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[求助] XRD 图谱分析江湖救急

江湖救急急急急急急急
在别的实验室做的XRD 分析煤中矿物含量那个老师信誓旦旦的说可以检测的不用处理 5%的误差我就做了可是给我的结果第一次矿物含量居然有50%的我问他这是定量分析！？他说是我说你这不对我灰分分析也就10% 你这太离谱了好吧第二次是少了很多但是我就心里不相信了因为时间很短就出来了差别这么大的结果
想自己分析但是不知道怎么处理只有图谱
各位帮帮我吧

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高手随处可见的环境下修行进行中

1楼 2013-09-09 21:43:05

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引用回帖:

3楼: Originally posted by vampireether at 2013-09-12 07:59:28
你应该把数据贴出来，光看图怎么分析

Lamda = 1.54060
  3.009, 64.991,  0.017
Data Number =    3709
Full Scall  =    1900
3.0094 1863
3.0261 1844
3.0428 1818
3.0595 1791
3.0762 1750
3.0929 1708
3.1096 1659
3.1263 1620
3.1430 1583
3.1598 1558
3.1765 1528
3.1932 1496
3.2099 1480
3.2266 1473
3.2433 1463
3.2600 1458
3.2767 1434
3.2934 1412
3.3102 1390
3.3269 1379
3.3436 1365
3.3603 1351
3.3770 1349
3.3937 1334
3.4104 1339
3.4271 1347
3.4438 1358
3.4606 1359
3.4773 1350
3.4940 1353
3.5107 1346
3.5274 1343
3.5441 1339
3.5608 1329
3.5775 1327
3.5943 1319
3.6110 1322
3.6277 1321
3.6444 1320
3.6611 1306
3.6778 1298
3.6945 1302
3.7112 1296
3.7279 1301
3.7447 1308
3.7614 1311
3.7781 1323
3.7948 1337
3.8115 1338
3.8282 1329
3.8449 1320
3.8616 1313
3.8783 1306
3.8951 1303
3.9118 1302
3.9285 1307
3.9452 1318
3.9619 1330
3.9786 1346
3.9953 1352
4.0120 1352
4.0287 1353
4.0455 1350
4.0622 1348
4.0789 1335
4.0956 1316
4.1123 1312
4.1290 1317
4.1457 1325
4.1624 1326
4.1791 1332
4.1959 1333
4.2126 1333
4.2293 1338
4.2460 1331
4.2627 1326
4.2794 1314
4.2961 1314
4.3128 1316
4.3295 1324
4.3463 1330
4.3630 1328
4.3797 1330
4.3964 1335
4.4131 1329
4.4298 1315
4.4465 1318
4.4632 1318
4.4799 1319
4.4967 1330
4.5134 1335
4.5301 1337
4.5468 1335
4.5635 1326
4.5802 1314
4.5969 1322
4.6136 1308
4.6303 1303
4.6471 1311
4.6638 1300
4.6805 1292
4.6972 1288
4.7139 1287
4.7306 1278
4.7473 1277
4.7640 1288
4.7808 1297
4.7975 1319
4.8142 1320
4.8309 1327
4.8476 1322
4.8643 1303
4.8810 1305
4.8977 1308
4.9144 1313
4.9312 1318
4.9479 1320
4.9646 1331
4.9813 1328
4.9980 1327
5.0147 1320
5.0314 1308
5.0481 1286
5.0648 1269
5.0816 1279
5.0983 1291
5.1150 1307
5.1317 1312
5.1484 1309
5.1651 1308
5.1818 1311
5.1985 1314
5.2152 1314
5.2320 1300
5.2487 1288
5.2654 1277
5.2821 1274
5.2988 1291
5.3155 1291
5.3322 1285
5.3489 1286
5.3656 1285
5.3824 1296
5.3991 1301
5.4158 1302
5.4325 1297
5.4492 1295
5.4659 1280
5.4826 1271
5.4993 1267
5.5160 1239
5.5328 1236
5.5495 1240
5.5662 1229
5.5829 1230
5.5996 1226
5.6163 1224
5.6330 1239
5.6497 1242
5.6664 1249
5.6832 1260
5.6999 1260
5.7166 1265
5.7333 1273
5.7500 1270
5.7667 1259
5.7834 1258
5.8001 1247
5.8168 1246
5.8336 1247
5.8503 1243
5.8670 1253
5.8837 1255
5.9004 1260
5.9171 1265
5.9338 1256
5.9505 1249
5.9673 1246
5.9840 1243
6.0007 1227
6.0174 1228
6.0341 1208
6.0508 1222
6.0675 1229
6.0842 1235
6.1009 1257
6.1177 1266
6.1344 1277
6.1511 1273
6.1678 1271
6.1845 1259
6.2012 1241
6.2179 1230
6.2346 1213
6.2513 1225
6.2681 1222
6.2848 1228
6.3015 1237
6.3182 1237
6.3349 1248
6.3516 1251
6.3683 1255
