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haijiaotang银虫 (正式写手)
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[求助]
维谱求助
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该类化合物是甾体皂苷 碳谱数据如下： 202.2， 171.1， 167.0 ，121.1， 104.3， 84.4 ，77.8 ，77.2， 77.15， 75.5， 73.9 ，72.8 ，70.3， 69.8， 68.6， 62.5， 52.2， 50.3， 48.3， 43， 39.1， 37.7 34.6 ，32.1， 31.9， 30.6， 30.3， 29.8 ，27.8， 22.0 ，21.7， 21.4， 21.1， 18.1 。 用氘代吡啶溶解。 |
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2楼2013-04-19 22:45:24
mzp-0
木虫 (正式写手)
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haijiaotang: 金币+5, ★★★很有帮助, 非常谢谢，很有参考价值 2013-04-20 21:22:32
haijiaotang(豆哥代发): 金币+5, 谢谢 2013-05-29 15:30:47
感谢参与，应助指数 +1
haijiaotang: 金币+5, ★★★很有帮助, 非常谢谢，很有参考价值 2013-04-20 21:22:32
haijiaotang(豆哥代发): 金币+5, 谢谢 2013-05-29 15:30:47
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1 . ecdysterone-3-O-β-D-glucopyranoside 相似度:79.4% Chinese Journal of Medicinal Chemistry 1998 8 199-200 New Phytoecdysterones from Rhaponticum uniflorum Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 2 . ecdysterone-3-O-β-D-glucopyranoside 相似度:79.4% Journal of Shenyang Pharmaceutical University 2000 17 58-59 Phytoecdysones of Rhaponticum uniflorum (L.) DC. Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 3 . 3-acetate β-ecdysterone C29H46O8 相似度:76.4% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 4 . 2-acetate β-ecdysterone C29H46O8 相似度:73.5% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 5 . 3-O-β-D-glucopyranoside 2-deoxyecdysterone C33H54O11 相似度:73.5% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 6 . 2-deoxycrustecdysone-3-O-β-d-glucopyra-noside C33H54O11 相似度:73.5% Chinese Chemical Letters 1991 2 13-14 PHYTOECDYSONES FROM THE ROOTS OF TINOSPORA CAPILLIPES CHUN QING SONG AND REN SHENG XU Structure 13C NMR 碳谱模拟图 7 . ponasteroside A 相似度:73.5% Journal of Natural Medicines 2009 63 215-219 A new ecdysteroside from Lygodium japonicum (Thunb.) Sw. Linxia Zhu, Guogang Zhang, Lijuan Chen, Shengchao Wang and Ping Li, et al. Structure 13C NMR 碳谱模拟图 8 . ecdysone-3-O-β-D-glucopyranoside C33H54O11 相似度:70.5% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 9 . fibraurecdyside A C34H56O12 相似度:70.5% Journal of Natural Products 2007 70 1930-1933 Cytochrome P3A4 Inhibitors and Other Constituents of Fibraurea tinctoria Chung-Ren Su,Yune-Fang Ueng, Nguyen Xuan Dung, M. Vijaya Bhaskar Reddy,and Tian-Shung Wu Structure 13C NMR 碳谱模拟图 10 . 2, 3-acetonide β-ecdysterone C30H48O7 相似度:70.5% Acta Botanica Yunnanica 2000 22(3) 351-357 Phytoecdysones from Porana discifera ZHU Wei-Ming,YANG Xiao-Sheng,HE Hong-Ping,HAO Xiao-Jiang Structure 13C NMR 碳谱模拟图 11 . 2-deoxyecdysterone 3-Acetate 相似度:70.5% Chemistry of Natural Compounds 1985 21 56-58 PHYTOECDYSTEROIDS OF PLANTS OF THE GENUS Silene.VIII. 2-DEOXYECDYSTERONE 3-ACETATE FROM Silene pvaemixta Z. Saatov, M. B. Gorovits,N. D. Abdullaev, B. Z. Usmanov, and N. K. Abubakirov Structure 13C NMR 碳谱模拟图 12 . 