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guigui2011

新虫 (初入文坛)

[求助] 微谱求助一个化合物结构,特急

13C NMR (101 MHz, CDCl3) δ
166.75,156.20,151.63,147.24,141.17,140.23,135.11,129.80,129.42,125.71,120.96,120.31,117.89,117.56,115.19,69.01,64.57,63.17,53.43,30.90,20.85,16.81
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jasminelw

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【答案】应助回帖

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guigui2011: 金币+10, 有帮助 2013-05-01 22:42:14
1 .     dehydroisopenicillide
C21H22O6     相似度:81.8%
Phytochemistry          1991          30          2096-2098
Penicillide and dehydroisopenicillide from Talaromyces derxii
Kazumi Suzuki, Koohei Nozawa, Shun-ichi Udagawa, Shoichi Nakajima, Ken-ichi Kawai
Structure      13C NMR   碳谱模拟图

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2 .     Methyl 2-[1-(4-phenoxyphenoxy)propan-2-yl]quinoline-6-carboxylate
C26H23NO5     相似度:72.7%
Heterocycles          2011          83          1649-1658
Synthesis of Fluorescence Pyriproxyfen Analogues as Juvenile Hormone Agonists
Hideki Abe, Akimi Sato, Shin-ichi Tokishita, Toshihiro Ohta, and Hisanaka Ito*
Structure      13C NMR   碳谱模拟图

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3 .     5,9,10-Trimethoxy-2-methyl-11H-benzofluorene-4,11-diol
C21H20O5     相似度:72.7%
Helvetica Chimica Acta          2011          94          578-591
Syntheses of Prekinamycin and a Tetracyclic Quinone from Common Synthetic Intermediates
Shingo Kimura, Satoshi Kobayashi, Takuya Kumamoto, Aki Akagi, Naomi Sato and Tsutomu Ishikawa
Structure      13C NMR   碳谱模拟图

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4 .     (E)-3-(2,3-dimethoxyphenyl)-1-[2-hydroxy-4-(3-methylbut-2-enyloxy)phenyl]prop-2-en-1-one
C22H24O5     相似度:69.5%
Bioorganic & Medicinal Chemistry          2011          19          7711-7719
Structure–activity relationships of chalcone analogs as potential inhibitors of ADP- and collagen-induced platelet aggregation
M. Vijaya Bhaskar Reddy, Wei-Jern Tsai, Keduo Qian, Kuo-Hsiung Lee, Tian-Shung Wu
Structure      13C NMR   碳谱模拟图

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5 .     5-((Benzo[d][1,3]dioxol-6-yl)methylene)-3-(4-methylpyridin-2yl)-2-(phenylimino)thiazolidin-4-one
C23H17N3O3S     相似度:68.1%
Molecules          2006          11          597-602
One-Pot Synthesis of 5-Arylidene-2-Imino-4-Thiazolidinones under Microwave Irradiation
Souad Kasmi-Mir, Ayada Djafri, Ludovic Paquin, Jack Hamelin and Mustapha Rahmouni
Structure      13C NMR   碳谱模拟图

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6 .     penicillide
C21H24O6     相似度:68.1%
Phytochemistry          1991          30          2096-2098
Penicillide and dehydroisopenicillide from Talaromyces derxii
Kazumi Suzuki, Koohei Nozawa, Shun-ichi Udagawa, Shoichi Nakajima, Ken-ichi Kawai
Structure      13C NMR   碳谱模拟图

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7 .     8-Benzyl-1-methyl-3-(phenylsulfonyl)-1,5,6,8-tetrahydro-2H-pyrrolo[3,4-h]quinolin-2-one
C25H22N2O3S     相似度:68.1%
Bioorganic & Medicinal Chemistry          2011          19          2326-2341
Pyrrolo[3,4-h]quinolinones a new class of photochemotherapeutic agents
Paola Barraja, Patrizia Diana, Alessandra Montalbano, Anna Carbone, Giampietro Viola,Giuseppe Basso, Alessia Salvador, Daniela Vedaldi, Francesco Dall’Acqua, Girolamo Cirrincione
Structure      13C NMR   碳谱模拟图

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8 .     Methyl 1-benzyl-2-[(2-methylthiazol-4-yl)methyl]-1H-benzoimidazole-5-carboxylate
C21H19N3O2S     相似度:68.1%
Archiv der Pharmazie          2011          2          78-83
Synthesis and Anti-Hepatitis B Virus Activity of a Novel Class of Thiazolylbenzimidazole Derivatives
Yu Luo, Jia-Ping Yao, Li Yang, Chun-Lan Feng, Wei Tang, Gui-Feng Wang, Jian-Pin Zuo,and Wei Lu
Structure      13C NMR   碳谱模拟图

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9 .     rac-11-Hydroxy-3-(1-hydroxy-3-methylbutyl)-4-methoxy-9-methyl-5H,7H-dibenzo[b,g] [1,5]dioxocin-5(7H)-one
C21H24O6     相似度:68.1%
Helvetica Chimica Acta          2012          95          626-635
A Convergent Approach to Dibenzodioxocinones: Synthesis of Racemic Penicillide
Chun-Lin Deng,Qiao Zhang,Lisong Fang,Xinsheng Lei,and Guoqiang Lin
Structure      13C NMR   碳谱模拟图

