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追索晨曦

新虫 (初入文坛)

[求助] 微谱 求助 !!急求!!!

碳谱数据如下,溶剂氘代甲醇
13.047,16.9538,19.4481,22.3268,29.3467,56.9077,60.1323  
谢谢各位了~~!!
还有一个C谱,溶剂氘代甲醇
数据 10.0081,12.6535,13.0060,18.8553,22.6298,23.5403,28.7298,29.3669,30.2134,30.3078,38.7617,60.1544,62.6233,65.2549,67.6865,128.4613,130.9656,132.1733,167.9419
谢谢各位了~~!! 急求这二个化合物~

[ Last edited by 追索晨曦 on 2013-5-15 at 23:22 ]
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wm0629

铁杆木虫 (著名写手)

【答案】应助回帖

★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与,应助指数 +1
追索晨曦: 金币+20, ★★★★★最佳答案, 谢谢啊~ 2013-05-16 08:36:01
化合物1:

查询结果:共查到5个化合物(查询结果仅供参考)
1 .     3-oxo-3-(pentylamino)propanoic acid
    相似度:57.1%
Journal of Medicinal Chemistry          1990          33          2465-2476
7-Oxabicyclo[2.2.1]heptyl carboxylic acids as thromboxane A2 antagonists: aza .omega.-chain analogs
Masami Nakane, Joyce A. Reid, Wen Ching Han, Jagabandhu Das, Vu Chi Truc, Martin F. Haslanger, Dianne Garber, Don N. Harris, Anders Hedberg,
Structure      13C NMR   碳谱模拟图
2 .     seco-((S)-Pro-(R)-Val)
    相似度:50%
Helvetica Chimica Acta          2009          92          1112-1117
Proline-Containing Dipeptides from a Marine Sponge of a Callyspongia Species
Bin Yang, Junde Dong, Xuefeng Zhou, Xianwen Yang, Kyung Jin Lee, Lishu Wang, Si Zhang, Yonghong Liu
Structure      13C NMR   碳谱模拟图
3 .     Cyclo-(Pro-Val)
    相似度:50%
Chemistry of Natural Compounds          2010          46          828-830
Secondary metabolites from green algae Ulva pertusa
Chang-Yun Wang, Lei Han, Kai Kang, Chang-Lun Shao and Yu-Xi Wei, et al.
Structure      13C NMR   碳谱模拟图
4 .     cyclo(Val-Pro)
    相似度:50%
Natural Product Research and Development          2006          18          405-407
Studies on the Chemical Constituents and Antitumor Activity of Secondary Metabolites of Marine-derived Streptomyces sp. 3275
ZHAO Wen-ying;Zhu Tian-jiao; GU Jing-yan; GU Qian-qun *; ZHU Wei-ming
Structure      13C NMR   碳谱模拟图
5 .     N-(4-Nitrobenzyl)-dipropyl amine
    相似度:50%
Bioorganic & Medicinal Chemistry          1999          7          1145-1150
A comparison of flexible and constrained haptens in eliciting antibody catalysts for paraoxon hydrolysis
David A. Spivak, Timothy Z. Hoffman, Alisa H. Moore, Matthew J. Taylor, Kim D. Janda
Structure      13C NMR   碳谱模拟图

化合物2:
查询结果:共查到4个化合物(查询结果仅供参考)
1 .     compound 3
C21H26N2O5     相似度:57.1%
Tetrahedron          1999          55          1457-1468
Structure and biomimetic, electrochemically-mediated semisynthesis of the novel pentacyclic indole danuphylline
Toh-Seok Kam, Tuck-Meng Lim, Yeun-Mun Choo
Structure      13C NMR   碳谱模拟图
2 .     9β-hydroxydarutigenol
C20H34O4     相似度:50%
Journal of Natural Products          2009          72          2005-2008
ent-Pimarane Diterpenoids from Siegesbeckia orientalis and Structure Revision of a Related Compound
Fei Wang, Xue-Lian Cheng, Ya-Ju Li, Song Shi, and Ji-Kai Liu
Structure      13C NMR   碳谱模拟图
3 .     ICM0301 C
C24H35O3Cl     相似度:50%
The Journal of Antibiotics          2004          57          104-109
ICM0301s, New Angiogenesis Inhibitors from Aspergillus sp. F-1491 II. Physico-chemical Properties and Structure Elucidation
TETSUYA SOMENO,HIROYUKI KUMAGAI,SHUN-ICHI OHBA,MASAHIDE AMEMIYA,HIROSHI NAGANAWA,MASAAKI ISHIZUKA and DAISHIRO IKEDA
Structure      13C NMR   碳谱模拟图
4 .     3α-hydroxy-3β,19-epoxy-6-aza-5-pregnen-20-one
C20H29NO3     相似度:50%
Steroids          2013          78          34-37
Synthesis of 6-azaprogesterone and 19-hydroxy-6-azasteroids
Mario D. Martínez, Valeria C. Edelsztein, Fernando J. Durán, Pablo H. Di Chenna, Gerardo Burton
Structure      13C NMR   碳谱模拟图
艰难困苦,玉汝于成。
2楼2013-05-16 07:39:57
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