Simla Basar, Angelika Koch, Wilfried A. König Structure 13C NMR ??????? 14 . (+)-aristolochene ?????:56.2% Phytochemistry 2002 59 597-602 De novo production of (+)-aristolochene by sporulated surface cultures of Penicillium roqueforti Jan C.R. Demyttenaere, An Adams, Kristof Van Belleghem, Norbert De Kimpe,Wilfried A. König, Alexey V. Tkachev Structure 13C NMR ??????? 15 . 2??,9??-dihydroxyaromadendr-1(10)-ene C15H24O2 ?????:56.2% Phytochemistry 2002 60 475-481 Aromadendrane transformations by Curvularia lunata ATCC 12017 Dwight O. Collins, William F. Reynolds, Paul B. Reese Structure 13C NMR ??????? 16 . (11S)-1??-hydroxyeudesm-4(14)-eno-13,6??-lactone C15H22O3 ?????:56.2% Journal of Natural Products 1999 62 22-30 Guaianolides as Immunomodulators. Synthesis and Biological Activities of Dehydrocostus Lactone, Mokko Lactone, Eremanthin, and Their Derivatives Saori Yuuya, Hisahiro Hagiwara, Toshio Suzuki, Masayoshi Ando, Atsushi Yamada, Kouji Suda, Takao Kataoka, and Kazuo Nagai Structure 13C NMR ??????? |
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