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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
去学吧: 金币+10, ★★★很有帮助 2013-06-21 17:08:53
????С??????????????????????????(,)??????磺
21.4,30.4,37.4,73.2,73.7,125.6,126.6,139.6,140.2,168.2
14.3,23.5,32.6,34.8,78.6,127.6,153.6,172.5
?????? ??? CDCl3 CD3CD2OD CD2Cl2 C5D5N C3D7NO CD3SOCD3 C4D8O (CH3)4Si C4D8O2 CD3COOD C4D8O2 H2O D2O CF3COOD CD3OD ND3 CD3COCD3 C6D6 CD3CN ??????
?????? (???????????????趨)
?????? %(?????>=50%)
???????????鵽173????????(???????????ο?)
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1 . 2,5-dipentadecyl-1,3,4-oxadiazole
C32H62ON2 ?????:62.5%
Chinese Chemical Letters 2008 19 2010-5-8
One-pot synthesis, antibacterial and antifungal activities of n o ve l 2 ,5 -disubstituted-1,3,4 oxadiazoles
Abdul Rauf??Shweta Sharma, Saloni Gangal
Structure 13C NMR ???????
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2 . 2,5-diheptadecyl-1,3,4-oxadiazole
C36H70ON2 ?????:62.5%
Chinese Chemical Letters 2008 19 2010-5-8
One-pot synthesis, antibacterial and antifungal activities of n o ve l 2 ,5 -disubstituted-1,3,4 oxadiazoles
Abdul Rauf??Shweta Sharma, Saloni Gangal
Structure 13C NMR ???????
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3 . (R)-5-butyltetrahydrofuran-2-ol(Major isomer)
C8H16O2 ?????:62.5%
Organic Letters 2007 Vol. 9, No. 10 1975-1978
Ene-yne Tetrahydrofurans from the Sponge Xestospongia muta. Exploiting a Weak CD Effect for Assignment of Configuration
Brandon I. Morinaka, Colin K. Skepper, and Tadeusz F. Molinski
Structure 13C NMR ???????
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4 . (8aS)-7-ethyl-4,7,8a,9-tetrahydro-3H-diimidazo [1,5-a:4',5'-d]pyridine-6,8-dione
C10H12N4O2 ?????:62.5%
Journal of Heterocyclic Chemistry 2002 39 417-420
Synthesis of 4,7,8a,9-tetrahydro-3H-diimidazo-[1,5-a:4',5'-d]pyridine derivatives
Miguel F. Braña, Cristina Guisado, Javier P??rez-Castells and Leticia P??rez-Serrano
Structure 13C NMR ???????
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5 . 7,10-dioctanoyldocetaxel
?????:62.5%
Bioorganic & Medicinal Chemistry 2000 8 145-156
Effects of the hydrophobicity of taxoids on their interaction with tubulin
Daniel Gu??nard, Sylviane Thoret, Joelle Dubois, Marie-Th??r??se Adeline, Qian Wang, Françoise Gu??ritte
Structure 13C NMR ???????
--------------------------------------------------------------------------------
6 . trans-1-bromo-4-octene
?????:62.5%
Russian Journal of Organic Chemistry 2003 39 478-485
Ethylation of 2-Alkenyltetrahydrofurans and 2-Alkenyltetrahydropyrans Catalyzed by Titaniun(IV) Isoprpopoxide. Supplement to the Synthesis of Pheromones of Lesser Plum Worm and Tea Leaf Roller Moth
E. A. Matyushenkov, D. G. Churikov, N. A. Sokolov and O. G. Kulinkovich
Structure 13C NMR ???????
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7 . hexanedioic acid monoethyl ester
C8H14O4 ?????:62.5%
Journal of Medicinal Chemistry 2007 50 1528-1536
Synthesis and Anti-Cancer Activity of C-Ring-Functionalized Prodigiosin Analogues
Jasmine Regourd, Adeeb Al-Sheikh Ali, and Alison Thompson
Structure 13C NMR ???????
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8 . compound 6
?????:62.5%
Organic Magnetic Resonance 1983 21
Carbon-13 NMR spectra and the method for their calculation for long-chain polybranched carboxylic acids and their derivatives
V. I. Dostovalova, A. B. Terent'ev, N. S. Ikonnikov and R. Kh. Freidlina
Structure 13C NMR ???????
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9 . compound 12
?????:62.5%
Organic Magnetic Resonance 1977 9 301-307
Carbon-13 n.m.r. spectra of branched carboxylic acids and their derivatives
A. B. Terent'ev, V. I. Dostovalova and R. Kh. Freidlina
Structure 13C NMR ???????
