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求助微谱数据1个
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化合物 溶剂：DMSO NMR：100HZ 碳谱数据 53.6,60.3,61.2,61.3,61.4,61.5,67.3,68.8,70.6,70.7,72.2,72.5,72.9,73.3,73.9,75.8, 76.9,92.6,99.2,101.8 |
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fu_jian2008
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【答案】应助回帖
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ygw198781: 金币+10, ★★★很有帮助 2013-05-30 15:16:51
感谢参与，应助指数 +1
ygw198781: 金币+10, ★★★很有帮助 2013-05-30 15:16:51
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compound 6 相似度:75% Organic letters 2001 3 3265-3268 Chemoenzymatic Iterative Synthesis of Difficult Linkages of Oligosaccharides on Soluble Polymeric Supports Fengyang Yan, Michel Gilbert, Warren W. Wakarchuk, Jean-Robert Brisson, and Dennis M. Whitfield Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . compound 4 相似度:75% Organic Magnetic Resonance 1984 22 109-113 1H and 13C chemical shift data of four peracetylated triglucoses. Application of two-dimensional techniques P. Bigler, W. Ammann and R. Richarz Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . Galactomannan 相似度:70% Chemistry of Natural Compounds 2009 45 297-299 POLYSACCHARIDES OF Fabaceae. II. GALACTOMANNANFROM Astragalus danicus SEEDS D. N. Olennikov1 and A. V. Rokhin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . GMM 相似度:70% Chemistry of Natural Compounds 1999 35 498-501 GALACTOMANNANS FROM TWO SPECIES OF Gleditsia STUDIED BY 13C NMR R. K. Rakhmanberdyeva, I M. R. Mirzaeva,"D. A. Rakhimov, I and N. D. Abdullaev I Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . β-D-吡喃葡萄糖基-(1→6)-β-D-吡喃葡萄糖基(1→4)2β2D2吡喃葡萄糖 相似度:70% Chinese Pharmaceutical Journal 2003 38 836-838 Studies on chemical constituents of Lysimachia davurica TIAN Jing kui, ZOU Zhong mei, XU Li zhen, Liu Jian xin, ZHANG Hong wu, YANG Shi lin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . D-(+)-raffinose 相似度:70% Chinese Pharmaceutical Journal 2007 42 337-338 Studies on Chemical Constituents of Lysionotus pauciflorus FENG Wei-sheng, LI Qian, ZHENG Xiao-ke Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . compound 6 相似度:69.5% Chemical & Pharmaceutical Bulletin 1987 35 3948-3951 AN ANTIFEEDANT FOR THE YELLOW BUTTERFLY LARVAE IN CAMELLIA JAPONICA : A REVISED STRUCTURE OF CAMELLIDIN II Atsushi Numata,Akihiko Kitajima,Takako Katsuno,Kyoko Yamamoto,Natsu Nagahama,Chika Takahashi,Ryoko Fujiki and Michiko Nabae Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 2'-fucosyllactose C18H32O15 相似度:69.5% Heterocycles 2012 84 637-655 Synthesis of Human Milk Oligosaccharides: 2'- and 3'-Fucosyllactose Claney L. Pereira and Frank E. McDonald* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . boholmycin hydrochloride C27H48N4O21 相似度:68% The Journal of Antibiotics 1988 41 855-861 BOHOLMYCIN, A NEW AMINOGLYCOSIDE ANTIBIOTIC I. PRODUCTION, ISOLATION AND PROPERTIES KYOICHIRO SAITOH, MITSUAKI TSUNAKAWA, KOJI TOMITA, TAKEO MIYAKI, MASATAKA KONISHI, HIROSHI KAWAGUCHI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . compound 2a 相似度:66.6% Chemical & Pharmaceutical Bulletin 1990 38 2381-2389 Structure Elucidation of Glycosidic Antibiotics, Glykenins, from Basidiomycetes sp. II. : Absolute Structures of Unusual Polyhydroxylated C26-Fatty Acids, Aglycones of Glykenins Fumiko NISHIDA,Yuji MORI,Naoko