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haijiaotang银虫 (正式写手)
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[求助]
维谱求助
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求助以下数据的化合物： 化合物1：碳谱数据如下 202.4 ，171.3 ,167.1, 122.0 , 115.7, 104.5 , 84.6 , 78.0, 77.4 , 77.3, 75.6, 74.1 , 72.9 , 70.5, 70.0, 68.8, 62.6, 52.4 , 50.5, 48.5, 43.1 , 39.2 , 37.8, 34.8 , 32.3 , 32.2, 30.7, 30.5 , 27.9 , 24.5, 22.1, 21.9 , 21.6, 18.3 化合物2：碳谱数据如下 202.3, 171.3 , 167.1 , 121.9 , 104.0, 84.6 , 78.8 , 78.1, 77.3, 75.6 , 74.4 , 72.2 , 70.1 , 68.8 , 63.2, 52.3 , 50.5 , 48.5 , 43.1, 39.2, 37.7 , 34.8 , 32.4 , 32.2 , 30.7, 30.5 , 27.9, 24.5, 22.2, 22.0, 21.6 , 21.4, 18.3 |
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wm0629
铁杆木虫 (著名写手)
- 应助: 341 (大学生)
- 金币: 6381.8
- 红花: 3
- 帖子: 1962
- 在线: 77.9小时
- 虫号: 2217415
- 注册: 2013-01-01
- 性别: GG
- 专业: 中药炮制
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
haijiaotang(豆哥代发): 金币+15, 谢谢 2013-04-28 08:17:23
感谢参与，应助指数 +1
haijiaotang(豆哥代发): 金币+15, 谢谢 2013-04-28 08:17:23
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化合物1： 1 . fibraurecdyside A C34H56O12 相似度:79.4% Journal of Natural Products 2007 70 1930-1933 Cytochrome P3A4 Inhibitors and Other Constituents of Fibraurea tinctoria Chung-Ren Su,Yune-Fang Ueng, Nguyen Xuan Dung, M. Vijaya Bhaskar Reddy,and Tian-Shung Wu Structure 13C NMR 碳谱模拟图 2 . ecdysterone-3-O-β-D-glucopyranoside 相似度:79.4% Chinese Journal of Medicinal Chemistry 1998 8 199-200 New Phytoecdysterones from Rhaponticum uniflorum Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 3 . ecdysterone-3-O-β-D-glucopyranoside 相似度:79.4% Journal of Shenyang Pharmaceutical University 2000 17 58-59 Phytoecdysones of Rhaponticum uniflorum (L.) DC. Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 4 . 3-acetate β-ecdysterone C29H46O8 相似度:76.4% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 5 . 2-deoxycrustecdysone-3-O-β-d-glucopyra-noside C33H54O11 相似度:76.4% Chinese Chemical Letters 1991 2 13-14 PHYTOECDYSONES FROM THE ROOTS OF TINOSPORA CAPILLIPES CHUN QING SONG AND REN SHENG XU Structure 13C NMR 碳谱模拟图 6 . ponasteroside A 相似度:76.4% Journal of Natural Medicines 2009 63 215-219 A new ecdysteroside from Lygodium japonicum (Thunb.) Sw. Linxia Zhu, Guogang Zhang, Lijuan Chen, Shengchao Wang and Ping Li, et al. Structure 13C NMR 碳谱模拟图 7 . ecdysterone 22-O-β-D-glucopyranoside 相似度:76.4% Natural Product Research and Development 2002 14(1) 9-12 STUDY ON THE CHEMICAL CONSTITUENTS OF LYCHNIS CORONARIA DAI Hao-fu; LIU Yu-qing; DENG Shi-ming; TAN Ning-hua; ZHOU Jun Structure 13C NMR 碳谱模拟图 8 . Sileneoside G C39H64O17 相似度:74.3% Chemistry of Natural Compounds 1998 34 602-604 PItYTOECDYSTEROIDS OF PLANTS OF THE Silene GENUS. XIX. THE STRUCTURE OF SILENEOSIDE G Z. T. Sadykov and Z. Saatov Structure 13C NMR 碳谱模拟图 9 . 25-acetoxy-20-hydroxyecdysone-3-β-D-glucopyranoside. C35H56O13 相似度:74.2% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 10 . 3-O-β-D-glucopyranoside 2-deoxyecdysterone C33H54O11 相似度:73.5% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 11 . 