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huzuyan

新虫 (初入文坛)

[求助] 微谱结构求助-9

13C NMR (101 MHz, MeOD) δ11.84, 12.03, 12.19, 15.58, 18.46, 19.01, 19.22, 19.37, 20.02, 20.42, 20.90, 21.27, 23.24, 24.51, 26.06, 26.59, 28.49, 28.76, 29.29, 29.46, 29.58, 29.67, 29.92, 31.56, 31.76, 32.63, 34.09, 36.05, 36.31, 36.64, 37.13, 37.20, 37.60, 37.70, 39.02, 39.36, 39.75, 41.10, 41.92, 42.20, 42.34, 42.45, 43.13, 46.01, 48.44, 49.62, 55.55, 55.89, 56.15, 65.57, 71.54, 71.64, 73.56, 124.06, 125.64,143.68, 146.46。
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fu_jian2008

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huzuyan: 金币+10, 有帮助, 谢谢帮忙 2013-07-08 14:34:23
1 .     amaroxocane A
C55H85Na3O17S3     相似度:64.9%
Journal of Natural Products          2009          72          259-264
Amaroxocanes A and B: Sulfated Dimeric Sterols Defend the Caribbean Coral Reef Sponge Phorbas amaranthus from Fish Predators
Brandon I. Morinaka, Joseph R. Pawlik, and Tadeusz F. Molinski
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

2 .     fibrosterol sulfate A
C54H84O19S4Na4     相似度:61.4%
The Journal of Organic Chemistry          2009          74          5902-5908
Fibrosterol Sulfates from the Philippine Sponge Lissodendoryx (Acanthodoryx) fibrosa: Sterol Dimers that Inhibit PKCζ
Emily L. Whitson, Tim S. Bugni, Priya S. Chockalingam, Gisela P. Concepcion, Xidong Feng, Guixian Jin, Mary Kay Harper, Gina C. Mangalindan, Leonard A. McDonald and Chris M. Ireland
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

3 .     hamigerol B
C56H85Na5O23S5     相似度:57.8%
Journal of Natural Products          2007          70          1195-1199
Hamigerols A and B, Unprecedented Polysulfate Sterol Dimers from the Mediterranean Sponge Hamigera hamigera
Jie-Fei Cheng, Jong-Soo Lee, Furong Sun, Elizabeth A. Jares-Erijman, Sue Cross, and Kenneth L. Rinehart
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

4 .     fibrosterol Sulfate B
C54H83O22S5Na5     相似度:57.8%
The Journal of Organic Chemistry          2009          74          5902-5908
Fibrosterol Sulfates from the Philippine Sponge Lissodendoryx (Acanthodoryx) fibrosa: Sterol Dimers that Inhibit PKCζ
Emily L. Whitson, Tim S. Bugni, Priya S. Chockalingam, Gisela P. Concepcion, Xidong Feng, Guixian Jin, Mary Kay Harper, Gina C. Mangalindan, Leonard A. McDonald and Chris M. Ireland
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

5 .     fibrosterol Sulfate C
C54H84O19S4Na4     相似度:57.8%
The Journal of Organic Chemistry          2009          74          5902-5908
Fibrosterol Sulfates from the Philippine Sponge Lissodendoryx (Acanthodoryx) fibrosa: Sterol Dimers that Inhibit PKCζ
Emily L. Whitson, Tim S. Bugni, Priya S. Chockalingam, Gisela P. Concepcion, Xidong Feng, Guixian Jin, Mary Kay Harper, Gina C. Mangalindan, Leonard A. McDonald and Chris M. Ireland
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

6 .     crellastatin I
C58H88O11S     相似度:56.8%
Tetrahedron          1999          55          13749-13756
Isolation and structural elucidation of the crellastatins I-M: cytotoxic bis-steroid derivatives from the vanuatu marine sponge Crella sp
Clelia Giannini, Angela Zampella, Cecile Debitus, Jean-Louis Menou, Christos Roussakis, Maria Valeria D'Auria
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

7 .     amaroxocane B
C54H82Na3O20S4     相似度:56.1%
Journal of Natural Products          2009          72          259-264
Amaroxocanes A and B: Sulfated Dimeric Sterols Defend the Caribbean Coral Reef Sponge Phorbas amaranthus from Fish Predators
Brandon I. Morinaka, Joseph R. Pawlik, and Tadeusz F. Molinski
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

8 .     hamigerol A
C56H84Na4O20S4     相似度:56.1%
Journal of Natural Products          2007          70          1195-1199
Hamigerols A and B, Unprecedented Polysulfate Sterol Dimers from the Mediterranean Sponge Hamigera hamigera
Jie-Fei Cheng, Jong-Soo Lee, Furong Sun, Elizabeth A. Jares-Erijman, Sue Cross, and Kenneth L. Rinehart
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

9 .     shishicrellastatin A
C56H83Na3O16S3     相似度:54.3%
Bioorganic & Medicinal Chemistry          2011          19          6594-6598
Shishicrellastatins, inhibitors of cathepsin B, from the marine sponge Crella (Yvesia) spinulata
Shuhei Murayama, Yasufumi Imae, Kentaro Takada, Jo Kikuchi, Yoichi Nakao, Rob W.M. van Soest, Shigeru Okada, Shigeki Matsunaga
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

10 .     shishicrellastatin B
C56H81Na3O16S3     相似度:54.3%
Bioorganic & Medicinal Chemistry          2011          19          6594-6598
Shishicrellastatins, inhibitors of cathepsin B, from the marine sponge Crella (Yvesia) spinulata
Shuhei Murayama, Yasufumi Imae, Kentaro Takada, Jo Kikuchi, Yoichi Nakao, Rob W.M. van Soest, Shigeru Okada, Shigeki Matsunaga
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