6.3850 1250
6.4017 1252
6.4185 1243
6.4352 1238
6.4519 1229
6.4686 1224
6.4853 1222
6.5020 1209
6.5187 1197
6.5354 1190
6.5521 1191
6.5689 1188
6.5856 1189
6.6023 1184
6.6190 1178
6.6357 1179
6.6524 1186
6.6691 1194
6.6858 1203
6.7025 1197
6.7193 1194
6.7360 1186
6.7527 1191
6.7694 1193
6.7861 1202
6.8028 1199
6.8195 1217
6.8362 1217
6.8529 1218
6.8697 1206
6.8864 1199
6.9031 1190
6.9198 1189
6.9365 1175
6.9532 1181
6.9699 1186
6.9866 1193
7.0033 1194
7.0201 1201
7.0368 1194
7.0535 1183
7.0702 1165
7.0869 1159
7.1036 1153
7.1203 1150
7.1370 1142
7.1538 1153
7.1705 1158
7.1872 1169
7.2039 1174
7.2206 1183
7.2373 1193
7.2540 1189
7.2707 1187
7.2874 1188
7.3042 1175
7.3209 1163
7.3376 1148
7.3543 1143
7.3710 1138
7.3877 1138
7.4044 1140
7.4211 1146
7.4378 1160
7.4546 1159
7.4713 1166
7.4880 1170
7.5047 1159
7.5214 1154
7.5381 1154
7.5548 1154
7.5715 1146
7.5882 1138
7.6050 1130
7.6217 1137
7.6384 1140
7.6551 1130
7.6718 1133
7.6885 1136
7.7052 1138
7.7219 1147
7.7386 1149
7.7554 1143
7.7721 1129
7.7888 1123
7.8055 1124
7.8222 1127
7.8389 1120
7.8556 1126
7.8723 1132
7.8890 1143
7.9058 1145
7.9225 1143
7.9392 1144
7.9559 1137
7.9726 1126
7.9893 1130
8.0060 1131
8.0227 1131
8.0394 1138
8.0562 1147
8.0729 1142
8.0896 1151
8.1063 1147
8.1230 1146
8.1397 1146
8.1564 1136
8.1731 1122
8.1898 1119
8.2066 1117
8.2233 1117
8.2400 1110
8.2567 1107
8.2734 1102
8.2901 1119
8.3068 1126
8.3235 1133
8.3403 1136
8.3570 1130
8.3737 1132
8.3904 1135
8.4071 1127
8.4238 1113
8.4405 1098
8.4572 1093
8.4739 1091
8.4907 1105
8.5074 1098
8.5241 1099
8.5408 1099
8.5575 1092
8.5742 1102
8.5909 1101
8.6076 1108
8.6243 1107
8.6411 1102
8.6578 1104
8.6745 1115
8.6912 1114
8.7079 1111
8.7246 1115
8.7413 1113
8.7580 1097
8.7747 1101
8.7915 1102
8.8082 1112
8.8249 1109
8.8416 1106
8.8583 1105
8.8750 1108
8.8917 1100
8.9084 1097
8.9251 1086
8.9419 1068
8.9586 1050
8.9753 1051
8.9920 1050
9.0087 1057
9.0254 1067
9.0421 1077
9.0588 1093
9.0755 1106
9.0923 1108
9.1090 1108
9.1257 1103
9.1424 1092
9.1591 1094
9.1758 1093
9.1925 1091
9.2092 1089
9.2259 1088
9.2427 1083
9.2594 1086
9.2761 1078
9.2928 1069
9.3095 1063
9.3262 1055
9.3429 1051
9.3596 1046
9.3763 1052
9.3931 1060
9.4098 1068
9.4265 1072
9.4432 1072
9.4599 1069
9.4766 1072
9.4933 1074
9.5100 1071
9.5268 1061
9.5435 1063
9.5602 1052
9.5769 1055
9.5936 1061
9.6103 1062
9.6270 1062
9.6437 1057
9.6604 1061
9.6772 1067
9.6939 1076
9.7106 1080
9.7273 1077
9.7440 1086
9.7607 1076
9.7774 1071
9.7941 1067
9.8108 1059
9.8276 1056
9.8443 1049
9.8610 1042
9.8777 1032
9.8944 1036
9.9111 1032
9.9278 1034
9.9445 1033
9.9612 1022
9.9780 1020
9.9947 1019
  10.0114 1023
  10.0281 1030
  10.0448 1029
  10.0615 1028
  10.0782 1031
  10.0949 1038
  10.1116 1044
  10.1284 1049
  10.1451 1050
  10.1618 1044
  10.1785 1036
  10.1952 1032
  10.2119 1032
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  10.2620 1030
  10.2788 1033
  10.2955 1051
  10.3122 1070
  10.3289 1072
  10.3456 1080
  10.3623 1069
  10.3790 1054
  10.3957 1050
  10.4124 1034
