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小木虫论坛-学术科研互动平台 » 生物医药区 » 药学 » 天然药物化学 » 微谱数据求助
北京石油化工学院2026年研究生招生接收调剂公告
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wawlgch

铜虫 (小有名气)

[求助] 微谱数据求助

碳谱数据，溶剂是 CDCl3
18.97,26.41,27.17, 29.69,32.84, 35.30, 41.41, 43.19, 53.16,57.19,57.26, 63.83, 169.44
谢谢各位大侠帮忙啊，急用
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wangwang1989

至尊木虫 (职业作家)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
wawlgch: 金币+10, ★有帮助 2013-06-10 14:56:34
wawlgch(豆哥代发): 金币+5, 谢谢 2013-06-14 08:44:52
1 .     (+)-matrine
    相似度:80%
Chemical & Pharmaceutical Bulletin          1996          44          1951-1953
(-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis
Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
2 .     matrine
    相似度:80%
China Journal of Chinese Materia Medica          2006          31          557-560
Constituents in the alkaloid fraction of Kushen decoction
LIU Bin, SHI Rengbing
Structure      13C NMR   碳谱模拟图
3 .     matrine
    相似度:80%
China Journal of Chinese Materia Medica          1997          22          741-743
Alkaloids in Sophora alopecuroides Seed and Relevant Tests for Activity
Zhang Lanzhen and Li, P J Houghton and S Jackson, P R Twentyman
Structure      13C NMR   碳谱模拟图
4 .     matrine
    相似度:80%
Natural Product Research and Development          2006          18          408-410
Studies on Cytotoxic Constituents from Sophora tonkinensis
DENG Yin-hua; SUN Li; ZHANG Wei; XU Kang-ping; LI Fu-shuang; TAN Jian-bing; CAO Jian-guo; TAN Gui-shan;
Structure      13C NMR   碳谱模拟图
5 .     matrine
C15H25N3O     相似度:80%
Journal of Northwest A&F University (Natural Science)          2012          40          96-102
Synthesis and identification of artificial antigen of matrine
LI Ying, MA Zhi-qing, FENG Jun-tao, ZHANG Xing
Structure      13C NMR   碳谱模拟图
6 .     martrine
    相似度:80%
Natural Medicines          1994          48          180-184
Analysis of Matrine, Matrine N-Oxide and Sophocarpine N-Oxide in Sophora Root "Kushen"
YAMAMOTO KEIICHI,ARIMOTO KEIKO,et al.
Structure      13C NMR   碳谱模拟图
7 .     ( +)-9α-hydroxymatrine
C15H24N2O2     相似度:73.3%
Phytochemistry          1983          22          2069-2072
(+)-9α-Hydroxymatrine from Sophora macrocarpa
Rosa Negrete, Bruce K. Cassels, Gert Eckhardt
Structure      13C NMR   碳谱模拟图
8 .     α-isolupanine
    相似度:66.6%
Journal of Natural Products          1999          62          1385-1389
Detecting Potential Teratogenic Alkaloids from Blue Cohosh Rhizomes Using an in Vitro Rat Embryo Culture
Edward J. Kennelly, Thomas J. Flynn, Eugene P. Mazzola, John A. Roach, Thomas G. McCloud, Darla E. Danford, and Joseph M. Betz
Structure      13C NMR   碳谱模拟图
9 .     (-)-13α-tigloyloxyaphylline
    相似度:66.6%
Pharmazie          1999          54          778-780
Minor lupin alkaloids from the seeds of Lupinus varius and Lupinus hartwegii
M.H. Mohamed - K.M. Mohamed - H.A. Hassanean - S.A. El-Moghazy
Structure      13C NMR   碳谱模拟图
10 .     (±)-norzizanone
    相似度:64.2%
Tetrahedron Letters          2000          41          10353-10356
A stereocontrolled total synthesis of (±)-norzizanone
Lokesh Chandra Pati, Arnab Roy, Debabrata Mukherjee
Structure      13C NMR   碳谱模拟图
11 .     Compound 16
    相似度:61.5%
Bioorganic & Medicinal Chemistry Letters          1993          3          359-362
Enantioselective preparation of novel bicyclo[3.2.0]heptane derivatives using ester hydrolysis catalyzed by novo lipolaseTM
Omar Parve, Anne Pals, Vello Kadarpik, Lilja Lahe, Ülo Lille, Peeter Sikk, Aivar Lóokene and, Toomas Välimäe
Structure      13C NMR   碳谱模拟图
12 .     7-methyl-8-phenyl-1-octanol
    相似度:61.5%
Tetrahedron Letters          2003          44          4451-4454
Preparation of alcohols from sulfones and trialkylboranes
Célia Billaud, Jean-Philippe Goddard, Thierry Le Gall, Charles Mioskowski
Structure      13C NMR   碳谱模拟图
13 .     Butyl N-(6-Aminohexyl)-β-alaninate
    相似度:61.5%
European Journal of Organic Chemistry          2012                   1164-1170
Promiscuous Behavior of Rhizomucor miehei Lipase in the Synthesis of N-Substituted β-Amino Esters
Leandro N. Monsalve, Florencia Gillanders and Alicia Baldessari
Structure      13C NMR   碳谱模拟图
14 .     Octahydro-pyrido[1,2-a]azepin-4-one
C10H17NO     相似度:61.5%
Tetrahedron          2012          68          5547-5553
Reductive transformations of unsaturated azabicyclic nitrolactams
