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[求助] 正相色谱分离克罗米通和羟苯乙酯分不开

最近在做克罗米通乳膏，发现用硅胶柱反式克罗米通与羟苯乙酯峰分不开，调节流动相比例，有时候能分开，但是相同比例流动相继续检测，保留时间不变，两个峰又跑一块儿去了。调流速和柱温都试过，分不开，求解决办法。

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