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去学吧银虫 (小有名气)
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[求助]
求助微谱
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MeOD溶解 C信号:14.3,23.5,32.6,34.8,78.6,127.6,153.6,172.5 |
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wangkaibo123
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kerry
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专家经验: +726 - PhEPI: 3
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去学吧: 金币+10, ★★★很有帮助 2013-06-21 17:08:53
感谢参与，应助指数 +1
去学吧: 金币+10, ★★★很有帮助 2013-06-21 17:08:53
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????С??????????????????????????(,)??????磺 21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2 14.3,23.5,32.6,34.8,78.6,127.6,153.6,172.5 ?????? ??? CDCl3 CD3CD2OD CD2Cl2 C5D5N C3D7NO CD3SOCD3 C4D8O (CH3)4Si C4D8O2 CD3COOD C4D8O2 H2O D2O CF3COOD CD3OD ND3 CD3COCD3 C6D6 CD3CN ?????? ?????? (???????????????趨) ?????? %(?????>=50%) ???????????鵽173????????(???????????ο?) -------------------------------------------------------------------------------- 1 . 2,5-dipentadecyl-1,3,4-oxadiazole C32H62ON2 ?????:62.5% Chinese Chemical Letters 2008 19 2010-5-8 One-pot synthesis, antibacterial and antifungal activities of n o ve l 2 ,5 -disubstituted-1,3,4 oxadiazoles Abdul Rauf??Shweta Sharma, Saloni Gangal Structure 13C NMR ??????? -------------------------------------------------------------------------------- 2 . 2,5-diheptadecyl-1,3,4-oxadiazole C36H70ON2 ?????:62.5% Chinese Chemical Letters 2008 19 2010-5-8 One-pot synthesis, antibacterial and antifungal activities of n o ve l 2 ,5 -disubstituted-1,3,4 oxadiazoles Abdul Rauf??Shweta Sharma, Saloni Gangal Structure 13C NMR ??????? -------------------------------------------------------------------------------- 3 . (R)-5-butyltetrahydrofuran-2-ol(Major isomer) C8H16O2 ?????:62.5% Organic Letters 2007 Vol. 9, No. 10 1975-1978 Ene-yne Tetrahydrofurans from the Sponge Xestospongia muta. Exploiting a Weak CD Effect for Assignment of Configuration Brandon I. Morinaka, Colin K. Skepper, and Tadeusz F. Molinski Structure 13C NMR ??????? -------------------------------------------------------------------------------- 4 . (8aS)-7-ethyl-4,7,8a,9-tetrahydro-3H-diimidazo [1,5-a:4',5'-d]pyridine-6,8-dione C10H12N4O2 ?????:62.5% Journal of Heterocyclic Chemistry 2002 39 417-420 Synthesis of 4,7,8a,9-tetrahydro-3H-diimidazo-[1,5-a:4',5'-d]pyridine derivatives Miguel F. Braña, Cristina Guisado, Javier P??rez-Castells and Leticia P??rez-Serrano Structure 13C NMR ??????? -------------------------------------------------------------------------------- 5 . 7,10-dioctanoyldocetaxel ?????:62.5% Bioorganic & Medicinal Chemistry 2000 8 145-156 Effects of the hydrophobicity of taxoids on their interaction with tubulin Daniel Gu??nard, Sylviane Thoret, Joelle Dubois, Marie-Th??r??se Adeline, Qian Wang, Françoise Gu??ritte Structure 13C NMR ??????? -------------------------------------------------------------------------------- 6 . trans-1-bromo-4-octene ?????:62.5% Russian Journal of Organic Chemistry 2003 39 478-485 Ethylation of 2-Alkenyltetrahydrofurans and 2-Alkenyltetrahydropyrans Catalyzed by Titaniun(IV) Isoprpopoxide. Supplement to the Synthesis of Pheromones of Lesser Plum Worm and Tea Leaf Roller Moth E. A. Matyushenkov, D. G. Churikov, N. A. Sokolov and O. G. Kulinkovich Structure 13C NMR ??????? -------------------------------------------------------------------------------- 7 . hexanedioic acid monoethyl ester C8H14O4 ?????:62.5% Journal of Medicinal Chemistry 2007 50 1528-1536 Synthesis and Anti-Cancer Activity of C-Ring-Functionalized Prodigiosin Analogues Jasmine Regourd, Adeeb Al-Sheikh Ali, and Alison Thompson Structure 13C NMR ??????? -------------------------------------------------------------------------------- 8 . compound 6 ?????:62.5% Organic Magnetic Resonance 1983 21 Carbon-13 NMR spectra and the method for their calculation for long-chain polybranched carboxylic acids and their derivatives V. I. Dostovalova, A. B. Terent'ev, N. S. Ikonnikov and R. Kh. Freidlina Structure 13C NMR ??????? -------------------------------------------------------------------------------- 9 . compound 12 ?????:62.5% Organic Magnetic Resonance 1977 9 301-307 Carbon-13 