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10 . compound 4
C154H258Cl4N4O9 ?????:60%
Tetrahedron Letters 2005 46 8845-8848
Calix[8]arene anions: solid state structure of an inclusion compound with a tetrabutylammonium cation
Paulina R. Mart??nez-Alanis, Ivan Castillo
Structure 13C NMR ???????
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11 . (3S,5S)-3-Azido-5-hexyldihydrofuran-2-one
C10H17N3O2 ?????:60%
Tetrahedron 2012 68 5396-5405
Stereoselective synthesis of cis- or trans-2,4-disubstituted butyrolactones from Wynberg lactone
Ashok Ganta, Julia L. Shamshina, Lauren R. Cafiero, Timothy S. Snowden
Structure 13C NMR ???????
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12 . 2-butyl-5-methoxytetrahydrofuran(Major isomer)
C9H18O2 ?????:55.5%
Organic Letters 2007 Vol. 9, No. 10 1975-1978
Ene-yne Tetrahydrofurans from the Sponge Xestospongia muta. Exploiting a Weak CD Effect for Assignment of Configuration
Brandon I. Morinaka, Colin K. Skepper, and Tadeusz F. Molinski
Structure 13C NMR ???????
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13 . N-ethyl-3-phenylpropanamide
C11H15NO ?????:55.5%
Heterocycles 2006 67 629-641
A Convenient Method for the Synthesis of Carboxamides and Thioesters by Using Tetrakis(2-methylimidazol-1-yl)silane
Takashi Tozawa, Yoshinobu Yamane, and Teruaki Mukaiyama*
Structure 13C NMR ???????
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14 . 7'-Hydroxy-n-octacosanoyl n-decanoate
C28H56O3 ?????:55.5%
Natural Product Research 2010 24 1059-1068
A new steroidal glycoside and fatty acid esters from the stem bark of Tectona grandis Linn.
Zeba Khan; M. Ali; Priyanka Bagri
Structure 13C NMR ???????
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15 . 7,10-dinonanoyldocetaxel
?????:55.5%
Bioorganic & Medicinal Chemistry 2000 8 145-156
Effects of the hydrophobicity of taxoids on their interaction with tubulin
Daniel Gu??nard, Sylviane Thoret, Joelle Dubois, Marie-Th??r??se Adeline, Qian Wang, Françoise Gu??ritte
Structure 13C NMR ???????
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16 . (E/Z)-7-Chloro-hept-5-enoic acid dimethylamide
C9H16ClNO ?????:55.5%
Tetrahedron 2012 68 1177-1184
Cross-metathesis of allyl halides with olefins bearing amide and ester groups
Jeong In Yun, Hyoung Rae Kim, Sang Kyum Kim, Deukjoon Kim, Jongkook Lee
Structure 13C NMR ???????
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17 . 3-(4'-pentylbiphenyl-4-yl)-1H-pyrazol-5(4H)-one
?????:55.5%
Russian Journal of Organic Chemistry 2010 46 1812-1816
Synthesis of new mesogens of the 3-arylisoxazolone and 3-arylpyrazolone series
V. N. Kovganko, N. N. Kovganko and M. A. Polovkov
Structure 13C NMR ???????
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18 . 4,4a,5,6,7a-tetrahydro-7-methylcyclopenta[c]pyran-3(1H)-one
C9H12O2 ?????:55.5%
Journal of the Chinese Chemical Society 1997 44 59-63
Total Synthesis of (??)-Patriscabrol and (??)-Boschnialactone
???(Jiun-Yuh Chiu);??????(Chih-Tsao Chiu);?????\(Nein-Chen Chang)
Structure 13C NMR ???????
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19 . 5,5-dichloroleucine N-acetyl-methyl ester
C9H15NO3Cl2 ?????:55.5%
Agricultural and Biological Chemistry 1989 53 505-511
Structure of Amino Acids Isolated from Hydrolyzed HV-Toxin M, a Host-specific Toxin-related Compound Produced by Helminthosporium victoriae
Yoshiki KONO, Takeshi KINOSHITA, Setsuo TAKEUCHI, J. M. DALY
Structure 13C NMR ???????
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20 . compound 14
?????:50%
Journal of Natural Products 2001 64 572-577
Polychlorinated Acetamides from the Cyanobacterium Microcoleus lyngbyaceus
Michael A. Orsini, Lewis K. Pannell, and Karen L. Erickson
Structure 13C NMR ???????
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21 . amphorogynine D
C8H13NO3 ?????:50%
Journal of Natural Products 1998 61 1444-1446
Pyrrolizidine Alkaloids from Amphorogyne spicata
Do Thi Thu Huong, Marie-Th??r??se Martin, Marc Litaudon, Thierry S??venet, and Mary Païs
Structure 13C NMR ???????
