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xike123xike新虫 (初入文坛)
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[求助]
新虫求微谱，谢谢了
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生物碱类化合物 溶剂：CDCL3+CD3OD(1:1) 碳谱：17.85,27.76,56.03,56.27,56.76,57.59,61.96,110.73,113.87,119.08,120.52,121.26,126.10,130.23,131.35,133.93,136.71,143.36,144.87,147.98,150.34,151.50 |
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wangkaibo123
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kerry
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专家经验: +726 - PhEPI: 3
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【答案】应助回帖
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感谢参与，应助指数 +1
xike123xike: 金币+10, ★★★★★最佳答案, 谢谢，很快。。。 2013-06-27 12:23:03
感谢参与，应助指数 +1
xike123xike: 金币+10, ★★★★★最佳答案, 谢谢，很快。。。 2013-06-27 12:23:03
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????С??????????????????????????(,)??????磺 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 ?????? ?????? (???????????????趨) ?????? %(?????>=50%) ???????????鵽913????????(???????????ο?) 1 . dehydrocorydaline ?????:100% Chinese Traditional and Herbal Drugs 2007 38 665-667 ???????????о? ????;???? Structure 13C NMR ??????? 2 . dehydrocorydaline C22H24NO4 ?????:100% Journal of the Chinese Chemical Society 1997 44 357-359 Cytotoxic Principles from Saussurea Lappa and Corydalis Turtshaninovii f. Yanhusuo ?????p(Tian-Shung Wu);?????Y(Yann-Lii Leuh);???L??(Chang-Sheng Kuoh);?????(Shwu-Duan Jiang);???鸦(Chieh-Fu Chen);?????(Kuo-Hsiung Lee) Structure 13C NMR ??????? 3 . dehydrocorydaline ?????:90.9% China Journal of Chinese Materia Medica 2009 34 1917-1920 Chemical constituents from Corydalis yanhusuo HU Tiantian, ZHANG Xue, MA Shizhong, CHENG Yiyu, YAO Xinsheng Structure 13C NMR ??????? 4 . dehydrocorydaline ?????:81.8% Journal of Asian Natural Products Research 2008 10 1117-1121 Two new protoberberine quaternary alkaloids from Corydalis yanhusuo Xing-Ye Cheng, Yue Shi, Shun-Liang Zheng, Wen Jin and Hong Sun Structure 13C NMR ??????? 5 . palmatine C21H22NO4 ?????:77.2% China Journal of Chinese Materia Medica 2008 33 1669-1670 ????????????о? ????, ???? Structure 13C NMR ??????? 6 . 11-Hydroxypalmatine C21H22NO5I ?????:77.2% Journal of Asian Natural products Research 2010 12 99-105 Anti-hyperglycemic effect of 11-hydroxypalmatine, a palmatine derivative from Stephania glabra tubers Deepak Kumar Semwal; Usha Rawat; Ravindra Semwal; Randhir Singh; Gur Jas Preet Singh Structure 13C NMR ??????? 7 . palmatine C21H23NO4 ?????:77.2% Chinese Journal of Natural Medicines 2007 5 31-34 Chemical Constituents of Corydalis saxicola WANG Qi-Zhi; LIANG Jing-Yu; YUAN Yue Structure 13C NMR ??????? 8 . Dehydrocorydaline ?????:77.2% Journal of China Pharmaceutical University 2002 33 483-486 Alkaloids from Rhizoma corydalis XU Xiang-Hong; WANG Zheng-Tao; YU Guo-Dian; RUAN Bi-Fang; LI Jun Structure 13C NMR ??????? 9 . palmatine ?????:77.2% China Journal of Chinese Materia Medica 2013 38 574-577 Akaloids from roots of Stephania dentifolia ZUO Ai-xue, LI Li, MA Yun-shu, RAO Gao-xiong Structure 13C NMR ??????? 10 . palmatine ?????:72.7% China Journal of Chinese Materia Medica 2005 30 1756-1757 Studies on the alkaloides from herb of Corydalis adunca ZHAO Dongbao, TANG Yanli, WANG Hanqiang Structure 13C NMR ??????? 11 . palmatine ?????:72.7% China Journal of Chinese Materia Medica 2010 35 1272-1275 Alkaloids in stems and leaves of Stephania cepharantha HE Li; ZHANG Yuanhu; TANG Lijia; SONG Shaohui; SUN Qianyun Structure 13C NMR ??????? 12 . 2,9,10-trimethoxy-3-ethoxy-5,6-dihydroisoquinolino[2,1-b]isoquinolin-7-ium C22H24NO4Cl ?????:72.7% Bioorganic & Medicinal Chemistry 2012 20 6552-6558 Synthesis and structure?Cactivity relationship of berberine analogues in LDLR up-regulation and AMPK activation Yan-Xiang Wang, Wei-Jia Kong, Ying-Hong Li, Sheng Tang, Zheng Li, Yang-Biao Li, Yong-Qiang Shan, Chong-Wen Bi, Jian-Dong Jiang, Dan-Qing Song Structure 13C NMR ??????? 13 . palmatine C21H21NO4 ?????:72.7% Chinese Traditional and Herbal Drugs 2012 43 32-37 Anti-hepatitis virus constituents from Corydalis saxicola WU Ying-rui; MA Yun-bao; ZHAO You-xing; YAO Shu-ying; ZHOU Jun; GONG Qing-fang; CHEN Ji-jun Structure 13C NMR ??????? 14 . palmatine ?????:72.7% Lishizhen Medicine and Materia Medica Research 2009 20 2437-2438 ????????????????о? ?????; ??????; ?????; ?????? Structure 13C NMR ??????? 15 . palmatine ?????:72.7% Lishizhen Medicine and Materia Medica Research 2011 22 327-328 Study on the Alkaloids of Sinomenium acutum SONG Shao-hui; ZHANG Yuan-hu; HUANG Zhu-yan Structure 13C NMR ??????? 16 . 13-???????????? ?????:72.7% China Journal of Chinese Materia Medica 2012 37 235-237 Chemical constituents from Corydalis yanhusuo LU Ziming; SUN Wuxing; DUAN Xuhong; YANG Zhiyun; LIU Yadong; TU Pengfei Structure 13C NMR ??????? 17 . ????? ?????:72.7% Journal of Chinese Medicinal Materials 2010 33 1881-1883 Study on the Alkaloids in Stepania hernandifolia TANG Li-jia, GUAN Huan-yu, ZHANG Yuan-hu, HE Li, YANG Xiao-sheng, HAO Xiao-jiang Structure 13C NMR ??????? |
2楼2013-06-26 19:07:22