20-Hydroxyecdysone 2-β-D-glucopyranoside 相似度:70.5% Biochemical Systematics and Ecology 1997 25 255-261 20-Hydroxyecdysone 2-β-D-glucopyranoside from the seeds of Xerophyllum tenax Brenda Alison, Pensri Whiting, Satyajit D. Sarker, Laurence Dinan, Eric Underwood, Vladimiršik, Huw H. Rees Structure 13C NMR 碳谱模拟图 13 . 2β,3β,14α,20R,22R-pentahydroxy-24R-methyl-5β-cholest-7-en-6-one-3-O-β-D-glucopyranoside C34H55O11 相似度:70.5% Natural Product Research 2009 23 1284-1288 A new compound from Lygodium japonicum (Thunb.) Sw. Linxia Zhu; Guogang Zhang; Shengchao Wang; Li Li; Ping Li; Shihua Wu; Xiaoqiu Wang; Lijuan Chen; Chunyuan Pan; Wenzhen Mi Structure 13C NMR 碳谱模拟图 14 . 20-hydroxyecdysone-2,3-acetonide 相似度:70.5% Chinese Pharmaceutical Journal 2005 40 1537-1538 Study on chemical constitutes of Cyanotis arachnoidea TAN Cheng-yu, WANG Jin-hui, LI Xian, DU Yu-guang, BAI Xue-fang Structure 13C NMR 碳谱模拟图 15 . 20-hydroxyecdysone 2,3-acetonide 相似度:70.5% Journal of Shenyang Pharmaceutical University 2006 23 562-564 Isolation and structural modif ication of 20-hydroxyecdysone YAN Jing-yu, CHENG Mao-sheng, HE Yan, LI Xian Structure 13C NMR 碳谱模拟图 16 . ecdysterone 22-O-β-D-glucopyranoside 相似度:70.5% Natural Product Research and Development 2002 14(1) 9-12 STUDY ON THE CHEMICAL CONSTITUENTS OF LYCHNIS CORONARIA DAI Hao-fu; LIU Yu-qing; DENG Shi-ming; TAN Ning-hua; ZHOU Jun Structure 13C NMR 碳谱模拟图 17 . 25-acetoxy-20-hydroxyecdysone-3-β-D-glucopyranoside. C35H56O13 相似度:68.5% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 18 . 3-O-β-D-glucopyranosyl-20-hydroxyecdysone C33H54O12 相似度:67.6% Natural Product Research 2005 19 245-251 Steroidal and Triterpenoidal saponins from the fruits of Diploclisia glaucescens U. L. B. Jayasinghe; B. A. I. S. Balasooriya; N. Hara; Y. Fujimoto Structure 13C NMR 碳谱模拟图 19 . 26-hydroxypinnatasterone peracetylated 相似度:67.6% Fitoterapia 2001 72 215-220 Ecdysteroids from two Brazilian Vitex species Tereza C. dos Santos, Franco Delle Monache, Suzana G. Leitão Structure 13C NMR 碳谱模拟图 20 . Polypodine B 2-β-D-glucoside C33H54O13 相似度:67.6% Steroids 2011 76 1419-1424 Ecdysteroids from Polypodium vulgare L. András Simon, Attila Ványolós, Zoltán Béni, Miklós Dékány, Gábor Tóth, Mária Báthori Structure 13C NMR 碳谱模拟图 21 . ecdysterone 25-O-β-D-glucopyranoside 相似度:67.6% Phytochemistry 1988 27 1665-1668 Three ecdysteroid glycosides from Pfaffia iresinoides Nobushige Nishimoto,Yoshinori Shiobara,Shun-suke Inoue,Masumi Fujino,Tsunematsu Takemoto,Cheow Lin Yeoh,Fernando de Oliveira,Gokithi Akisue,Maria Kubota Akisue,Goro Hashimoto Structure 13C NMR 碳谱模拟图 22 . ecdysterone-25-O-β-D-glucopyranoside 相似度:67.6% Journal of Shenyang Pharmaceutical University 2000 17 194-197 Phytoecdysones of Rhaponticum uniflorum (L.) DC. Li Xiqiang, Wang Jinhui, Wang Suxian, Li Xian Structure 13C NMR 碳谱模拟图 23 . ecdysteroside 相似度:66.6% Phytochemistry 1998 47 1233-1235 Ecdysteroside, a phytoecdysteroid from Silene tatarica U. A. Baltayev Structure 13C NMR 碳谱模拟图 24 . lygodiumsteroside A C35H54O12 相似度:65.7% Journal of Natural Medicines 2009 63 215-219 A new ecdysteroside from Lygodium japonicum (Thunb.) Sw. Linxia Zhu, Guogang Zhang, Lijuan Chen, Shengchao Wang and Ping Li, et al. Structure 13C NMR 碳谱模拟图 25 . 