n.m.r. spectra of branched carboxylic acids and their derivatives A. B. Terent'ev, V. I. Dostovalova and R. Kh. Freidlina Structure 13C NMR ??????? -------------------------------------------------------------------------------- 10 . compound 4 C154H258Cl4N4O9 ?????:60% Tetrahedron Letters 2005 46 8845-8848 Calix[8]arene anions: solid state structure of an inclusion compound with a tetrabutylammonium cation Paulina R. Mart??nez-Alanis, Ivan Castillo Structure 13C NMR ??????? -------------------------------------------------------------------------------- 11 . (3S,5S)-3-Azido-5-hexyldihydrofuran-2-one C10H17N3O2 ?????:60% Tetrahedron 2012 68 5396-5405 Stereoselective synthesis of cis- or trans-2,4-disubstituted butyrolactones from Wynberg lactone Ashok Ganta, Julia L. Shamshina, Lauren R. Cafiero, Timothy S. Snowden Structure 13C NMR ??????? -------------------------------------------------------------------------------- 12 . 2-butyl-5-methoxytetrahydrofuran(Major isomer) C9H18O2 ?????:55.5% Organic Letters 2007 Vol. 9, No. 10 1975-1978 Ene-yne Tetrahydrofurans from the Sponge Xestospongia muta. Exploiting a Weak CD Effect for Assignment of Configuration Brandon I. Morinaka, Colin K. Skepper, and Tadeusz F. Molinski Structure 13C NMR ??????? -------------------------------------------------------------------------------- 13 . N-ethyl-3-phenylpropanamide C11H15NO ?????:55.5% Heterocycles 2006 67 629-641 A Convenient Method for the Synthesis of Carboxamides and Thioesters by Using Tetrakis(2-methylimidazol-1-yl)silane Takashi Tozawa, Yoshinobu Yamane, and Teruaki Mukaiyama* Structure 13C NMR ??????? -------------------------------------------------------------------------------- 14 . 7'-Hydroxy-n-octacosanoyl n-decanoate C28H56O3 ?????:55.5% Natural Product Research 2010 24 1059-1068 A new steroidal glycoside and fatty acid esters from the stem bark of Tectona grandis Linn. Zeba Khan; M. Ali; Priyanka Bagri Structure 13C NMR ??????? -------------------------------------------------------------------------------- 15 . 7,10-dinonanoyldocetaxel ?????:55.5% Bioorganic & Medicinal Chemistry 2000 8 145-156 Effects of the hydrophobicity of taxoids on their interaction with tubulin Daniel Gu??nard, Sylviane Thoret, Joelle Dubois, Marie-Th??r??se Adeline, Qian Wang, Françoise Gu??ritte Structure 13C NMR ??????? -------------------------------------------------------------------------------- 16 . (E/Z)-7-Chloro-hept-5-enoic acid dimethylamide C9H16ClNO ?????:55.5% Tetrahedron 2012 68 1177-1184 Cross-metathesis of allyl halides with olefins bearing amide and ester groups Jeong In Yun, Hyoung Rae Kim, Sang Kyum Kim, Deukjoon Kim, Jongkook Lee Structure 13C NMR ??????? -------------------------------------------------------------------------------- 17 . 3-(4'-pentylbiphenyl-4-yl)-1H-pyrazol-5(4H)-one ?????:55.5% Russian Journal of Organic Chemistry 2010 46 1812-1816 Synthesis of new mesogens of the 3-arylisoxazolone and 3-arylpyrazolone series V. N. Kovganko, N. N. Kovganko and M. A. Polovkov Structure 13C NMR ??????? -------------------------------------------------------------------------------- 18 . 4,4a,5,6,7a-tetrahydro-7-methylcyclopenta[c]pyran-3(1H)-one C9H12O2 ?????:55.5% Journal of the Chinese Chemical Society 1997 44 59-63 Total Synthesis of (??)-Patriscabrol and (??)-Boschnialactone ???(Jiun-Yuh Chiu);??????(Chih-Tsao Chiu);?????\(Nein-Chen Chang) Structure 13C NMR ??????? -------------------------------------------------------------------------------- 19 . 5,5-dichloroleucine N-acetyl-methyl ester C9H15NO3Cl2 ?????:55.5% Agricultural and Biological Chemistry 1989 53 505-511 Structure of Amino Acids Isolated from Hydrolyzed HV-Toxin M, a Host-specific Toxin-related Compound Produced by Helminthosporium victoriae Yoshiki KONO, Takeshi KINOSHITA, Setsuo TAKEUCHI, J. M. DALY Structure 13C NMR ??????? -------------------------------------------------------------------------------- 20 . compound 14 ?????:50% Journal of Natural Products 2001 64 572-577 Polychlorinated Acetamides from the Cyanobacterium Microcoleus lyngbyaceus Michael A. Orsini, Lewis K. Pannell, and Karen L. Erickson Structure 13C NMR ??????? -------------------------------------------------------------------------------- 21 . amphorogynine D C8H13NO3 ?????:50% Journal of Natural Products 1998 61 1444-1446 Pyrrolizidine Alkaloids from Amphorogyne spicata Do Thi Thu Huong, Marie-Th??r??se Martin, Marc Litaudon, Thierry S??venet, and Mary Païs Structure 13C NMR ??????? -------------------------------------------------------------------------------- 22 . aminozooanemonin C7H11N3O2 ?????:50% Journal of Natural Products 1998 61 1171-1173 Novel Betaines from the Marine Sponge Agelas dispar Francesco Cafieri, Ernesto Fattorusso, and Orazio Taglialatela-Scafati Structure 13C NMR ??????? -------------------------------------------------------------------------------- 23 . (5S)-decan-5-olide ?????:50% Chemical & Pharmaceutical Bulletin 1990 38 2381-2389 Structure Elucidation of Glycosidic Antibiotics, Glykenins, from Basidiomycetes sp. II. : Absolute Structures of Unusual Polyhydroxylated C26-Fatty Acids, Aglycones of Glykenins Fumiko NISHIDA,Yuji MORI,Naoko ROKKAKU,Sayuri ISOBE,Takeyuki FURUSE,Makoto SUZUKI,Vithaya MEEVOOTISOM,Timothy W. FLEGEL,Yodhathai THEBTARANONTH and Suthum INTARARUANGSORN Structure 13C NMR ??????? -------------------------------------------------------------------------------- 24 . N,N-ditroc-L-2-aminoadipamic acid methyl ester C13H16Cl6N2O7 ?????:50% Chemical & Pharmaceutical Bulletin 1987 35 2994-3001 Chemical Conversion of L-??, ??-Diamino Acids to L-??-Carbamoyl-??-amino Acids by Ruthenium Tetroxide Oxidation SHIGEYUKI YOSHIFUJI,KEN-ICHI TANAKA and YOSHIHIRO NITTA Structure 13C NMR ??????? -------------------------------------------------------------------------------- 25 . 4-Isopropylphenol ?????:50% Chemistry of Natural Compounds 2008 44 450-454 REACTION OF MENTHOL AND PHENOL IN THE PRESENCE OF ALUMINIUM ALKOXIDES I. Yu. Chukicheva, I. V. Fedorova,A. A. Koroleva, and A. V. Kuchin Structure 13C NMR ??????? -------------------------------------------------------------------------------- 26 . alkoxylactol ?????:50% Chemistry of Natural Compounds 2000 36 535-536 SYNTHESIS OF 4 -HYDROXY-6,6-DIMETHYL-3-OXABICYCLO [3.1.0]HEX-2-ONE BY OZONOLYSIS OF (1R, cis)-4,7,7-TRIMETHYL--3-OXABICYCLO[4.1.0]HEPT-4-EN-2-ONE M. I. Kislitsin, O. S. Kukovinets, R. A. Zainullin,F. Z. Galin, M. I. Abdullin, and G. A. Tolstikov Structure 13C NMR ??????? -------------------------------------------------------------------------------- 27 . (4R,6R)-4-(Iodomethyl)-6-pentyl-1,3-dioxan-2-one C10H17IO3 ?????:50% Helvetica Chimica Acta 2009 92 1840-1844 A Stereoselective Total Synthesis of Verbalactone Biswanath Das, Keetha Laxminarayana, Martha Krishnaiah, Duddukuri Nandan Kumar Structure 13C NMR ??????? -------------------------------------------------------------------------------- 28 . Bis(2-phenylethyl)-2,2'-azodiisobutyrate C24H30N2O4 ?????:50% Molecules 2000 5 730-736 Synthesis and Characterization of New Surface Active Azo Initiators for Radical Reactions Milos Sedlak1 and Klaus Tauer2 Structure 13C NMR ??????? -------------------------------------------------------------------------------- 29 . Bis(3-phenylpropyl)-2,2'-azodiisobutyrate C26H34N2O4 ?????:50% Molecules 2000 5 730-736 Synthesis and Characterization of New Surface Active Azo Initiators for Radical Reactions Milos Sedlak1 and Klaus Tauer2 Structure 13C NMR ??????? -------------------------------------------------------------------------------- 30 . (S)-2-Chloro-1-octanol ?????:50% Molecules 2009 14 4275-4283 Preparation of (S)-1-Halo-2-octanols Using Ionic Liquids and Biocatalysts Mireia Orom??-Farr??s, Jordi Eras, N??ria Sala, Merc?? Torres and Ramon Canela Structure 13C NMR ??????? -------------------------------------------------------------------------------- 31 . (S)-2-Bromo-1-octanol ?????:50% Molecules 2009 14 4275-4283 Preparation of (S)-1-Halo-2-octanols Using Ionic Liquids and Biocatalysts Mireia Orom??-Farr??s, Jordi Eras, N??ria Sala, Merc?? Torres and Ramon Canela Structure 13C NMR ??????? -------------------------------------------------------------------------------- 32 . 1-Heptanethiol ?????:50% Molecules 2009 14 4634-4643 3-(2-Aminophenyl)-4-methyl-1, 3-thiazole-2(3H)-thione as an Ecofriendly Sulphur Transfer Agent to Prepare Alkanethiols in High Yield and High Purity Mohammed Amine Mehdid, Ayada Djafri, Christian Roussel and Federico Andreoli Structure 13C NMR ??????? |
2楼2013-06-21 16:56:47