Mihály Viktor Pilipecz, Tamás Róbert Varga, Pál Scheiber, Zoltán Mucsi, Amélie Fàvre-Mourgues, Sándor Boros, László Balázs, Gábor Tóth, Péter Nemes
Structure      13C NMR   碳谱模拟图
15 .     (-)-14β-hydroxymatrine
C15H24N2O2     相似度:60%
Chemical & Pharmaceutical Bulletin          1996          44          1951-1953
(-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis
Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
16 .     (-)-14β-hydroxymatrine
    相似度:60%
Chemical & Pharmaceutical Bulletin          1999          47          448-450
(-)-14β-Acetoxymatrine and (+)-14α-Acetoxymatrine, Two New Matrine-Type Lupin Alkaloids from the Leaves of Sophora tonkinensis
Ping XIAO,Hajime KUBO,Hideaki KOMIYA,Kimio HIGASHIYAMA,Yuning YAN,Jia-shi LI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
17 .     (+)-12-hydroxycedrol
C15H26O2     相似度:60%
Phytochemistry          1995          40          69-72
The in vitro biosynthesis of indole-3-butyric acid in maize
Jutta Ludwig-Müller, Willy Hilgenberg, Ephraim Epstein
Structure      13C NMR   碳谱模拟图
18 .     cedran-8β,12-diol
C15H26O2     相似度:60%
Phytochemistry          1993          33          835-837
Biotransformation of the sesquiterpenoid, cedrol, by Cephalosporium aphidicola
James R. Hanson, Habib Nasir
Structure      13C NMR   碳谱模拟图
19 .     α-isoplupanine
    相似度:60%
Phytochemistry          1991          30          2393-2395
A lupine alkaloid from Leontice leontopetalum
Taleb H. Al-Tel, Salim S. Sabri, Musa H. Abu Zarga, Azra Pervin, Zahir Shah, Atta-ur-Rahman, David S. Rycroft
Structure      13C NMR   碳谱模拟图
20 .     2β-hydroxycaryophyllene oxide
C15H24O2     相似度:60%
Zeitschrift für Naturforschung B          2006          61b          197-200
Biotransformation of (-)-Caryophyllene Oxide by Cell Suspension Culture of Catharanthus roseus
Muhammad Iqbal Choudhary, Zafar A. Siddiqui, Saifullah Khan, Saifullah, Syed G. Musharraf, and Atta-ur-Rahman
Structure      13C NMR   碳谱模拟图
21 .     Oxymatrin
    相似度:60%
Archives of Pharmacal Research          2005          28          190-194
Monoamine oxidase inhibitory components from the roots ofSophora flavescens
Ji-Sang Hwang, Seon A Lee, Seong Su Hong, Kyong Soon Lee and Myung Koo Lee, et al.
Structure      13C NMR   碳谱模拟图
22 .     14β-acetoxymatrine
C17H26N2O3     相似度:58.8%
Chemical & Pharmaceutical Bulletin          1996          44          1951-1953
(-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis
Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
23 .     14α-acetoxymatrine
C17H26N2O3     相似度:58.8%
Chemical & Pharmaceutical Bulletin          1996          44          1951-1953
(-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis
Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
24 .     (-)-14β-acetoxymatrine
C17H26N2O3     相似度:58.8%
Chemical & Pharmaceutical Bulletin          1999          47          448-450
(-)-14β-Acetoxymatrine and (+)-14α-Acetoxymatrine, Two New Matrine-Type Lupin Alkaloids from the Leaves of Sophora tonkinensis
Ping XIAO,Hajime KUBO,Hideaki KOMIYA,Kimio HIGASHIYAMA,Yuning YAN,Jia-shi LI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
25 .     (+)-14α-acetoxymatrine
C17H26N2O3     相似度:58.8%
Chemical & Pharmaceutical Bulletin          1999          47          448-450
(-)-14β-Acetoxymatrine and (+)-14α-Acetoxymatrine, Two New Matrine-Type Lupin Alkaloids from the Leaves of Sophora tonkinensis
Ping XIAO,Hajime KUBO,Hideaki KOMIYA,Kimio HIGASHIYAMA,Yuning YAN,Jia-shi LI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
26 .     (3S,3aS,6S,7R,9aS)-N-(6-hydroxy-1,1,7-trimethyldecahydro-3a,7-methanocyclopentacyclooct-3-yl)acetamide
C17H29NO2     相似度:58.8%
Russian Journal of Organic Chemistry          2004          40          1593-1598
Reactions of caryophyllene, isocaryophyllene, and their epoxy derivatives with acetonitrile under ritter reaction conditions
O. I. Yarovaya, D. V. Korchagina, T. V. Rybalova, Yu. V. Gatilov and M. P. Polovinka, et al.
Structure      13C NMR   碳谱模拟图
27 .     Isomére cis (1aR,3aS,5S,7aS)
C14H20O4     相似度:57.1%
Helvetica Chimica Acta          2001          Vol. 84          2430
Epoxyesters p-menthaniques et pinaniques en milieu basique -Parfum de noix de coco
Marie-Joséphe Bourgeois et Evelyne Montaudon
Structure      13C NMR   碳谱模拟图
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我有一个梦想，我想当校长
2楼2013-06-10 11:31:32
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nkx1979