ROKKAKU,Sayuri ISOBE,Takeyuki FURUSE,Makoto SUZUKI,Vithaya MEEVOOTISOM,Timothy W. FLEGEL,Yodhathai THEBTARANONTH and Suthum INTARARUANGSORN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . compound 2b 相似度:66.6% Chemical & Pharmaceutical Bulletin 1990 38 2381-2389 Structure Elucidation of Glycosidic Antibiotics, Glykenins, from Basidiomycetes sp. II. : Absolute Structures of Unusual Polyhydroxylated C26-Fatty Acids, Aglycones of Glykenins Fumiko NISHIDA,Yuji MORI,Naoko ROKKAKU,Sayuri ISOBE,Takeyuki FURUSE,Makoto SUZUKI,Vithaya MEEVOOTISOM,Timothy W. FLEGEL,Yodhathai THEBTARANONTH and Suthum INTARARUANGSORN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . rehmannioside B 相似度:66.6% Phytochemistry 1982 21 133-138 Iridoid glycosides of Rehmannia glutinosa Haruji Oshio, Hiroyuki Inouye Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 2,3-HHDP-D-glucose 相似度:66.6% Chinese Traditional and Herbal Drugs 1999 30(9) 645-648 桃金娘中的黄酮苷和一种逆没食子丹宁 候爱君,刘延泽,吴养洁 Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . 4-O-[4-O-(β-D-Galactopyranosyl)-β-D-galactopyranosyl]-D-glucopyranose C18H32O16 相似度:65.2% Journal of the Chemical Society, Perkin Transactions 1 1996 1921-1926 Glycosidase-catalysed oligosaccharide synthesis of di-, tri- and tetra-saccharides using the N-acetylhexosaminidase from Aspergillus oryzae and the β-galactosidase from Bacillus circulans Suddham Singh, Michaela Scigelova, Gabin Vic and David H. G. Crout Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . compound 13 相似度:65% Chemical & Pharmaceutical Bulletin 1992 40 1404-1410 Marine Natural Products. XXIX. Heterosigma-glycolipids I, II, III, and IV, Four Diacylglyceroglycolipids Possessing ω3-Polyunsaturated Fatty Acid Residues, from the Raphidopycean Dinoflagellate Heterosigma akashiwo Motomasa KOBAYASHI,Kozo HAYASHI,Kazuyoshi KAWAZOE and Isao KITAGAWA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . GMT 相似度:65% Chemistry of Natural Compounds 1999 35 498-501 GALACTOMANNANS FROM TWO SPECIES OF Gleditsia STUDIED BY 13C NMR R. K. Rakhmanberdyeva, I M. R. Mirzaeva,"D. A. Rakhimov, I and N. D. Abdullaev I Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . compound 1 相似度:65% Organic letters 2001 3 747-750 A New Phenoxyacetate-Based Linker System for the Solid-Phase Synthesis of Oligosaccharides Xiangyang Wu, Matthias Grathwohl, and Richard R. Schmidt Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . Compound 4 相似度:65% Bioorganic & Medicinal Chemistry Letters 2000 10 365-368 A novel thermophilic Glycosynthase that effects branching glycosylation A. Trincone, G. Perugino, M. Rossi, M. Moracci Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . Compound 5 相似度:65% Bioorganic & Medicinal Chemistry Letters 2000 10 365-368 A novel thermophilic Glycosynthase that effects branching glycosylation A. Trincone, G. Perugino, M. Rossi, M. Moracci Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . lactosucrose {O-β-D-fructofuranosyl-(2→1)-O-[β-D-galactopyranosyl-(1→4)]-α-D-glucopyranoside} C18H32O16 相似度:65% Magnetic Resonance in Chemistry 2002 40 541-544 NMR analysis of mono-and difructosyllactosucrose synthesized by 1F-fructosyltransferase purified from roots of asparagus (Asparagus officinalis L.) Akira Yamamori, Eri Fukushi, Shuichi Onodera, Jun Kawabata and Norio Shiomi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . compound Px 