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liuminzhuo

木虫 (初入文坛)

[求助] 微谱求助,在线等

化合物1
102.66;107.94;113.35;136.07;145.45;149.16;160.00
化合物2
60.99;61.59;63.02;69.54;73.27;73.92;76.08;101.16;108.56;111.14;111.56;112.03;112.11;112.74;114.30;119.17;138.38;140.10;141.66;141.87;145.34;151.17;152.78;158.30;158.38;165.69
化合物3
28.93;30.60;35.34;39.05;39.32;39.49;42.64;46.10;63.07;63.53;64.35;68.72;70.19;72.27;72.59;73.58;73.66;74.10;76.34;76.56;89.84;93.76;104.28;104.72;104.79;104.86;108.60;108.72;108.84;112.95;114.68;114.80;114.88;124.06;124.12;124.25;135.79;141.93;142.90;145.42;145.53;147.18;147.26;164.33;168.54;168.79;171.53;171.61;171.78;172.30;174.98;175.05
打谱溶剂均为DMSO
多谢了。。。
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wm0629

铁杆木虫 (著名写手)

化合物3没有找到相似的。
艰难困苦,玉汝于成。
4楼2013-04-27 18:10:44
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wm0629

铁杆木虫 (著名写手)

【答案】应助回帖

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liuminzhuo: 金币+50 2013-04-27 19:15:30
化合物2:

