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[求助]
微谱数据求助
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碳谱数据，溶剂是 CDCl3 18.97,26.41,27.17, 29.69,32.84, 35.30, 41.41, 43.19, 53.16,57.19,57.26, 63.83, 169.44 谢谢各位大侠帮忙啊，急用 |
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wangwang1989
至尊木虫 (职业作家)
- 应助: 525 (博士)
- 金币: 11769.2
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- 注册: 2011-10-30
- 专业: 天然药物化学
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
wawlgch: 金币+10, ★有帮助 2013-06-10 14:56:34
wawlgch(豆哥代发): 金币+5, 谢谢 2013-06-14 08:44:52
感谢参与，应助指数 +1
wawlgch: 金币+10, ★有帮助 2013-06-10 14:56:34
wawlgch(豆哥代发): 金币+5, 谢谢 2013-06-14 08:44:52
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1 . (+)-matrine 相似度:80% Chemical & Pharmaceutical Bulletin 1996 44 1951-1953 (-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 2 . matrine 相似度:80% China Journal of Chinese Materia Medica 2006 31 557-560 Constituents in the alkaloid fraction of Kushen decoction LIU Bin, SHI Rengbing Structure 13C NMR 碳谱模拟图 3 . matrine 相似度:80% China Journal of Chinese Materia Medica 1997 22 741-743 Alkaloids in Sophora alopecuroides Seed and Relevant Tests for Activity Zhang Lanzhen and Li, P J Houghton and S Jackson, P R Twentyman Structure 13C NMR 碳谱模拟图 4 . matrine 相似度:80% Natural Product Research and Development 2006 18 408-410 Studies on Cytotoxic Constituents from Sophora tonkinensis DENG Yin-hua; SUN Li; ZHANG Wei; XU Kang-ping; LI Fu-shuang; TAN Jian-bing; CAO Jian-guo; TAN Gui-shan; Structure 13C NMR 碳谱模拟图 5 . matrine C15H25N3O 相似度:80% Journal of Northwest A&F University (Natural Science) 2012 40 96-102 Synthesis and identification of artificial antigen of matrine LI Ying, MA Zhi-qing, FENG Jun-tao, ZHANG Xing Structure 13C NMR 碳谱模拟图 6 . martrine 相似度:80% Natural Medicines 1994 48 180-184 Analysis of Matrine, Matrine N-Oxide and Sophocarpine N-Oxide in Sophora Root "Kushen" YAMAMOTO KEIICHI,ARIMOTO KEIKO,et al. Structure 13C NMR 碳谱模拟图 7 . ( +)-9α-hydroxymatrine C15H24N2O2 相似度:73.3% Phytochemistry 1983 22 2069-2072 (+)-9α-Hydroxymatrine from Sophora macrocarpa Rosa Negrete, Bruce K. Cassels, Gert Eckhardt Structure 13C NMR 碳谱模拟图 8 . α-isolupanine 相似度:66.6% Journal of Natural Products 1999 62 1385-1389 Detecting Potential Teratogenic Alkaloids from Blue Cohosh Rhizomes Using an in Vitro Rat Embryo Culture Edward J. Kennelly, Thomas J. Flynn, Eugene P. Mazzola, John A. Roach, Thomas G. McCloud, Darla E. Danford, and Joseph M. Betz Structure 13C NMR 碳谱模拟图 9 . (-)-13α-tigloyloxyaphylline 相似度:66.6% Pharmazie 1999 54 778-780 Minor lupin alkaloids from the seeds of Lupinus varius and Lupinus hartwegii M.H. Mohamed - K.M. Mohamed - H.A. Hassanean - S.A. El-Moghazy Structure 13C NMR 碳谱模拟图 10 . (±)-norzizanone 相似度:64.2% Tetrahedron Letters 2000 41 10353-10356 A stereocontrolled total synthesis of (±)-norzizanone Lokesh Chandra Pati, Arnab Roy, Debabrata Mukherjee Structure 13C NMR 碳谱模拟图 11 . Compound 16 相似度:61.5% Bioorganic & Medicinal Chemistry Letters 1993 3 359-362 Enantioselective preparation of novel bicyclo[3.2.0]heptane derivatives using ester hydrolysis catalyzed by novo lipolaseTM Omar Parve, Anne Pals, Vello Kadarpik, Lilja Lahe, Ülo Lille, Peeter Sikk, Aivar Lóokene and, Toomas Välimäe Structure 13C NMR 碳谱模拟图 12 . 