相似度:65% Phytochemistry 2010 71 1095-1103 Metabolism of galactosyl-oligosaccharides in Stellaria media – Discovery of stellariose synthase, a novel type of galactosyltransferase Mieke Vanhaecke, Natalia Dyubankova, Eveline Lescrinier, Wim Van den Ende Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . β-D-fructofuranosyl-(2→1)-β-D-fructofuranosyl-(21)-α-D-glucopyranoside 相似度:65% Natural Product Sciences 2010 16 20-25 Isolation of Phenolics, Nucleosides, Saccharides and an Alkaloid from the root of Aralia cordata Hyun, Sook-Kyung; Jung, Hyun-Ah; Min, Byung-Sun; Jung, Jee-H.; Choi, Jae-Sue Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . 3,4-α-D-diglucosyl-2-phosphoryl ribitol 相似度:65% Bioscience, Biotechnology, and Biochemistry 2009 73 530-535 Structures of Two Monomeric Units of Teichoic Acid Prepared from the Cell Wall of Lactobacillus plantarum NRIC 1068 Satoru TOMITA, Kazuo FURIHATA, Tomoo NUKADA, Eiichi SATOH, Tai UCHIMURA and Sanae OKADA Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . saccharide 相似度:65% Bioscience, Biotechnology, and Biochemistry 2010 74 2130-2132 Synthesis of β-D-Fructopyranosyl-(2→6)-D-glucopyranose from D-Glucose and D-Fructose by a Thermal Treatment Akira YAMAMORI, Hideki OKADA, Naoki KAWAZOE, Shuichi ONODERA and Norio SHIOMI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . compound 2 相似度:65% Organic Magnetic Resonance 1984 22 109-113 1H and 13C chemical shift data of four peracetylated triglucoses. Application of two-dimensional techniques P. Bigler, W. Ammann and R. Richarz Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . Methyl [β-D-glucopyranosyl-(1→4)-β-(1-thio-△5,5a carbaglucopyranosyl)-(1→4)-β-(α-D-glucopyranoside)] C20H34O14S 相似度:65% Bioorganic & Medicinal Chemistry 2011 19 3812-3830 Syntheses of cellotriose and cellotetraose analogues as transition state mimics for mechanistic studies of cellulases Shogo Noguchi, Shintaro Takemoto, Shun-ichi Kidokoro, Kazunori Yamamoto, Masaru Hashimoto Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 27 . Methyl β-D-glucopyranosyl-(1→4)-β-D-glucopyranosyl-(1→4)-α-D-4-thioglucopyranoside C19H34O15S 相似度:65% Bioorganic & Medicinal Chemistry 2011 19 3812-3830 Syntheses of cellotriose and cellotetraose analogues as transition state mimics for mechanistic studies of cellulases Shogo Noguchi, Shintaro Takemoto, Shun-ichi Kidokoro, Kazunori Yamamoto, Masaru Hashimoto Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 28 . 2-(trimethylsilyl)ethyl 4,6-O-[(R)-1-methoxycarbonylethylidene]-β-D-galactopyranosyl-(1→4)-β-D-mannopyranosyl-(1→4)-β-D-galactopyranoside C26H48O18Si 相似度:64% Indian Journal of Chemistry 2005 44B 137-140 Synthesis of (R)-4,6-O-pyruvated trisaccharide related to the repeating unit of the antigen from Shigella dysenteriae type 9 in the form of its 2-(trimethylsilyl)ethyl glycoside Roy,Samarpita; Sarkar,Sujit Kumar; Roy,Nirmolendu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 29 . Methyl α-D-mannopyranosyl-(1 → 3)-α-D-manno-pyranosyl-(1→ 3)-α-D-mannopyranosyl-(1→ 3)-α-D-manno-pyranoside C25H45O21 相似度:62.5% Bioorganic & Medicinal Chemistry 2008 16 699-709 Synthesis and heparanase inhibitory activity of sulfatedmannooligosaccharides related to the antiangiogenic agent PI-88 Jon K. Fairweather, Edward Hammond, Ken D. Johnstone and Vito Ferro Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 30 . compound 2c 相似度:61.9% Chemical & Pharmaceutical Bulletin 1990 38 2381-2389 Structure Elucidation of Glycosidic Antibiotics, Glykenins, from Basidiomycetes sp. II. : Absolute Structures of Unusual Polyhydroxylated C26-Fatty Acids, Aglycones of Glykenins Fumiko NISHIDA,Yuji MORI,Naoko ROKKAKU,Sayuri ISOBE,Takeyuki FURUSE,Makoto SUZUKI,Vithaya MEEVOOTISOM,Timothy W. FLEGEL,Yodhathai THEBTARANONTH and Suthum INTARARUANGSORN Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 31 . compound 5 相似度:61.9% Chemical & Pharmaceutical Bulletin 1985 33 3473-3478 Studies on the Constituents of Hedera rhombea BEAN. IV. On the Hederagenin Glycosides. (2) HARUHISA KIZU,SATOSHI HIRABAYASHI,MIZUMI SUZUKI and TSUYOSHI TOMIMORI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 32 . hederagenin-28-α-L-rhamnopyranosyl-(1→4 )-β-D-glucopyranosyl-(1→6 )-β-D-glucopyranosylester 相似度:61.9% Acta Botanica Sinica 1994 36 75-79 Triterpene Glycosides In The Leaves of Acanthopanax giraldii Cheng Dong-liang, Shao Yu and Yang Li Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 33 . allobetonicoside 相似度:61.9% Natural Product Research 2006 20 648-652 Monoterpenoids from Stachys glutinosa L . Anna Maria Serrilli; Alessia Ramunno; Francesco Piccioni; Mauro Serafini; Mauro Ballero; Armandodoriano Bianco Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 34 . allosyl-epoxydecaloside C21H32O15 相似度:61.9% Journal of Natural Products 1980 Vol 43 649-707 Iridoids. A Review Leticia J. El-Naggar, Jack L. Beal Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 35 . α-L-rhamno-pyranosyl(1→4)-O-β-D-glucopyranosyl(1→6)-β-D-glucopyranose 1α-epimer 相似度:61.9% Phytochemistry 1991 30 3717-3720 A bidesmosidic triterpenoid saponin fromSchefflera octophylla T.V. Sung, J. Peter-Katalinic, G. Adam Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 36 . allosyl-epoxydecaloside C21H32O15 相似度:61.9% Phytochemistry 1981 20 71-83 Iridoid mono- and di-glycosides in Mentzelia Søren Rosendal Jensen, Carl Bjarne Mikkelsen, Bent Juhl Nielsen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 37 . Methyl 2-acetamido-2-deoxy-3-O-α-L-fucopyranosyl)-4-O-(2-acetamido-2-deoxy-β-D-galactopyranosyl)-β-D-glucopyranoside C23H40N2O15 相似度:61.9% Bioorganic & Medicinal Chemistry 1996 4 1989-2001 Synthesis and conformational studies of the tyvelose capped, Lewis-x like tetrasaccharide epitope of Trichinella spiralis Jian Zhang, Albin Otter, David R. Bundle Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 38 . melittoside nonaacetate 相似度:60.8% Natural Product Research 2007 21 692-697 A novel iridoid glycoside from the aerial parts of the Tunisian Prasium majus Saoussen Hammami; Hichem Ben Jannet; Maria Letizia Ciavatta; Guido Cimino; Zine Mighri Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 39 . pedicularioside F nonaacetate 相似度:60.8% Phytochemistry 1992 31 263-266 Phenylpropanoid and iridoid glycosides from Pedicularis lasiophrys Jia Zhongjian, Liu Zimin, Wang Changzeng Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 40 . O-(2,3,5-tri-O-acetyl-α-L-arabinofuranosyl)-(1→4)-[2,3,4,6-tetra-O-acetyl-β-D-glucopyranosyl-(1→3)]-2-O-acetyl-α-L-rhamnopyranosyl-(1→2)-3,4,6-tri-O-acetyl-α-D-glucopyranose C45H63O30 相似度:60.8% Heterocycles 2000 52 775-798 Synthesis of Neosaponins Carrying Oligosaccharides from Natural Products Tsuyoshi Ikeda, Junei Kinjo, Tetsuya Kajimoto, and