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swordofsea金虫 (初入文坛)
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[求助]
求助一化合物微谱数据结构
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求助一化合物微谱数据结构 求助，我的一个化合物的碳谱数据是100.57,69.7,69.23,68.33,63.88,61.38,60.92,31.44,18.89,13.28，溶剂是D2O 化合物二的碳谱数据是97.22，92.57,77.07,75.18,73.43,72.60,72.28,70.90,70.67,61.55,61.48 溶剂是DMSO 化合物3的碳谱数据是104.60,102.40,98.49,97.31,92.64,83.32,82.32,81.38,71.16,76.31,76.16,75.74,75.26,73.50,72.75,72.37,71.00,70.73,70.32,69.60,68.18,64.72,64.13,63.48,63.41,63.37,61.64,61.51.溶剂是DMSO求助一下，忙着毕业。可以把数据发到我哦邮箱来jxbzyyhp@sina.com |
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lifeliuyan
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
swordofsea: 金币+10, ★★★★★最佳答案 2013-09-28 15:07:19
swordofsea: 金币+5, ★★★★★最佳答案 2013-09-28 15:07:44
swordofsea: 金币+10, ★★★★★最佳答案 2013-09-28 15:07:19
swordofsea: 金币+5, ★★★★★最佳答案 2013-09-28 15:07:44
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化合物3 查询结果：共查到492个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . granatumoside 相似度:80.6% Indian Journal of Chemistry 2006 45B 1681-1685 Phytochemical investigation of the flowers of Punica granatum Ali,M; Sharma,N Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . compound 1a 相似度:71.4% Chemical & Pharmaceutical Bulletin 1998 46 1891-1900 Studies on the Constituents of Clematis Species. VII. Triterpenoid Saponins from the Roots of Clematis terniflora DC. var. robusta TAMURA Yukio KAWATA,Haruhisa KIZU and Tsuyoshi TOMIMORI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . Compound 9 相似度:71.4% Bioorganic & Medicinal Chemistry Letters 1996 6 2841-2846 Solid phase synthesis of polylactosamine oligosaccharide Hiroki Shimizu, Yukishige Ito, Osamu Kanie, Tomoya Ogawa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . polysaccharide B 相似度:68.9% Journal of Asian Natural Products Research 2009 11 951-957 Structural characterization of polysaccharides from the roots of Urtica fissa Yan Li, Yan-Liang Wang, Li Li,Liu Liu, Yu-Xin Lu,Xiao-Chen Cheng and Qing-Lin Zhang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . marubajalapin II C59H98O21 相似度:67.8% Chemical & Pharmaceutical Bulletin 1992 40 3169-3173 Resin Glycosides. XVI. Marubajalapins I-VII, New Ether-Soluble Resin Glycosides from Pharbitis purpurea Masateru ONO,Takashi UEGUCHI,Hiroko MURATA,Toshio KAWASAKI and Kazumoto MIYAHARA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . marubajalapin IV C58H102O21 相似度:67.8% Chemical & Pharmaceutical Bulletin 1992 40 3169-3173 Resin Glycosides. XVI. Marubajalapins I-VII, New Ether-Soluble Resin Glycosides from Pharbitis purpurea Masateru ONO,Takashi UEGUCHI,Hiroko MURATA,Toshio KAWASAKI and Kazumoto MIYAHARA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . marubajalapinVI C60H106O21 相似度:67.8% Chemical & Pharmaceutical Bulletin 1992 40 3169-3173 Resin Glycosides. XVI. Marubajalapins I-VII, New Ether-Soluble Resin Glycosides from Pharbitis purpurea Masateru ONO,Takashi UEGUCHI,Hiroko MURATA,Toshio KAWASAKI and Kazumoto MIYAHARA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . CSP-I 相似度:67.8% Chemical & Pharmaceutical Bulletin 1988 36 2654-2660 Studies on the Structure of a Minor Polysaccharide from the Bark of Melia azadirachta YUMI KUROKAWA,TADAHIRO TAKEDA,YUKIO OGIHARA,MASAKI SHIMIZU and MAKOTO TAKAI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . soyasaponin A5 C52H84O23 相似度:67.8% Chemical & Pharmaceutical Bulletin 1988 36 2829-2839 Saponin and Sapogenol. XLIII. : Acetyl-soyasaponins A4, A5, and A6, New Astringent Bisdesmosides of Soyasapogenol A, from Japanese Soybean, the Seeds of Glycine max MERRILL. TOSHIO TANIYAMA,YOSHIKO NAGAHAMA,MASAYUKI YOSHIKAWA and ISAO KITAGAWA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . compound 5a 相似度:67.8% Chemical & Pharmaceutical Bulletin 1998 46 1891-1900 Studies on the Constituents of Clematis Species. VII. Triterpenoid Saponins from the Roots of Clematis terniflora DC. var. robusta TAMURA