3-O-β-D-glucopyranosyl-20-hydroxyecdysone C33H54O12 相似度:73.5% Natural Product Research 2005 19 245-251 Steroidal and Triterpenoidal saponins from the fruits of Diploclisia glaucescens U. L. B. Jayasinghe; B. A. I. S. Balasooriya; N. Hara; Y. Fujimoto Structure 13C NMR 碳谱模拟图 12 . 2β,3β,14α,20R,22R-pentahydroxy-24R-methyl-5β-cholest-7-en-6-one-3-O-β-D-glucopyranoside C34H55O11 相似度:73.5% Natural Product Research 2009 23 1284-1288 A new compound from Lygodium japonicum (Thunb.) Sw. Linxia Zhu; Guogang Zhang; Shengchao Wang; Li Li; Ping Li; Shihua Wu; Xiaoqiu Wang; Lijuan Chen; Chunyuan Pan; Wenzhen Mi Structure 13C NMR 碳谱模拟图 13 . ecdysterone 25-O-β-D-glucopyranoside 相似度:73.5% Phytochemistry 1988 27 1665-1668 Three ecdysteroid glycosides from Pfaffia iresinoides Nobushige Nishimoto,Yoshinori Shiobara,Shun-suke Inoue,Masumi Fujino,Tsunematsu Takemoto,Cheow Lin Yeoh,Fernando de Oliveira,Gokithi Akisue,Maria Kubota Akisue,Goro Hashimoto Structure 13C NMR 碳谱模拟图 14 . ecdysterone-25-O-β-D-glucopyranoside 相似度:73.5% Journal of Shenyang Pharmaceutical University 2000 17 194-197 Phytoecdysones of Rhaponticum uniflorum (L.) DC. Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 15 . ecdysteroside 相似度:71.7% Phytochemistry 1998 47 1233-1235 Ecdysteroside, a phytoecdysteroid from Silene tatarica U. A. Baltayev Structure 13C NMR 碳谱模拟图 16 . pterosterone-3-O-β-D-glucopyranoside C33H54O12 相似度:70.5% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 17 . 2-acetate β-ecdysterone C29H46O8 相似度:70.5% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 18 . 2, 3-acetonide β-ecdysterone C30H48O7 相似度:70.5% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 19 . 20-Hydroxyecdysone 2-β-D-glucopyranoside 相似度:70.5% Biochemical Systematics and Ecology 1997 25 255-261 20-Hydroxyecdysone 2-β-D-glucopyranoside from the seeds of Xerophyllum tenax Brenda Alison, Pensri Whiting, Satyajit D. Sarker, Laurence Dinan, Eric Underwood, Vladimiršik, Huw H. Rees Structure 13C NMR 碳谱模拟图 20 . 20-hydroxyecdysone-2,3-acetonide 相似度:70.5% Chinese Pharmaceutical Journal 2005 40 1537-1538 Study on chemical constitutes of Cyanotis arachnoidea TAN Cheng-yu, WANG Jin-hui, LI Xian, DU Yu-guang, BAI Xue-fang Structure 13C NMR 碳谱模拟图 21 . 20-hydroxyecdysone 2,3-acetonide 相似度:70.5% Journal of Shenyang Pharmaceutical University 2006 23 562-564 Isolation and structural modif ication of 20-hydroxyecdysone YAN Jing-yu, CHENG Mao-sheng, HE Yan, LI Xian Structure 13C NMR 碳谱模拟图 22 . E-2-deoxy-20-hydroxyecdysone 3-[4-(1-β-D-glucopyranosyl)]-caffeate 相似度:69.4% Molecules 2012 17 11598-11606 E- and Z-Isomers of New Phytoecdysteroid Conjugates from French Polynesian Microsorum membranifolium (Polypodiaceae) Fronds Raimana Ho, Jean-Pierre Girault, Phila Raharivelomanana and René Lafont Structure 13C NMR 碳谱模拟图 23 . scillarenin 3-O-β-D-glucopyranosyl-(1→4)-39-O-acetyl-α-L-rhamnopyranoside C38H54O14 相似度:68.4% Chemical & Pharmaceutical Bulletin 2001 49(3) 282-286 Bufadienolides and a New Lignan from the Bulbs of Urginea maritima Masaru IIZUKA, Tsutomu WARASHINA, and Tadataka NORO Structure 13C NMR 碳谱模拟图 24 . ecdysone-3-O-β-D-glucopyranoside C33H54O11 相似度:67.6% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 25 . 