木虫 (正式写手)
感谢参与，应助指数 +1
豆哥: 应助指数-1, 微谱求助请参考http://emuch.net/bbs/viewthread.php?tid=4896611，一个帖子只能一个应助。 2013-06-14 08:45:27
1 .     (+)-matrine
    相似度:80%
Chemical & Pharmaceutical Bulletin          1996          44          1951-1953
(-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis
Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA
Structure      13C NMR   碳谱模拟图
2 .     matrine
    相似度:80%
China Journal of Chinese Materia Medica          2006          31          557-560
Constituents in the alkaloid fraction of Kushen decoction
LIU Bin, SHI Rengbing
Structure      13C NMR   碳谱模拟图
3 .     matrine
    相似度:80%
China Journal of Chinese Materia Medica          1997          22          741-743
Alkaloids in Sophora alopecuroides Seed and Relevant Tests for Activity
Zhang Lanzhen and Li, P J Houghton and S Jackson, P R Twentyman
Structure      13C NMR   碳谱模拟图
4 .     matrine
    相似度:80%
Natural Product Research and Development          2006          18          408-410
Studies on Cytotoxic Constituents from Sophora tonkinensis
DENG Yin-hua; SUN Li; ZHANG Wei; XU Kang-ping; LI Fu-shuang; TAN Jian-bing; CAO Jian-guo; TAN Gui-shan;
Structure      13C NMR   碳谱模拟图
5 .     matrine
C15H25N3O     相似度:80%
Journal of Northwest A&F University (Natural Science)          2012          40          96-102
Synthesis and identification of artificial antigen of matrine
LI Ying, MA Zhi-qing, FENG Jun-tao, ZHANG Xing
Structure      13C NMR   碳谱模拟图
6 .     martrine
    相似度:80%
Natural Medicines          1994          48          180-184
Analysis of Matrine, Matrine N-Oxide and Sophocarpine N-Oxide in Sophora Root "Kushen"
YAMAMOTO KEIICHI,ARIMOTO KEIKO,et al.
Structure      13C NMR   碳谱模拟图
7 .     ( +)-9α-hydroxymatrine
C15H24N2O2     相似度:73.3%
Phytochemistry          1983          22          2069-2072
(+)-9α-Hydroxymatrine from Sophora macrocarpa
Rosa Negrete, Bruce K. Cassels, Gert Eckhardt
Structure      13C NMR   碳谱模拟图
8 .     α-isolupanine
    相似度:66.6%
Journal of Natural Products          1999          62          1385-1389
Detecting Potential Teratogenic Alkaloids from Blue Cohosh Rhizomes Using an in Vitro Rat Embryo Culture
Edward J. Kennelly, Thomas J. Flynn, Eugene P. Mazzola, John A. Roach, Thomas G. McCloud, Darla E. Danford, and Joseph M. Betz
Structure      13C NMR   碳谱模拟图
9 .     (-)-13α-tigloyloxyaphylline
    相似度:66.6%
Pharmazie          1999          54          778-780
Minor lupin alkaloids from the seeds of Lupinus varius and Lupinus hartwegii
M.H. Mohamed - K.M. Mohamed - H.A. Hassanean - S.A. El-Moghazy
Structure      13C NMR   碳谱模拟图
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天道酬勤
3楼2013-06-11 13:22:39
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