1 .     4'-O-galloy-3,3'-di-O-methylellagic acid 4-O-β-D-xylopyranoside
C28H22O16     相似度:84.6%
Chemical & Pharmaceutical Bulletin          2008          56(6)          847-850
α-Glucosidase Inhibitors Ellagic Acid Derivatives with Immunoinhibitory Properties from Terminalia superba
Turibio Kuiate TABOPDA,Joseph NGOUPAYO, Jiawei LIU,Muhammad Shaiq ALI,Shamsun Nahar KHAN,Bonaventure Tchaleu NGADJUI,and Bang LUU
Structure      13C NMR   碳谱模拟图
2 .     3,3'-di-O-methylellagic acid-4'-O-β-D-xylopyranoside
C21H18O12     相似度:73.0%
China Journal of Chinese Materia Medica          2006          31          1503-1506
Studies on chemical constituents in roots of Euphorbia soongarica
SHI Xinhong, DU xiaohong, DU Xiaoli, KONG Lingyi
Structure      13C NMR   碳谱模拟图
3 .     3,3'-di-O-methylellagic acid-4-O-β-D-glucopyranoside
C22H20O13     相似度:73.0%
China Journal of Chinese Materia Medica          2006          31          1503-1506
Studies on chemical constituents in roots of Euphorbia soongarica
SHI Xinhong, DU xiaohong, DU Xiaoli, KONG Lingyi
Structure      13C NMR   碳谱模拟图
4 .     4-O-β-D-(xylopyranosyl)-3,3'-di-O-methylellagic acid
C21H18O12     相似度:73.0%
Natural Product Sciences          2006          12          125-128
Phenolic compounds from the Stems of Sapium japonicum
Kang, Shin-Jung; Hong, Seong-Su; Hwang, Bang-Yeon; Ro, Jai-Seup; Lee, Kyong-Soon; Towers, G.H.N.
Structure      13C NMR   碳谱模拟图
5 .     4-O-[β-D-xylopyranosyl]-3,3'-di-O-methylellagic acid
    相似度:73.0%
Phytochemistry          1990          29          251-256
Ellagic compounds from Diplopanax stachyanthus
Duc Do Khac,Sung Tran-Van,Angela Martha Campos,Jean-Yves Lallemand,Marcel Fetizon
Structure      13C NMR   碳谱模拟图
6 .     3,3',4-di-O-methyl ellagic acid-4'-O-β-D-glucopyranoside
    相似度:73.0%
Chinese Traditional and Herbal Drugs          2008          39          1612-1616
Chemical constituents of Discocleidion rufescens(Ⅲ)
ZHU Hua-xu; TANG Yu-ping; GONG Zhu-nan; MIN Zhi-da
Structure      13C NMR   碳谱模拟图
7 .     3,3',4-di-O-methyl ellagic acid-4'-O-β-D-xylopyranoside
    相似度:73.0%
Chinese Traditional and Herbal Drugs          2008          39          1612-1616
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ZHU Hua-xu; TANG Yu-ping; GONG Zhu-nan; MIN Zhi-da
Structure      13C NMR   碳谱模拟图
8 .     3,3'-di-O-methylellagic-4'-O-β-D-xylopyranoside
    相似度:73.0%
Journal of China Pharmaceutical University          2002          33          370-373
Ellagic Acid Derivatives from the Stem Bark of Sapium sebiferum
LIU Run-Hui; CHEN Li-li; KONG Ling-Yi
Structure      13C NMR   碳谱模拟图
9 .     3,3'-di-O-methylellagic acid-4'-O-β-D-glucopyranoside
    相似度:73.0%
Natural Product Research and Development          2009          21          73-75
Studies on the Chemical Constituents of Polygonum runcinatum Buch.-Ham.var.sinense Hemsl.
WANG Li-ning;XU Bi-xue; CAO Pei-xue; LIANG Guang-yi
Structure      13C NMR   碳谱模拟图
10 .     3,3'-di-O-methylellagic acid-4-O-β-D-glucopyranoside
    相似度:73.0%
Zeitschrift für Naturforschung C          2008          63          794-800
Identification of Ellagic Acid Derivatives in Methanolic Extracts from Qualea Species
A. L. M. Nasser, C. B. A. Carli, C. M. Rodrigues, D. C. G. Maia, I. Z. Carlos, M. N. Eberlin, C. A. Hiruma-Lima, and W. Vilegas
Structure      13C NMR   碳谱模拟图
11 .     3,3'-di-O-methylellagic acid-4'-O-β-D-glucopyranoside
    相似度:73.0%
Lishizhen Medicine and Materia Medica Research          2009          20          369-370
Chemical Studies on Fructus Polygoni Orientalis
HAO Ning; KANG Ting-guo; DOU De-qiang; ZHAI Yan-jun
Structure      13C NMR   碳谱模拟图
12 .     3,4'-di-Omethylellagic acid 3'-O-β-D-xylopyranoside
C21H18O12     相似度:69.2%
Chemical & Pharmaceutical Bulletin          2008          56(6)          847-850
α-Glucosidase Inhibitors Ellagic Acid Derivatives with Immunoinhibitory Properties from Terminalia superba
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Structure      13C NMR   碳谱模拟图
13 .     3,3',4'-Tri-O-methylellagic acid-4'-O-β-D-glucopyranoside
    相似度:69.2%
Chemistry of Natural Compounds          2007          43          125-127
ELLAGIC ACID DERIVATIVES FROM THE STEM BARK OF Dipentodon sinicus
Guan Ye, Hua Peng, Mingsong Fan,and Cheng-Gang Huang
Structure      13C NMR   碳谱模拟图
14 .     3,3'-Di-O-methylellagic acid-4'-O-β-D-glucopyranoside
    相似度:69.2%
Chemistry of Natural Compounds          2007          43          125-127
ELLAGIC ACID DERIVATIVES FROM THE STEM BARK OF Dipentodon sinicus
Guan Ye, Hua Peng, Mingsong Fan,and Cheng-Gang Huang
Structure      13C NMR   碳谱模拟图
15 .     compound 1
    相似度:69.2%
Archives of Pharmacal Research          2009          32          515-520
New anthracene glycosides from Rhodomyrtus tomentosa stimulate osteoblastic differentiation of MC3T3-E1 cells
Nguyen Huu Tung, Yan Ding, Eun Mi Choi, Phan Van Kiem and Chau Van Minh, et al.
Structure      13C NMR   碳谱模拟图
16 .     3,3',4'-O-trimethylellagicacid4-O-β-D-xyloside
    相似度:69.2%
Journal of Integrative Plant Biology          2005          47          251-256
Two New Triterpenoids from the Roots of Sanguisorba officinalis L.
Fan ZHANG, Tie-Jun FU, Shu-Lin PENG, Zhong-Rong LIU and Li-Sheng DING*
Structure      13C NMR   碳谱模拟图
17 .     3,3',4-tri-O-methylellagicacid-4'-O-β-D-glucopyranoside
    相似度:69.2%
Zeitschrift für Naturforschung C          2008          63          794-800
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Structure      13C NMR   碳谱模拟图
18 .     3,3'-di-O-methylellagic acid-4'-O-β-D-glucopyranoside
C22H20O13     相似度:69.2%
Records of Natural Products          2013          7          129-132
Chemical Constituents of Canarium subulatum and Their Anti-herpetic and DPPH Free Radical Scavenging Properties
Boonchoo Sritularak, Nopporn Boonplod, Vimolmas Lipipun and Kittisak Likhitwitayawuid
Structure      13C NMR   碳谱模拟图
19 .     3,3'-di-O-methylellagic acid 4-(5''-acetyl)- -l-arabinofuranoside
C23H20O13     相似度:65.3%
Phytochemistry          2001          57          1287-1291
An ellagic compound and iridoids from Cornus capitata root cultures
Norie Tanaka, Takashi Tanaka, Toshihiro Fujioka, Hiroko Fujii,Kunihide Mihashi, Koichiro Shimomura, Kanji Ishimaru
Structure      13C NMR   碳谱模拟图
20 .     stachyanthuside A
C21H18O3     相似度:65.3%
Journal of Asian Natural Products Research          2004          6          271-276
TWONEW ELLAGIC ACID GLYCOSIDES FROMLEAVES OF DIPLOPANAX STACHYANTHUS
XIAO-HONG YAN and YUE-WEI GUO
Structure      13C NMR   碳谱模拟图
21 .     3,3',4-tri-O-methylellagic acid-4'-O-β-D-glucopyranoside
C23H22O13     相似度:65.3%
China Journal of Chinese Materia Medica          2006          31          1503-1506
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SHI Xinhong, DU xiaohong, DU Xiaoli, KONG Lingyi
Structure      13C NMR   碳谱模拟图
22 .     3,3',4-tri-O-methyl ellagic acid-4'-O-β-D-glucopyranoside
    相似度:65.3%
Chinese Traditional and Herbal Drugs          2008          39          1612-1616
Chemical constituents of Discocleidion rufescens(Ⅲ)
ZHU Hua-xu; TANG Yu-ping; GONG Zhu-nan; MIN Zhi-da
Structure      13C NMR   碳谱模拟图
艰难困苦,玉汝于成。
3楼2013-04-27 18:05:15
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liuminzhuo

木虫 (初入文坛)

引用回帖:
4楼: Originally posted by wm0629 at 2013-04-27 18:10:44
化合物3没有找到相似的。

谢谢了,信号实在太多了
5楼2013-04-28 17:08:12
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