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10 .     methyl (E)-3-(2-benzyloxy-3-ethoxy)phenyl-2-(cyano-methyl)propenoate
C21H21NO4     相似度:68.1%
Journal of Heterocyclic Chemistry          2008          45          1701-1706
Application of the acetate of baylis-hillman adducts of salicylaldehydes in the synthesis of methyl 2-oxo-2,3-dihydrobenzooxepine-4-carboxylates
Sang-Hyun Ahn,Hee Nam Lim and Kee-Jung Lee
Structure      13C NMR   碳谱模拟图

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11 .     Compound 9a
C46H48N4O8S2     相似度:68.1%
Bioorganic & Medicinal Chemistry Letters          2010          20          6831-6835
Design, synthesis and reactivity of C2-symmetric azobenzene-based amino acid-bis(propargyl sulfones)
Debarati Mitra, Deb Ranjan Banerjee, Amit Kumar Das, Amit Basak
Structure      13C NMR   碳谱模拟图

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12 .     Compound 7a
C22H18D2O5     相似度:68.1%
Bioorganic & Medicinal Chemistry Letters          1995          5          51-54
Kinamycin biosytheesis. Synthesis, detection, and incorporation of kinobscurinone, a benzofluorenone
Steven J. Gould, Chris R. Melville
Structure      13C NMR   碳谱模拟图

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13 .     penicillide
    相似度:68.1%
Journal of Natural Medicines          2006          60          185-190
New penicillide derivatives isolated from Penicillium simplicissimum
Shin-ichirou Komai, Tomoo Hosoe, Takeshi Itabashi, Koohei Nozawa and Takashi Yaguchi, et al.
Structure      13C NMR   碳谱模拟图

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14 .     (2Z)-2-(10-cyano-2-isopropyl-1,2,3,4-tetrahydrobenzo-1,6-naphthyridin-1-yl)but-2-enedioate
C22H23N3O4     相似度:68.1%
Tetrahedron Letters          2005          46          1975-1979
Transformations of tetrahydrobenzo[1,6]naphthyridines and tetrahydropyrido[4,3-b]pyrimidines under the action of dimethyl acetylene dicarboxylate
Leonid G. Voskressensky, Tatiana N. Borisova, Innokenti S. Kostenev, Ilia V. Vorobiev, Alexey V. Varlamov
Structure      13C NMR   碳谱模拟图

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15 .     vermixocin A
C21H24O6     相似度:68.1%
The Journal of Antibiotics          1992          45          1268-1272
VERMIXOCINS A AND B, TWO NOVEL METABOLITES FROM Penicillium vermiculatum
B. PROKSA, D. UHRÍN, J. ADAMCOVÁ, J. FUSKA
Structure      13C NMR   碳谱模拟图

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16 .     methyl (E)-2-(tert-butoxycarbonylamino)-(1,2-dihydroacenaphthylen-5-yl)but-2-enoate
C22H25NO4     相似度:68.1%
European Journal of Organic Chemistry          2010                   464-475
Synthesis and Photophysical Studies of New Fluorescent Indole Derivatives Obtained from β-Bromodehydroamino Acids – Interaction with Fluoride Anions
Goreti Pereira, Elisabete M. S. Castanheira, Paula M. T. Ferreira and Maria-João R. P. Queiroz
Structure      13C NMR   碳谱模拟图

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17 .     (2E,2'E)-dibutyl 3,3'-[5-(4-tert-butylphenyl)thiophene-2,3-diyl]diacrylate
C28H37O4S     相似度:68.1%
Tetrahedron          2013          69          160-173
Synthesis of functionalized benzothiophenes and dibenzothiophenes by twofold Heck and subsequent 6π-electrocyclization reactions of 2,3-dibromothiophenes and 2,3-dibromobenzothiophenes
Serge-Mithérand Tengho Toguem, Imran Malik, Munawar Hussain, Jamshed Iqbal, Alexander Villinger, Peter Langer
Structure      13C NMR   碳谱模拟图

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18 .     1-{2-[1-(tert-Butoxycarbonyl)-1H-indol-3-yl]ethyl}-5-methyl-1,2,3,6-tetrahydropyridine 1-Oxide
C21H28N2O3     相似度:68.1%
European Journal of Organic Chemistry          2012                   1147-1157
Synthesis of the Indolic Pentacyclic Core of Manadomanzamine A Following Biogenetically Based Strategies
Lok-Hang Yan, Philippe Nuhant, Isabelle Sinigaglia, Yann Fromentin, Christian Marazano, Bernard Delpech and Erwan Poupon
Structure      13C NMR   碳谱模拟图

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19 .     11-(Benzyloxy)-3-(1-hydroxy-3-methylbut-3-en-1-yl)-4-methoxy-9-methyl-5H,7H-dibenzo[b,g][1,5]-dioxocin-5-one
C28H28O6     相似度:65.3%
Helvetica Chimica Acta          2012          95          626-635
A Convergent Approach to Dibenzodioxocinones: Synthesis of Racemic Penicillide
Chun-Lin Deng,Qiao Zhang,Lisong Fang,Xinsheng Lei,and Guoqiang Lin
Structure      13C NMR   碳谱模拟图

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20 .     isosalviamine C
C23H19NO4     相似度:65.2%
Journal of Natural Products          2006          69(1)          93-96
Abietane Diterpene Alkaloids from Salvia Yunnanensis
Fu-Wen Lin, Amooru G. Damu, and Tian-Shung Wu
Structure      13C NMR   碳谱模拟图
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