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xike123xike

新虫 (初入文坛)

[求助] 新虫求微谱,谢谢了

生物碱类化合物
溶剂:CDCL3+CD3OD(1:1)
碳谱:17.85,27.76,56.03,56.27,56.76,57.59,61.96,110.73,113.87,119.08,120.52,121.26,126.10,130.23,131.35,133.93,136.71,143.36,144.87,147.98,150.34,151.50
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wangkaibo123

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kerry

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【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
xike123xike: 金币+10, ★★★★★最佳答案, 谢谢,很快。。。 2013-06-27 12:23:03
????С??????????????????????????(,)??????磺
21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2

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???????????鵽913????????(???????????ο?)
1 .     dehydrocorydaline
    ?????:100%
Chinese Traditional and Herbal Drugs          2007          38          665-667
???????????о?
????;????
Structure      13C NMR   ???????
2 .     dehydrocorydaline
C22H24NO4     ?????:100%
Journal of the Chinese Chemical Society          1997          44          357-359
Cytotoxic Principles from Saussurea Lappa and Corydalis Turtshaninovii f. Yanhusuo
?????p(Tian-Shung Wu);?????Y(Yann-Lii Leuh);???L??(Chang-Sheng Kuoh);?????(Shwu-Duan Jiang);???鸦(Chieh-Fu Chen);?????(Kuo-Hsiung Lee)
Structure      13C NMR   ???????
3 .     dehydrocorydaline
    ?????:90.9%
China Journal of Chinese Materia Medica          2009          34          1917-1920
Chemical constituents from Corydalis yanhusuo
HU Tiantian, ZHANG Xue, MA Shizhong, CHENG Yiyu, YAO Xinsheng
Structure      13C NMR   ???????
4 .     dehydrocorydaline
    ?????:81.8%
Journal of Asian Natural Products Research          2008          10          1117-1121
Two new protoberberine quaternary alkaloids from Corydalis yanhusuo
Xing-Ye Cheng, Yue Shi, Shun-Liang Zheng, Wen Jin and Hong Sun
Structure      13C NMR   ???????
5 .     palmatine
C21H22NO4     ?????:77.2%
China Journal of Chinese Materia Medica          2008          33          1669-1670
????????????о?
????, ????
Structure      13C NMR   ???????
6 .     11-Hydroxypalmatine
C21H22NO5I     ?????:77.2%
Journal of Asian Natural products Research          2010          12          99-105
Anti-hyperglycemic effect of 11-hydroxypalmatine, a palmatine derivative from Stephania glabra tubers
Deepak Kumar Semwal; Usha Rawat; Ravindra Semwal; Randhir Singh; Gur Jas Preet Singh
Structure      13C NMR   ???????
7 .     palmatine
C21H23NO4     ?????:77.2%
Chinese Journal of Natural Medicines          2007          5          31-34
Chemical Constituents of Corydalis saxicola
WANG Qi-Zhi; LIANG Jing-Yu; YUAN Yue
Structure      13C NMR   ???????
8 .     Dehydrocorydaline
    ?????:77.2%
Journal of China Pharmaceutical University          2002          33          483-486
Alkaloids from Rhizoma corydalis
XU Xiang-Hong; WANG Zheng-Tao; YU Guo-Dian; RUAN Bi-Fang; LI Jun
Structure      13C NMR   ???????
9 .     palmatine
    ?????:77.2%
China Journal of Chinese Materia Medica          2013          38          574-577
Akaloids from roots of Stephania dentifolia
ZUO Ai-xue, LI Li, MA Yun-shu, RAO Gao-xiong
Structure      13C NMR   ???????
10 .     palmatine
    ?????:72.7%
China Journal of Chinese Materia Medica          2005          30          1756-1757
Studies on the alkaloides from herb of Corydalis adunca
ZHAO Dongbao, TANG Yanli, WANG Hanqiang
Structure      13C NMR   ???????
11 .     palmatine
    ?????:72.7%
China Journal of Chinese Materia Medica          2010          35          1272-1275
Alkaloids in stems and leaves of Stephania cepharantha
HE Li; ZHANG Yuanhu; TANG Lijia; SONG Shaohui; SUN Qianyun
Structure      13C NMR   ???????
12 .     2,9,10-trimethoxy-3-ethoxy-5,6-dihydroisoquinolino[2,1-b]isoquinolin-7-ium
C22H24NO4Cl     ?????:72.7%
Bioorganic & Medicinal Chemistry          2012          20          6552-6558
Synthesis and structure?Cactivity relationship of berberine analogues in LDLR up-regulation and AMPK activation
Yan-Xiang Wang, Wei-Jia Kong, Ying-Hong Li, Sheng Tang, Zheng Li, Yang-Biao Li, Yong-Qiang Shan, Chong-Wen Bi, Jian-Dong Jiang, Dan-Qing Song
Structure      13C NMR   ???????
13 .     palmatine
C21H21NO4     ?????:72.7%
Chinese Traditional and Herbal Drugs          2012          43          32-37
Anti-hepatitis virus constituents from Corydalis saxicola
WU Ying-rui; MA Yun-bao; ZHAO You-xing; YAO Shu-ying; ZHOU Jun; GONG Qing-fang; CHEN Ji-jun
Structure      13C NMR   ???????
14 .     palmatine
    ?????:72.7%
Lishizhen Medicine and Materia Medica Research          2009          20          2437-2438
????????????????о?
?????; ??????; ?????; ??????
Structure      13C NMR   ???????
15 .     palmatine
    ?????:72.7%
Lishizhen Medicine and Materia Medica Research          2011          22          327-328
Study on the Alkaloids of Sinomenium acutum
SONG Shao-hui; ZHANG Yuan-hu; HUANG Zhu-yan
Structure      13C NMR   ???????
16 .     13-????????????
    ?????:72.7%
China Journal of Chinese Materia Medica          2012          37          235-237
Chemical constituents from Corydalis yanhusuo
LU Ziming; SUN Wuxing; DUAN Xuhong; YANG Zhiyun; LIU Yadong; TU Pengfei
Structure      13C NMR   ???????
17 .     ?????
    ?????:72.7%
Journal of Chinese Medicinal Materials          2010          33          1881-1883
Study on the Alkaloids in Stepania hernandifolia
TANG Li-jia, GUAN Huan-yu, ZHANG Yuan-hu, HE Li, YANG Xiao-sheng, HAO Xiao-jiang
Structure      13C NMR   ???????
Domyallbesttohaveahappylife.
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