7-methyl-8-phenyl-1-octanol 相似度:61.5% Tetrahedron Letters 2003 44 4451-4454 Preparation of alcohols from sulfones and trialkylboranes Célia Billaud, Jean-Philippe Goddard, Thierry Le Gall, Charles Mioskowski Structure 13C NMR 碳谱模拟图 13 . Butyl N-(6-Aminohexyl)-β-alaninate 相似度:61.5% European Journal of Organic Chemistry 2012 1164-1170 Promiscuous Behavior of Rhizomucor miehei Lipase in the Synthesis of N-Substituted β-Amino Esters Leandro N. Monsalve, Florencia Gillanders and Alicia Baldessari Structure 13C NMR 碳谱模拟图 14 . Octahydro-pyrido[1,2-a]azepin-4-one C10H17NO 相似度:61.5% Tetrahedron 2012 68 5547-5553 Reductive transformations of unsaturated azabicyclic nitrolactams Mihály Viktor Pilipecz, Tamás Róbert Varga, Pál Scheiber, Zoltán Mucsi, Amélie Fàvre-Mourgues, Sándor Boros, László Balázs, Gábor Tóth, Péter Nemes Structure 13C NMR 碳谱模拟图 15 . (-)-14β-hydroxymatrine C15H24N2O2 相似度:60% Chemical & Pharmaceutical Bulletin 1996 44 1951-1953 (-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 16 . (-)-14β-hydroxymatrine 相似度:60% Chemical & Pharmaceutical Bulletin 1999 47 448-450 (-)-14β-Acetoxymatrine and (+)-14α-Acetoxymatrine, Two New Matrine-Type Lupin Alkaloids from the Leaves of Sophora tonkinensis Ping XIAO,Hajime KUBO,Hideaki KOMIYA,Kimio HIGASHIYAMA,Yuning YAN,Jia-shi LI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 17 . (+)-12-hydroxycedrol C15H26O2 相似度:60% Phytochemistry 1995 40 69-72 The in vitro biosynthesis of indole-3-butyric acid in maize Jutta Ludwig-Müller, Willy Hilgenberg, Ephraim Epstein Structure 13C NMR 碳谱模拟图 18 . cedran-8β,12-diol C15H26O2 相似度:60% Phytochemistry 1993 33 835-837 Biotransformation of the sesquiterpenoid, cedrol, by Cephalosporium aphidicola James R. Hanson, Habib Nasir Structure 13C NMR 碳谱模拟图 19 . α-isoplupanine 相似度:60% Phytochemistry 1991 30 2393-2395 A lupine alkaloid from Leontice leontopetalum Taleb H. Al-Tel, Salim S. Sabri, Musa H. Abu Zarga, Azra Pervin, Zahir Shah, Atta-ur-Rahman, David S. Rycroft Structure 13C NMR 碳谱模拟图 20 . 2β-hydroxycaryophyllene oxide C15H24O2 相似度:60% Zeitschrift für Naturforschung B 2006 61b 197-200 Biotransformation of (-)-Caryophyllene Oxide by Cell Suspension Culture of Catharanthus roseus Muhammad Iqbal Choudhary, Zafar A. Siddiqui, Saifullah Khan, Saifullah, Syed G. Musharraf, and Atta-ur-Rahman Structure 13C NMR 碳谱模拟图 21 . Oxymatrin 相似度:60% Archives of Pharmacal Research 2005 28 190-194 Monoamine oxidase inhibitory components from the roots ofSophora flavescens Ji-Sang Hwang, Seon A Lee, Seong Su Hong, Kyong Soon Lee and Myung Koo Lee, et al. Structure 13C NMR 碳谱模拟图 22 . 14β-acetoxymatrine C17H26N2O3 相似度:58.8% Chemical & Pharmaceutical Bulletin 1996 44 1951-1953 (-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 23 . 14α-acetoxymatrine C17H26N2O3 相似度:58.8% Chemical & Pharmaceutical Bulletin 1996 44 1951-1953 (-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 24 . (-)-14β-acetoxymatrine C17H26N2O3 相似度:58.8% Chemical & Pharmaceutical Bulletin 1999 47 448-450 (-)-14β-Acetoxymatrine and (+)-14α-Acetoxymatrine, Two New Matrine-Type Lupin Alkaloids from the Leaves of Sophora tonkinensis Ping XIAO,Hajime KUBO,Hideaki KOMIYA,Kimio HIGASHIYAMA,Yuning YAN,Jia-shi LI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 25 . (+)-14α-acetoxymatrine C17H26N2O3 相似度:58.8% Chemical & Pharmaceutical Bulletin 1999 47 448-450 (-)-14β-Acetoxymatrine and (+)-14α-Acetoxymatrine, Two