2-deoxyecdysterone 3-Acetate 相似度:67.6% Chemistry of Natural Compounds 1985 21 56-58 PHYTOECDYSTEROIDS OF PLANTS OF THE GENUS Silene.VIII. 2-DEOXYECDYSTERONE 3-ACETATE FROM Silene pvaemixta Z. Saatov, M. B. Gorovits,N. D. Abdullaev, B. Z. Usmanov, and N. K. Abubakirov Structure 13C NMR 碳谱模拟图 26 . 20-hydroxyecdysone 2,3-monoacetonide 相似度:67.6% Phytochemistry 1994 37 707-711 Ecdysteroids from the roots of Leuzea carthamoides Jaroslav Píš, Miloš Buděšínsky̌, Karel Vokáč, Věra Laudová, Juraj Harmatha Structure 13C NMR 碳谱模拟图 化合物2： 1 . 2-deoxycrustecdysone-3-O-β-d-glucopyra-noside C33H54O11 相似度:84.8% Chinese Chemical Letters 1991 2 13-14 PHYTOECDYSONES FROM THE ROOTS OF TINOSPORA CAPILLIPES CHUN QING SONG AND REN SHENG XU Structure 13C NMR 碳谱模拟图 2 . ponasteroside A 相似度:84.8% Journal of Natural Medicines 2009 63 215-219 A new ecdysteroside from Lygodium japonicum (Thunb.) Sw. Linxia Zhu, Guogang Zhang, Lijuan Chen, Shengchao Wang and Ping Li, et al. Structure 13C NMR 碳谱模拟图 3 . 3-acetate β-ecdysterone C29H46O8 相似度:81.8% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 4 . 20-Hydroxyecdysone 2-β-D-glucopyranoside 相似度:81.8% Biochemical Systematics and Ecology 1997 25 255-261 20-Hydroxyecdysone 2-β-D-glucopyranoside from the seeds of Xerophyllum tenax Brenda Alison, Pensri Whiting, Satyajit D. Sarker, Laurence Dinan, Eric Underwood, Vladimiršik, Huw H. Rees Structure 13C NMR 碳谱模拟图 5 . ecdysterone 22-O-β-D-glucopyranoside 相似度:81.8% Natural Product Research and Development 2002 14(1) 9-12 STUDY ON THE CHEMICAL CONSTITUENTS OF LYCHNIS CORONARIA DAI Hao-fu; LIU Yu-qing; DENG Shi-ming; TAN Ning-hua; ZHOU Jun Structure 13C NMR 碳谱模拟图 6 . fibraurecdyside A C34H56O12 相似度:79.4% Journal of Natural Products 2007 70 1930-1933 Cytochrome P3A4 Inhibitors and Other Constituents of Fibraurea tinctoria Chung-Ren Su,Yune-Fang Ueng, Nguyen Xuan Dung, M. Vijaya Bhaskar Reddy,and Tian-Shung Wu Structure 13C NMR 碳谱模拟图 7 . 3-O-β-D-glucopyranoside 2-deoxyecdysterone C33H54O11 相似度:78.7% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 8 . 3-O-β-D-glucopyranosyl-20-hydroxyecdysone C33H54O12 相似度:78.7% Natural Product Research 2005 19 245-251 Steroidal and Triterpenoidal saponins from the fruits of Diploclisia glaucescens U. L. B. Jayasinghe; B. A. I. S. Balasooriya; N. Hara; Y. Fujimoto Structure 13C NMR 碳谱模拟图 9 . ecdysterone-3-O-β-D-glucopyranoside 相似度:78.7% Chinese Journal of Medicinal Chemistry 1998 8 199-200 New Phytoecdysterones from Rhaponticum uniflorum Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 10 . ecdysterone-3-O-β-D-glucopyranoside 相似度:78.7% Journal of Shenyang Pharmaceutical University 2000 17 58-59 Phytoecdysones of Rhaponticum uniflorum (L.) DC. Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 11 . 25-acetoxy-20-hydroxyecdysone-3-β-D-glucopyranoside. C35H56O13 相似度:77.1% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 12 . 