11 .     23-(6-Methyl)heptanoic acid demalonylazalomycin F3a ester
C60H105N3O15     相似度:51.6%
Marine Drugs          2013          11          817-829
New Azalomycin F Analogs from Mangrove Streptomyces sp. 211726 with Activity against Microbes and Cancer Cells
Ganjun Yuan, Kui Hong, Haipeng Lin, Zhigang She and Jia Li
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

12 .     H-β3hVal-β3hLys-β3hSer(X)-β3hPhe-β3hGlu-β3hSer(X)-β3hTyr-β3hIle-OH
C58H91N9O14     相似度:50.8%
Helvetica Chimica Acta          2009          92          2643-2658
Synthesis and High-Resolution NMR Structure of a β3-Octapeptide with and without a Tether Introduced by Olefin Metathesis
Marc-Olivier Ebert, James Gardiner, Steven Ballet, Andrew D. Abell, Dieter Seebach
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

13 .     auriculatusaponin F
Cl57H90O25     相似度:50.8%
Journal of Asian Natural Products Research          1998          1          1-14
Triterpenoid Saponins from Aster auriculatus
CHANG ZENG WANG and DE QUAN YU
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

14 .     3-O-β-D-吡喃木糖基-(1→2)-β-D-吡喃葡萄糖醛酸基-3β,21β,22β,23,29-五羟基齐墩果-12-烯-21-O-α-(2,3,4-O-三乙酰基)-L-鼠李糖甙
C53H82O22     相似度:50.8%
Journal of Tropical and Subtropical Botany          1998          6          357-361
马来叉柱花叶中的一个新甜味甙的结构
潘文斗, 票原良枝, 赤羽丈明, 大谷裕之, 日裹亚西
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

15 .     3-O-α-L-rhamnopyranosyl-(1→4)-β-D-galactopyranosyl-(1→3)[β-D-glucopyranosyl-(1→2)]-β-D-glucuronopyranosyl 22-O-angeloylerythrodiol
C59H94O24     相似度:50.8%
Journal of Natural Products          2008          71(5)          918-921
Acylated Triterpenoid Saponins from Schima noronhae and Their Cell Growth Inhibitory Activity
Takashi Ohtsuki, Takashi Miyagawa, Takashi Koyano, Thaworn Kowithayakorn, Nobuo Kawahara, Yukihiro Goda, and Masami Ishibashi
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

16 .     23-Valine demalonylazalomycin F5a ester
C59H104N4O15     相似度:50.8%
Marine Drugs          2013          11          817-829
New Azalomycin F Analogs from Mangrove Streptomyces sp. 211726 with Activity against Microbes and Cancer Cells
Ganjun Yuan, Kui Hong, Haipeng Lin, Zhigang She and Jia Li
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

17 .     dipteroside B
C58H90O22     相似度:50%
Helvetica Chimica Acta          2008          Vol. 91          1728
Triterpenoid Ester Saponins from Dipteronia dyeriana
Rong Guo, Min Luo, Chun-Lin Long, Ma-Lin Li, Zhi-Qin Ouyang, Yi-Ping Zhou, Yue-Hu Wang, Xing-Yu Li, and Ya-Na Shi
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

18 .     dipteroside D
C60H92O22     相似度:50%
Helvetica Chimica Acta          2008          Vol. 91          1728
Triterpenoid Ester Saponins from Dipteronia dyeriana
Rong Guo, Min Luo, Chun-Lin Long, Ma-Lin Li, Zhi-Qin Ouyang, Yi-Ping Zhou, Yue-Hu Wang, Xing-Yu Li, and Ya-Na Shi
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

19 .     malonyl-4,5-dihydroniphimycin
C62H107N3O21     相似度:50%
Zeitschrift für Naturforschung B          2007          62b          1187-1192
Malonyl-4, 5-dihydroniphimycin: A New Polyol Macrolide Antibiotic, Produced by Streptomyces hygroscopicus
Veneta Ivanova, Mariana Kolarova, and Krasja Aleksieva
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

20 .     crellastatin J
C58H88O13S     相似度:50%
Tetrahedron          1999          55          13749-13756
Isolation and structural elucidation of the crellastatins I-M: cytotoxic bis-steroid derivatives from the vanuatu marine sponge Crella sp
Clelia Giannini, Angela Zampella, Cecile Debitus, Jean-Louis Menou, Christos Roussakis, Maria Valeria D'Auria
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

21 .     crellastatin M
C58H88O15S2     相似度:50%
Tetrahedron          1999          55          13749-13756
Isolation and structural elucidation of the crellastatins I-M: cytotoxic bis-steroid derivatives from the vanuatu marine sponge Crella sp
Clelia Giannini, Angela Zampella, Cecile Debitus, Jean-Louis Menou, Christos Roussakis, Maria Valeria D'Auria
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------

22 .     3-O-{β-D-xylopyranosyl-(1→2)-α-L-arabinopyranosyl-(1→6)-2-acetamido-2-deoxy-β-D-glucopyranosyl}echinocystic acid 28-O-{β-D-apiofuranosyl-(1→2)-β-D-xylopyranosyl} ester
C58H93NO25     相似度:50%
Natural Product Communications          2008          3          1763-1770
Triterpenoidal Saponins and Prosapogenins fromAlbizia lebbeck (Leguminosae)
Janelle P. Scott, Winston F. Tinto and William F. Reynolds
Structure      13C NMR   碳谱模拟图

--------------------------------------------------------------------------------


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