24小时热门版块排行榜    

查看: 202  |  回复: 7
当前主题已经存档。
【悬赏金币】回答本帖问题,作者huoyingfei将赠送您 2 个金币
当前只显示满足指定条件的回帖,点击这里查看本话题的所有回帖

huoyingfei

铜虫 (小有名气)

[求助] 液氮.操作

请各位大虾帮帮我.

In a 50 ml three-necked flask with the
middle neck connected to a dry ice cold-finger condenser,  The flask was flushed with N, for
15 min before NH3,(g) was introduced via the one neck and NH3,(l) allowed to
condense on the cold finger. About 15 ml of liquid ammonia were condensed
(- 77°C). The solution was stirred for 30 min with a magnetic stirrer and the NH,
then allowed to evaporate (about 1 h) by removing the dry ice from the condenser.
谁做过这方面的试验,帮我看看怎么做,我新手,不知道该怎么做.关键是a dry ice cold-finger condenser,是什么,还有 NH3,(l) allowed to
condense on the cold finger. About 15 ml of liquid ammonia were condensed
(- 77°C). 多谢了

» 猜你喜欢

人类一思考,上帝就发笑! 让上帝笑去吧
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

yuxinghai455

银虫 (正式写手)

In a 50 ml three-necked flask with the
middle neck connected to a dry ice cold-finger condenser  在50ml三颈瓶中间颈口连接干冰冷凝器。
NH3,(l) allowed to condense on the cold finger.液氨可通过干冰冷凝器冷凝。
About 15 ml of liquid ammonia were condensed(- 77°C).
反应需要15ml左右的被冷却的液氨。
3楼2007-10-06 13:16:05
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
查看全部 8 个回答

huoyingfei

铜虫 (小有名气)

不好意思,是液氨,不是液氮.

不好意思.是液氨的操作,
人类一思考,上帝就发笑! 让上帝笑去吧
2楼2007-10-06 12:27:59
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

mooncakexzj

荣誉版主 (文坛精英)

优秀区长优秀区长优秀版主优秀版主

In a 50 ml three-necked flask with the middle neck connected to a dry ice cold-finger condenser  在50ml三颈瓶中间颈口连接干冰冷凝器。The flask was flushed with N, for 15 min before NH3,(g) was introduced via the one neck,在氨气通入以前,三口瓶应该通入氮气15分钟(应该是赶走空气)and NH3,(l) allowed to condense on the cold finger.液氨可通过干冰冷凝器冷凝。About 15 ml of liquid ammonia were condensed(- 77°C). 反应需要15ml左右的被冷却的液氨。
海上生明月,天涯共此时!
4楼2007-10-06 14:09:47
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖

huoyingfei

铜虫 (小有名气)

干冰冷凝器?

干冰冷凝器是什么?可以买到么?是不是在指型冷凝器上加个降温的装置.
谢谢!
人类一思考,上帝就发笑! 让上帝笑去吧
5楼2007-10-06 18:36:57
已阅   回复此楼   关注TA 给TA发消息 送TA红花 TA的回帖
不应助 确定回帖应助 (注意:应助才可能被奖励,但不允许灌水,必须填写15个字符以上)
最具人气热帖推荐 [查看全部] 作者 回/看 最后发表
[考研] 环境学硕288求调剂 +8 皮皮皮123456 2026-03-22 8/400 2026-03-23 23:47 by 热情沙漠
[考研] 306求0703调剂一志愿华中师范 +7 纸鱼ly 2026-03-21 8/400 2026-03-23 23:31 by chixmc
[考研] 上海电力大学材料防护与新材料重点实验室招收调剂研究生(材料、化学、电化学,环境) +3 我爱学电池 2026-03-23 3/150 2026-03-23 17:16 by AZMK
[考研] 307求调剂 +3 余意卿 2026-03-21 3/150 2026-03-23 10:32 by Iveryant
[考研] 寻找调剂 +4 倔强芒? 2026-03-21 4/200 2026-03-22 16:14 by 木托莫露露
[考研] 一志愿中南化学(0703)总分337求调剂 +9 niko- 2026-03-19 10/500 2026-03-22 16:08 by ColorlessPI
[考研] 289求调剂 +7 怀瑾握瑜l 2026-03-20 7/350 2026-03-22 15:57 by ColorlessPI
[考研] 0856材料专硕353求调剂 +4 NIFFFfff 2026-03-20 4/200 2026-03-22 09:49 by 2026paper
[考研] 一志愿华中科技大学071000,求调剂 +4 沿岸有贝壳6 2026-03-21 4/200 2026-03-22 07:21 by ilovexiaobin
[考研] 0805 316求调剂 +3 大雪深藏 2026-03-18 3/150 2026-03-21 18:55 by 学员8dgXkO
[考研] 材料工程专硕 348分求调剂 +3 冬辞. 2026-03-17 5/250 2026-03-21 18:47 by 学员8dgXkO
[考研] 0703化学调剂 +4 妮妮ninicgb 2026-03-21 4/200 2026-03-21 18:39 by 学员8dgXkO
[考研] 299求调剂 +5 shxchem 2026-03-20 7/350 2026-03-21 17:09 by ColorlessPI
[考研] 268求调剂 +9 简单点0 2026-03-17 9/450 2026-03-21 15:37 by lature00
[考研] 一志愿天津大学化学工艺专业(081702)315分求调剂 +12 yangfz 2026-03-17 12/600 2026-03-21 03:30 by JourneyLucky
[考研] 332求调剂 +4 ydfyh 2026-03-17 4/200 2026-03-21 02:20 by JourneyLucky
[考研] 一志愿武理材料305分求调剂 +6 想上岸的鲤鱼 2026-03-18 7/350 2026-03-21 01:03 by JourneyLucky
[考研] 330求调剂 +4 小材化本科 2026-03-18 4/200 2026-03-20 23:13 by JourneyLucky
[考研] 生物学调剂招人!!! +3 山海天岚 2026-03-17 4/200 2026-03-19 21:34 by 怎么释怀
[考研] 考研调剂 +3 淇ya_~ 2026-03-17 5/250 2026-03-17 09:25 by Winj1e
信息提示
请填处理意见