Yukio KAWATA,Haruhisa KIZU and Tsuyoshi TOMIMORI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . decaisoside D C52H84O21 相似度:67.8% Phytochemistry 1993 33 427-430 Dammarane triterpenes from Cleome africana Kong Jie, Li Xing-Cong, Wei Bi-Yu, Yang Chong-Ren Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . boholmycin hydrochloride C27H48N4O21 相似度:67.8% The Journal of Antibiotics 1988 41 855-861 BOHOLMYCIN, A NEW AMINOGLYCOSIDE ANTIBIOTIC I. PRODUCTION, ISOLATION AND PROPERTIES KYOICHIRO SAITOH, MITSUAKI TSUNAKAWA, KOJI TOMITA, TAKEO MIYAKI, MASATAKA KONISHI, HIROSHI KAWAGUCHI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . Dephosphorylated polysaccharide 相似度:67.8% Russian Journal of Bioorganic Chemistry 2007 33 57-60 The Structure of the Glycerophosphate-Containing O-Specific Polysaccharide from Escherichia coli O130 A. V. Perepelov, B. Lu, S. N. Senchenkova, S. D. Shevelev, W. Wang, A. S. Shashkov, L. Feng, L. Wang, and Yu. A. Knirel Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . difructosyllactosucrose 相似度:66.6% Magnetic Resonance in Chemistry 2002 40 541-544 NMR analysis of mono-and difructosyllactosucrose synthesized by 1F-fructosyltransferase purified from roots of asparagus (Asparagus officinalis L.) Akira Yamamori, Eri Fukushi, Shuichi Onodera, Jun Kawabata and Norio Shiomi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . glycoside I 相似度:65.5% Chemistry of Natural Compounds 1988 24 193-200 TRITERPENE SAPONINS OF Caltha polypetala.GLYCOSIDES G and I M. M. Vugalter, G. E. Dekanosidze,O. D, Dzhikiya, A. S. Shashkov,and E. P. Kemertelidze Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . desulfated frondoside C C61H100O26 相似度:65.5% Canadian Journal of Chemistry 1998 76 137-141 Frondoside C, a new nonholostane triterpene glycoside from the sea cucumber Cucumaria frondosa: structure and cytotoxicity of its desulfated derivative Sergey A. Avilov, Olga A. Drozdova, Vladimir I. Kalinin, Anatoly I. Kalinovsky,Valentin A. Stonik, Elena N. Gudimova, Ricardo Riguera, and Carlos JimØnez Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . O-β-D-fructofuranosyl-(2→6)-O-β-D-glucopyranosyl-(1→3)-D-glucopyranose 相似度:65.5% Chemistry Central Journal 2009 3 8 Structural analysis of three novel trisaccharides isolated from the fermented beverage of plant extracts Hideki Okada, Eri Fukushi, Akira Yamamori, Naoki Kawazoe, Shuichi Onodera, Jun Kawabata and Norio Shiomi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . AOS-3 相似度:64.2% Journal of Natural Products 2001 64 1174-1178 A Hemicellulose B Fraction from Grape Skin (Vitis vinifera, Palomino Variety) José M. Igartuburu, E. Pando, F. Rodríguez Luis, and Antonio Gil-Serrano Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . coixan B 相似度:64.2% Planta Medica 1986 52 64-65 Isolation and Hypoglycemic Activity of Coixans A, B and C, Glycans of Coix lachryma-jobi var. ma-yuen Seeds Michiko Takahashi, Chohachi Konno and Hiroshi Hikino Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . compound 17 相似度:64.2% Chemical & Pharmaceutical Bulletin 1989 37 42-45 Saponins from Leaves of Acanthopanax senticosus HARMS., Ciwujia. II. : Structures of Ciwujianosides A1, A2, A3, A4 and D6 Chun-Jie SHAO,Ryoji KASAI,Jing-Da XU and Osamu TANAKA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . malonylgypenoside V C57H93NaO25 相似度:64.2% Chemical & Pharmaceutical Bulletin 1989 37 135-139 Dammarane Saponins of Gynostemma pentaphyllum MAKINO and Isolation of Malonylginsenosides-Rb1, -Rd, and Malonylgypenoside V Masaaki KUWABARA,Fumiaki KAWANISHI,Takeya KOMIYA and Haruji OSHIO Structure 13C NMR 碳谱模拟图 |
» 本帖已获得的红花（最新10朵）
swordofsea7楼2013-09-28 14:24:18
lifeliuyan
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2楼2013-09-27 19:51:56
swordofsea
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13.28,18.89,31.44,60.92,61.38,63.88,68.33,69.23,69.70,100.57溶剂是D2O 化合物2：61.48,61.55,70.67,70.90,72.28,72.60,73.43,75.18,77.07,92.57,97.22溶剂是DMSO 化合物3：61.51,61.64,63.37,63.41,63.48,64.13,64.72,68.18,69.60,70.32,70.73,71.00,72.37,72.75,73.50,75.26,75.74,76.16,76.31,77.16,81.38,82.32,83.32,92.64,97.31,98.49,102.40,104.60溶剂是DMSO可以发到我邮箱来jxbzyyhp@sina.com |