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22 . aminozooanemonin
C7H11N3O2 ?????:50%
Journal of Natural Products 1998 61 1171-1173
Novel Betaines from the Marine Sponge Agelas dispar
Francesco Cafieri, Ernesto Fattorusso, and Orazio Taglialatela-Scafati
Structure 13C NMR ???????
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23 . (5S)-decan-5-olide
?????:50%
Chemical & Pharmaceutical Bulletin 1990 38 2381-2389
Structure Elucidation of Glycosidic Antibiotics, Glykenins, from Basidiomycetes sp. II. : Absolute Structures of Unusual Polyhydroxylated C26-Fatty Acids, Aglycones of Glykenins
Fumiko NISHIDA,Yuji MORI,Naoko ROKKAKU,Sayuri ISOBE,Takeyuki FURUSE,Makoto SUZUKI,Vithaya MEEVOOTISOM,Timothy W. FLEGEL,Yodhathai THEBTARANONTH and Suthum INTARARUANGSORN
Structure 13C NMR ???????
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24 . N,N-ditroc-L-2-aminoadipamic acid methyl ester
C13H16Cl6N2O7 ?????:50%
Chemical & Pharmaceutical Bulletin 1987 35 2994-3001
Chemical Conversion of L-??, ??-Diamino Acids to L-??-Carbamoyl-??-amino Acids by Ruthenium Tetroxide Oxidation
SHIGEYUKI YOSHIFUJI,KEN-ICHI TANAKA and YOSHIHIRO NITTA
Structure 13C NMR ???????
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25 . 4-Isopropylphenol
?????:50%
Chemistry of Natural Compounds 2008 44 450-454
REACTION OF MENTHOL AND PHENOL IN THE PRESENCE OF ALUMINIUM ALKOXIDES
I. Yu. Chukicheva, I. V. Fedorova,A. A. Koroleva, and A. V. Kuchin
Structure 13C NMR ???????
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26 . alkoxylactol
?????:50%
Chemistry of Natural Compounds 2000 36 535-536
SYNTHESIS OF 4 -HYDROXY-6,6-DIMETHYL-3-OXABICYCLO [3.1.0]HEX-2-ONE BY OZONOLYSIS OF (1R, cis)-4,7,7-TRIMETHYL--3-OXABICYCLO[4.1.0]HEPT-4-EN-2-ONE
M. I. Kislitsin, O. S. Kukovinets, R. A. Zainullin,F. Z. Galin, M. I. Abdullin, and G. A. Tolstikov
Structure 13C NMR ???????
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27 . (4R,6R)-4-(Iodomethyl)-6-pentyl-1,3-dioxan-2-one
C10H17IO3 ?????:50%
Helvetica Chimica Acta 2009 92 1840-1844
A Stereoselective Total Synthesis of Verbalactone
Biswanath Das, Keetha Laxminarayana, Martha Krishnaiah, Duddukuri Nandan Kumar
Structure 13C NMR ???????
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28 . Bis(2-phenylethyl)-2,2'-azodiisobutyrate
C24H30N2O4 ?????:50%
Molecules 2000 5 730-736
Synthesis and Characterization of New Surface Active Azo Initiators for Radical Reactions
Milos Sedlak1 and Klaus Tauer2
Structure 13C NMR ???????
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29 . Bis(3-phenylpropyl)-2,2'-azodiisobutyrate
C26H34N2O4 ?????:50%
Molecules 2000 5 730-736
Synthesis and Characterization of New Surface Active Azo Initiators for Radical Reactions
Milos Sedlak1 and Klaus Tauer2
Structure 13C NMR ???????
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30 . (S)-2-Chloro-1-octanol
?????:50%
Molecules 2009 14 4275-4283
Preparation of (S)-1-Halo-2-octanols Using Ionic Liquids and Biocatalysts
Mireia Orom??-Farr??s, Jordi Eras, N??ria Sala, Merc?? Torres and Ramon Canela
Structure 13C NMR ???????
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31 . (S)-2-Bromo-1-octanol
?????:50%
Molecules 2009 14 4275-4283
Preparation of (S)-1-Halo-2-octanols Using Ionic Liquids and Biocatalysts
Mireia Orom??-Farr??s, Jordi Eras, N??ria Sala, Merc?? Torres and Ramon Canela
Structure 13C NMR ???????
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32 . 1-Heptanethiol
?????:50%
Molecules 2009 14 4634-4643
3-(2-Aminophenyl)-4-methyl-1, 3-thiazole-2(3H)-thione as an Ecofriendly Sulphur Transfer Agent to Prepare Alkanethiols in High Yield and High Purity
Mohammed Amine Mehdid, Ayada Djafri, Christian Roussel and Federico Andreoli
Structure 13C NMR ??????? |
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重庆大学材料与化工085600，初试370+，求求调剂建议
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