2β,3β,14α,20R,22R-pentahydroxy-24R-methyl-5β-cholest-7-en-6-one-3-O-β-D-glucopyranoside C34H55O11 相似度:76.4% Natural Product Research 2009 23 1284-1288 A new compound from Lygodium japonicum (Thunb.) Sw. Linxia Zhu; Guogang Zhang; Shengchao Wang; Li Li; Ping Li; Shihua Wu; Xiaoqiu Wang; Lijuan Chen; Chunyuan Pan; Wenzhen Mi Structure 13C NMR 碳谱模拟图 13 . pterosterone-3-O-β-D-glucopyranoside C33H54O12 相似度:75.7% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 14 . ecdysone-3-O-β-D-glucopyranoside C33H54O11 相似度:75.7% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 15 . 2-acetate β-ecdysterone C29H46O8 相似度:75.7% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 16 . ecdysterone 25-O-β-D-glucopyranoside 相似度:75.7% Phytochemistry 1988 27 1665-1668 Three ecdysteroid glycosides from Pfaffia iresinoides Nobushige Nishimoto,Yoshinori Shiobara,Shun-suke Inoue,Masumi Fujino,Tsunematsu Takemoto,Cheow Lin Yeoh,Fernando de Oliveira,Gokithi Akisue,Maria Kubota Akisue,Goro Hashimoto Structure 13C NMR 碳谱模拟图 17 . ecdysterone-25-O-β-D-glucopyranoside 相似度:75.7% Journal of Shenyang Pharmaceutical University 2000 17 194-197 Phytoecdysones of Rhaponticum uniflorum (L.) DC. Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 18 . 2, 3-acetonide β-ecdysterone C30H48O7 相似度:72.7% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 19 . 2-deoxyecdysterone 3-Acetate 相似度:72.7% Chemistry of Natural Compounds 1985 21 56-58 PHYTOECDYSTEROIDS OF PLANTS OF THE GENUS Silene.VIII. 2-DEOXYECDYSTERONE 3-ACETATE FROM Silene pvaemixta Z. Saatov, M. B. Gorovits,N. D. Abdullaev, B. Z. Usmanov, and N. K. Abubakirov Structure 13C NMR 碳谱模拟图 20 . limnantheoside B C32H52O10 相似度:72.7% Phytochemistry 1997 44 513-521 Ecdysteroid xylosides from Limnanthes douglasii Satyajit D. Sarker, Jean-Pierre Girault, René Lafont, Laurence N. Dinan Structure 13C NMR 碳谱模拟图 21 . Polypodine B 2-β-D-glucoside C33H54O13 相似度:72.7% Steroids 2011 76 1419-1424 Ecdysteroids from Polypodium vulgare L. András Simon, Attila Ványolós, Zoltán Béni, Miklós Dékány, Gábor Tóth, Mária Báthori Structure 13C NMR 碳谱模拟图 22 . pfaffiaglycoside C C33H54O11 相似度:72.7% Chemical & Pharmaceutical Bulletin 2010 58 690-695 Brazilian Natural Medicines. IV. New Noroleanane-Type Triterpene and Ecdysterone-Type Sterol Glycosides and Melanogenesis Inhibitors from the Roots of Pfaffia glomerata Seikou Nakamura, Gang Chen, Souichi Nakashima, Hisashi Matsuda, Yuehu Pei and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 23 . pterosterone 24-O-β-D-glucopyranoside C33H54O12 相似度:72.7% Phytochemistry 1988 27 1665-1668 Three ecdysteroid glycosides from Pfaffia iresinoides Nobushige Nishimoto,Yoshinori Shiobara,Shun-suke Inoue,Masumi Fujino,Tsunematsu Takemoto,Cheow Lin Yeoh,Fernando de Oliveira,Gokithi Akisue,Maria Kubota Akisue,Goro Hashimoto Structure 13C NMR 碳谱模拟图 24 . 20-hydroxyecdysone-2,3-acetonide 相似度:72.7% Chinese Pharmaceutical Journal 2005 40 1537-1538 Study on chemical constitutes of Cyanotis arachnoidea TAN Cheng-yu, WANG Jin-hui, LI Xian, DU Yu-guang, BAI Xue-fang Structure 13C NMR 碳谱模拟图 |
2楼2013-04-28 07:49:12