3楼2013-09-27 20:05:04
swordofsea
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4楼2013-09-28 12:05:25
lifeliuyan
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
swordofsea: 金币+10, ★★★★★最佳答案 2013-09-28 14:24:38
感谢参与，应助指数 +1
swordofsea: 金币+10, ★★★★★最佳答案 2013-09-28 14:24:38
|
查询结果：共查到138个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . n-butyl-β-D-fructopyranoside C10H20O6 相似度:100% Journal of Shenyang Pharmaceutical University 2008 25 883-885 Chemical constituents of Castanea mollissima LIU Min, ZHANG Dong-song, HUANG Shun-wang, GAO Hui-yuan, WU Li-jun Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . butyl-O-β-D-fructopyranoside 相似度:100% Journal of China Pharmaceutical University 2007 38 21-24 Chemical constituents from Thalictrum fortunei ZHANG Xian-tao; WANG Hao; YIN Zhi-qi; YE Wen-cai; ZHAO Shou-xun Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . n-butyl-β-D-fructopyranoside C10H20O6 相似度:100% Indian Journal of Chemistry 1988 27B 12-16 Chemistry of Ayurvedic Crude Drugs  art VIII-Shatavari-2:Structure Elucidation of Bioacetive Shatavarin-I & other GlycosidesJAYSHREE JOSHI & SUKH DEV Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . n-butyl-O-β-D-fructopyranoside 相似度:90% Acta Pharmaceutica Sinica 2005 Vol 40 533-535 A new flavonoid glycoside from the roots and stems of Sphaerophysa salsula HOU Bai-ling; LI Zhan-lin; LI Xian Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . n-butyl-β-D-fructopyranoside 相似度:90% Chinese Traditional and Herbal Drugs 2009 40 874-876 线叶蓟的化学成分研究 刘学杰;仲英;王姣 Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . n-butyl-β-D-fructopyranoside C10H20O6 相似度:90% Chinese Traditional and Herbal Drugs 2000 31 897-898 植物一内生真菌次生代谢产物的研究(Ⅰ) 于能江,郭顺星 Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 1-butyl-3,4,5-trihydroxy-cyclohexanol 相似度:90% Chinese Traditional and Herbal Drugs 1998 29 1-3 Separation and Identification of Thellungianol from Thellung Pimpinella (Pimpinella thellungiana) Xue Kongfang; Ma Pei(Beijing Institute of Pharmaceutical Industry; Beijing )Wang Jingzun; Wang Lei(Beijing Institute of Microchemistry); Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . n-butyl-β-D-fructopyranoside 相似度:90% Chinese Journal of Natural Medicines 2005 3 86-89 Acetylenes and Flavonoids from Artemisia scopariaⅡ XIE Tao; LIU Jing; LIANG Jing-Yu; ZHANG Zhi-Ming; WEI Xiu-Li Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . n-Butyl-β-D-fructopyranoside 相似度:90% Archives of Pharmacal Research 2010 33 515-521 A new phenylpropane glycoside from the rhizome of Sparganium stoloniferum Seung Young Lee, Sang Un Choi, Jei Hyun Lee, Dong Ung Lee and Kang Ro Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 正丁基-β-D-吡喃果糖苷 相似度:90% Chinese Journal of Medicinal Chemistry 2005 15 217-220 The chemical constituents from Sa ussurea lappa C. B Clarke YIN Hong-quan, QI Xiu-lan, HUA Hui-ming, PEI Yue-hu Structure 13C NMR 碳谱模拟图 |
5楼2013-09-28 14:18:42
lifeliuyan
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【答案】应助回帖
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swordofsea: 金币+10, ★★★★★最佳答案 2013-09-28 14:24:20
swordofsea: 金币+10, ★★★★★最佳答案 2013-09-28 14:24:20
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化合物2 查询结果：共查到387个化合物(查询结果仅供参考) -------------------------------------------------------------------------------- 1 . glucose C6H12O6 相似度:91.6% Chinese Journal of Medicinal Chemistry 2011 21 220-225 Chemical constituents from dried fruits of Rubus chingii XIAO Hong-ming, ZU Ling-bo, LI Shi-ping, WANG Kai-jin, LI Ning* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . 3-azido-3-deoxy-α-D-glucopyranosyl-(1→1')-β-D-glucopyranoside C12H21N3O10 相似度:91.6% Tetrahedron 2013 69 816-825 Synthesis of 3,3′-neotrehalosadiamine and related 1,1′-aminodisaccharides using disarmed, armed, and superarmed building blocks Shazia Anjum, Natasha D. Vetter, Joseph E. Rubin, David R.J. Palmer Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . inotodisaccharide 相似度:91.6% Mycosystema 2010 29 897-910 Metabonomic analysis on production of antioxidant secondary metabolites by two geographically isolated strains of Inonotus obliquus in submerged cultures ZHENG Wei-Fa DAI Yu-Cheng SUN Jing ZHAO Yan-Xia MIAO Kang-Jie PAN Shen-Yuan ZHANG Mei-Mei WEI Jiang-Chun Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . compound 11 相似度:83.3% Chinese Traditional and Herbal Drugs 2010 41 689-692 Chemical constituents from roots of Tinospora sagittata var. yunnanensis CHENG Chun-mei; DAI Yun; HUANG Xiang-zhong; ZHU Yun; DAI Jian-hui; LIU Xiao-fang; WANG Jiong Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . Mixture of α- and β-D-Galactose 相似度:81.8% Phytochemistry 1998 49 1791-1795 Seven imidazole alkaloids from Lepidium sativum Ulrich H. Maier, Heidrun Gundlach, Meinhart H. Zenk Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . α-D-Glucopyranosido-β-D-fructofuranoside C12H22O11 相似度:75% Chemistry of Natural Compounds 2007 43 214-215 CHEMICAL RESEARCH OF Caragana microphylla Seeds Yan Huo, Cheng Guo, Shan Lu,Qiao-Yan Zhang, and Lu-Ping Qin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 6-O-Monoester of Karatavikic acid and Sucrose 相似度:75% Chemistry of Natural Compounds 1996 32 532-534 MODIFICATIONS BASED ON COUMARINS.I. SYNTHESIS OF MONOESTERS OF KARATAVIKIC AND GALBANIC ACIDS WITH SUCROSE A. F. Artamonova, K. A. Nusipbekova, F. S. Nigmat-llina,G. K. Nikonov, and B. Zh. Dzhienbaev Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 6-O-Mouomethyl Ester of Galvanic acid and Sucrose 相似度:75% Chemistry of Natural Compounds 1996 32 532-534 MODIFICATIONS BASED ON COUMARINS.I. SYNTHESIS OF MONOESTERS OF KARATAVIKIC AND GALBANIC ACIDS WITH SUCROSE A. F. Artamonova, K. A. Nusipbekova, F. S. Nigmat-llina,G. K. Nikonov, and B. Zh. Dzhienbaev Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . trans-O-Methylmarmesinic acid C27H38O15 相似度:75% Chemistry of Natural Compounds 1993 29 84-86 SYNTHESIS OF A MONOESTER OF SUCROSE WITH trans-O-METHYLMARMESINIC ACID A. F. Artamonov, F. S. Nigmatullina,and G. K. Nikonov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . Sucrose 相似度:75% Chemistry of Natural Compounds 1993 29 84-86 SYNTHESIS OF A MONOESTER OF SUCROSE WITH trans-O-METHYLMARMESINIC ACID A. F. Artamonov, F. S. Nigmatullina,and G. K. Nikonov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . compound IV 相似度:75% Chemistry of Natural Compounds 1988 24 421-424 SYNTHESIS AND ISOLATION OF MONOESTERS OF SUCROSE AND ARACHIDONIC ACID G. A. Frangulyan, A. V. Komkov, and E. P. Prokof'ev Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . sucrose 相似度:75% China Journal of Chinese Materia Medica 2002 27 361-362 Studies on the Chemical Constituents in Root of Rheum rhizastachyum ZHAO Jun, CHANG Junmin, DU Niansheng Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . sucrose 相似度:75% Acta Pharmaceutica Sinica 2005 Vol 40 994-996 Isolation and structure identification of the chemical constituents from Gypsophila oldhamiana SUN Jing-yong ZHONG Ying ZUO Chun-xu YIN Jun-ting WANG Bin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . Sucrose 相似度:75% Phytochemistry 1993 32 741-745 Sinapic acid esters from Polygala virgata Ahmad Bashir, Matthias Hamburger, Jerome D. Msonthi, Kurt Hostettmann Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . 蔗糖(sucrose) 相似度:75% Chinese Traditional and Herbal Drugs 2011 42(5) 841-843 Chemical constituents in root of Actinidia chinensis CHEN Xiao-xiao, YANG Shang-jun, BAI Shao-yan Structure 13C NMR 碳谱模拟图 |
6楼2013-09-28 14:19:53
swordofsea
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8楼2013-09-28 15:08:34
lifeliuyan
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客气 9楼2013-09-28 15:34:25
swordofsea
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- 性别: GG
- 专业: 中药炮制
10楼2013-10-02 18:30:47