  10.4292 1020
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  10.4626 1015
  10.4793 1023
  10.4960 1035
  10.5127 1032
  10.5294 1025
  10.5461 1030
  10.5628 1031
  10.5796 1028
  10.5963 1027
  10.6130 1023
  10.6297 1027
  10.6464 1026
  10.6631 1032
  10.6798 1042
  10.6965 1045
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  10.7300 1042
  10.7467 1047
  10.7634 1054
  10.7801 1048
  10.7968 1044
  10.8135 1039
  10.8302 1039
  10.8469 1036
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  10.8804 1039
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  10.9138 1038
  10.9305 1033
  10.9472 1031
  10.9639 1032
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  11.0141 1029
  11.0308 1031
  11.0475 1021
  11.0642 1020
  11.0809 1013
  11.0976 1005
  11.1143 1001
  11.1310 1002
  11.1477 1004
  11.1645 1011
  11.1812 1024
  11.1979 1022
  11.2146 1033
  11.2313 1026
  11.2480 1030
  11.2647 1029
  11.2814 1020
  11.2981 1014
  11.3149 1003
  11.3316 1006
  11.3483 1009
  11.3650 1015
  11.3817 1024
  11.3984 1022
  11.4151 1018
  11.4318 1017
  11.4485 1022
  11.4653 1016
  11.4820 1015
  11.4987 1004
  11.5154    990
  11.5321    994
  11.5488    999
  11.5655 1003
  11.5822 1004
  11.5989 1000
  11.6157 1002
  11.6324 1009
  11.6491 1011
  11.6658 1007
  11.6825 1007
  11.6992 1012
  11.7159 1012
  11.7326 1017
  11.7493 1024
  11.7661 1031
  11.7828 1031
  11.7995 1031
  11.8162 1037
  11.8329 1033
  11.8496 1031
  11.8663 1032
  11.8830 1044
  11.8998 1061
  11.9165 1063
  11.9332 1079
  11.9499 1089
  11.9666 1086
  11.9833 1085
  12.0000 1081
  12.0167 1075
  12.0334 1068
  12.0502 1066
  12.0669 1078
  12.0836 1090
  12.1003 1108
  12.1170 1125
  12.1337 1159
  12.1504 1189
  12.1671 1218
  12.1838 1263
  12.2006 1298
  12.2173 1341
  12.2340 1387
  12.2507 1430
  12.2674 1477
  12.2841 1503
  12.3008 1509
  12.3175 1485
  12.3342 1448
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  12.4011 1169
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  12.6016 1019
  12.6183 1021
  12.6350 1021
  12.6518 1014
  12.6685 1014
  12.6852 1010
  12.7019 1003
  12.7186    993
  12.7353    987
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  13.0027    978
  13.0194    977
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  13.0695 1003
  13.0863 1006
  13.1030    996
  13.1197    993
  13.1364    991
  13.1531    985
  13.1698    985
  13.1865    988
  13.2032    987
  13.2199    986
  13.2367    984
  13.2534    987
  13.2701    993
  13.2868    985
  13.3035    972
  13.3202    974
  13.3369    971
  13.3536    974
  13.3703    987
  13.3871    996
  13.4038 1005
  13.4205 1009
  13.4372 1002
  13.4539 1000
  13.4706    992
  13.4873    973
  13.5040    964
  13.5207    958
  13.5375    953
  13.5542    968
  13.5709    982
  13.5876    985
  13.6043    990
  13.6210    995
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  14.0054    948
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