Toshihiro Nohara* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 41 . SSG 相似度:60% Chemical & Pharmaceutical Bulletin 1990 38 1745-1747 Further Examination on the Structure of an Alkali-SOluble Glucan Isolated from Omphalia lapidescens : Studies on Fungal Polysaccharide. XXXVI Kazuo SAITO,Motohiro NISHIJIMA and Toshio MIYAZAKI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 42 . glycoside E C44H70O16 相似度:60% Chemical & Pharmaceutical Bulletin 1983 31 1980-1990 Comparative Studies on the Constituents of Ophiopogonis Tuber and Its Congeners. I. Studies of the Constituents of the Subterranean Part of Liriope platyphylla WANG et TANG. (1) YOSHIAKI WATANABE,SHUICHI SANADA,YOSHITERU IDA and JUNZO SHOJI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 43 . PLWH-2' 相似度:60% Chemistry of Natural Compounds 2009 45 864-866 Lamiaceae CARBOHYDRATES.VII. GLUCOARABINOGALACTAN FROM Panzerina lanata D. N. Olennikov A. V. Nazarova,A. V. Rokhin,L. M. Tankhaeva,and T. V. Kornopol′tseva Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 44 . ASGM-D 相似度:60% Chemistry of Natural Compounds 2008 44 685-687 POLYSACCHARIDES OF Fabaceae. I. GALACTOMANNAN OF Astragalus sericeocanus SEEDS D. N. Olennikov and A. V. Rokhin Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 45 . 6'-O-Triphenylmethylmelezitose C37H46O16 相似度:60% Chemistry of Natural Compounds 2001 37 397-401 SYNTHESIS OF MELEZITOSE DERIVATIVES L. Tsao, Kh. Dou, G. Sun' , and Yu. Lyu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 46 . decaisoside A C47H76O16 相似度:60% Phytochemistry 1993 33 427-430 Dammarane triterpenes from Cleome africana Kong Jie, Li Xing-Cong, Wei Bi-Yu, Yang Chong-Ren Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 47 . β-D-Galactopyranosyl-(1→4)-β-L-fucopyranosyl-(1→6)-1-deoxy-1-azido-D-mannitol C18H33O14N3 相似度:60% Chemical & Pharmaceutical Bulletin 2011 59(10) 1307-1310 Synthesis of New Galβ1→4Fuc Segments Useful for Biological Investigations Kazusa NISHIYAMA, Atsushi YAMADA, Tomoharu TAKEUCHI, Yoichiro ARATA, Ken-ichi KASAI, Tetsuta OSHITARI, Hideaki NATSUGARI, and Hideyo TAKAHASHI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 48 . Compound 4 相似度:60% Bioorganic & Medicinal Chemistry Letters 1999 9 35-38 Chemical and enzymatic synthesis of glycoconjugates 5: One-pot regioselective synthesis of bioactive galactobiosides using a CLONEZYMETM thermophilic glycosidase library Jun Li, Dan E. Robertson, Jay M. Short, Peng George Wang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 49 . 3-((2S,3R,4R,5S,6R)-3,4-dihydroxy-6-(hydroxymethyl)-5-((2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)tetrahydro-2H-pyran-2-yloxy)tetrahydro-2H-pyran-2-yloxy)-1-(4H-imidazo[4,5-c][1,2,5]oxadiazol-5-yl)pentane-1,2,4,5-tetraol C20H32N4O16 相似度:60% Molecules 2010 15 1340-1353 I2-Catalyzed Oxidative Condensation of Aldoses with Diamines: Synthesis of Aldo-Naphthimidazoles for Carbohydrate Analysis Chunchi Lin, Wei-Ting Hung, Chien-Yuan Kuo, Kuo-Shiang Liao, Yin-Chen Liu and Wen-Bin Yang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 50 . faralatroside-PA 相似度:60% Phytochemistry 1981 20 1113-1116 Faralatroside and faratroside, two flavonol triglycosides from Colubrina faralaotra Hélène Guinaudeau, Otto Seligmann, Hildebert Wagner, Andras Neszmelyi Structure 13C NMR 碳谱模拟图 |
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