New Matrine-Type Lupin Alkaloids from the Leaves of Sophora tonkinensis Ping XIAO,Hajime KUBO,Hideaki KOMIYA,Kimio HIGASHIYAMA,Yuning YAN,Jia-shi LI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 26 . (3S,3aS,6S,7R,9aS)-N-(6-hydroxy-1,1,7-trimethyldecahydro-3a,7-methanocyclopentacyclooct-3-yl)acetamide C17H29NO2 相似度:58.8% Russian Journal of Organic Chemistry 2004 40 1593-1598 Reactions of caryophyllene, isocaryophyllene, and their epoxy derivatives with acetonitrile under ritter reaction conditions O. I. Yarovaya, D. V. Korchagina, T. V. Rybalova, Yu. V. Gatilov and M. P. Polovinka, et al. Structure 13C NMR 碳谱模拟图 27 . Isomére cis (1aR,3aS,5S,7aS) C14H20O4 相似度:57.1% Helvetica Chimica Acta 2001 Vol. 84 2430 Epoxyesters p-menthaniques et pinaniques en milieu basique -Parfum de noix de coco Marie-Joséphe Bourgeois et Evelyne Montaudon Structure 13C NMR 碳谱模拟图 |
2楼2013-06-10 11:31:32
感谢参与，应助指数 +1
豆哥: 应助指数-1, 微谱求助请参考http://emuch.net/bbs/viewthread.php?tid=4896611，一个帖子只能一个应助。 2013-06-14 08:45:27
豆哥: 应助指数-1, 微谱求助请参考http://emuch.net/bbs/viewthread.php?tid=4896611，一个帖子只能一个应助。 2013-06-14 08:45:27
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1 . (+)-matrine 相似度:80% Chemical & Pharmaceutical Bulletin 1996 44 1951-1953 (-)-14β-Hydroxymatrine, a New Lupine Alkaloid from the Roots of Sophora tonkinensis Ping XIAO,Jiashi LI,Hajime KUBO,Kazuki SAITO,Isamu MURAKOSHI and Shigeru OHMIYA Structure 13C NMR 碳谱模拟图 2 . matrine 相似度:80% China Journal of Chinese Materia Medica 2006 31 557-560 Constituents in the alkaloid fraction of Kushen decoction LIU Bin, SHI Rengbing Structure 13C NMR 碳谱模拟图 3 . matrine 相似度:80% China Journal of Chinese Materia Medica 1997 22 741-743 Alkaloids in Sophora alopecuroides Seed and Relevant Tests for Activity Zhang Lanzhen and Li, P J Houghton and S Jackson, P R Twentyman Structure 13C NMR 碳谱模拟图 4 . matrine 相似度:80% Natural Product Research and Development 2006 18 408-410 Studies on Cytotoxic Constituents from Sophora tonkinensis DENG Yin-hua; SUN Li; ZHANG Wei; XU Kang-ping; LI Fu-shuang; TAN Jian-bing; CAO Jian-guo; TAN Gui-shan; Structure 13C NMR 碳谱模拟图 5 . matrine C15H25N3O 相似度:80% Journal of Northwest A&F University (Natural Science) 2012 40 96-102 Synthesis and identification of artificial antigen of matrine LI Ying, MA Zhi-qing, FENG Jun-tao, ZHANG Xing Structure 13C NMR 碳谱模拟图 6 . martrine 相似度:80% Natural Medicines 1994 48 180-184 Analysis of Matrine, Matrine N-Oxide and Sophocarpine N-Oxide in Sophora Root "Kushen" YAMAMOTO KEIICHI,ARIMOTO KEIKO,et al. Structure 13C NMR 碳谱模拟图 7 . ( +)-9α-hydroxymatrine C15H24N2O2 相似度:73.3% Phytochemistry 1983 22 2069-2072 (+)-9α-Hydroxymatrine from Sophora macrocarpa Rosa Negrete, Bruce K. Cassels, Gert Eckhardt Structure 13C NMR 碳谱模拟图 8 . α-isolupanine 相似度:66.6% Journal of Natural Products 1999 62 1385-1389 Detecting Potential Teratogenic Alkaloids from Blue Cohosh Rhizomes Using an in Vitro Rat Embryo Culture Edward J. Kennelly, Thomas J. Flynn, Eugene P. Mazzola, John A. Roach, Thomas G. McCloud, Darla E. Danford, and Joseph M. Betz Structure 13C NMR 碳谱模拟图 9 . (-)-13α-tigloyloxyaphylline 相似度:66.6% Pharmazie 1999 54 778-780 Minor lupin alkaloids from the seeds of Lupinus varius and Lupinus hartwegii M.H. Mohamed - K.M. Mohamed - H.A. Hassanean - S.A. El-Moghazy Structure 13C NMR 碳谱模拟图 |
3楼2013-06-11 13:22:39