2,22-dideoxy-20-hydroxyecdysone 25-O-β-D-glucopyranoside C33H54O10 相似度:64.7% Phytochemistry 2009 70 430-436 Ecdysteroids and a sucrose phenylpropanoid ester from Froelichia floridana Ping Wang, Shiyou Li, Stacy Ownby, Zhizhen Zhang, Wei Yuan, Wanli Zhang, R. Scott Beasley Structure 13C NMR 碳谱模拟图 26 . 2-O-acetylpolyporusterone A 相似度:64.7% Chemical & Pharmaceutical Bulletin 1992 40 143-147 Studies on Constituents of Fruit Body of Polyporus umbellatus and Their Cytotoxic Activity Takatomi OHSAWA,Masae YUKAWA,Chusei TAKAO,Mitsuo MURAYAMA and Hideo BANDO Structure 13C NMR 碳谱模拟图 27 . limnantheoside B C32H52O10 相似度:64.7% Phytochemistry 1997 44 513-521 Ecdysteroid xylosides from Limnanthes douglasii Satyajit D. Sarker, Jean-Pierre Girault, René Lafont, Laurence N. Dinan Structure 13C NMR 碳谱模拟图 28 . ajugasterone C-20,22-acetonide 相似度:64.7% Acta Pharmaceutica Sinica 2003 Vol 38 760-762 Chemical constituents of Cyanotis arachnoidea TAN Cheng yu; WANG Jin hui; LI Xian; DU Yu guang; BAI Xue fang Structure 13C NMR 碳谱模拟图 29 . pfaffiaglycoside C C33H54O11 相似度:64.7% Chemical & Pharmaceutical Bulletin 2010 58 690-695 Brazilian Natural Medicines. IV. New Noroleanane-Type Triterpene and Ecdysterone-Type Sterol Glycosides and Melanogenesis Inhibitors from the Roots of Pfaffia glomerata Seikou Nakamura, Gang Chen, Souichi Nakashima, Hisashi Matsuda, Yuehu Pei and Masayuki Yoshikawa Structure 13C NMR 碳谱模拟图 30 . blechnoside A 相似度:64.7% Phytochemistry 1986 25 1301-1304 Blechnosides A and B: Ecdysteroid glycosides from Blechnum minus Apichart Suksamrarn, John S. Wilkie, Denis H.S. Horn Structure 13C NMR 碳谱模拟图 31 . 2-deoxy-20-hydroxyecdysone 3-O-β-D-glucopyranoside 相似度:64.7% Chinese Traditional and Herbal Drugs 2010 41 689-692 Chemical constituents from roots of Tinospora sagittata var. yunnanensis CHENG Chun-mei; DAI Yun; HUANG Xiang-zhong; ZHU Yun; DAI Jian-hui; LIU Xiao-fang; WANG Jiong Structure 13C NMR 碳谱模拟图 32 . 20-hydroxyecdysone O-(2-chloropyridin-5-ylmethyl)oxime 相似度:64.7% Chemistry of Natural Compounds 2012 47 944-946 Synthesis of the O-(2-chloropyridin-5-ylmethyl)oxime of 20-hydroxyecdysone N. V. Kovganko, S. K. Ananich, S. N. Sokolov and Yu. G. Chernov Structure 13C NMR 碳谱模拟图 33 . Sileneoside G C39H64O17 相似度:64.1% Chemistry of Natural Compounds 1998 34 602-604 PItYTOECDYSTEROIDS OF PLANTS OF THE Silene GENUS. XIX. THE STRUCTURE OF SILENEOSIDE G Z. T. Sadykov and Z. Saatov Structure 13C NMR 碳谱模拟图 34 . oleandrigenin β-D-glucosyl-β-D-sarmentoside C38H58O14 相似度:63.1% Phytochemistry 1992 31 2459-2463 Cardenolide triosides of oleander leaves Fumiko Abe, Tatsuo Yamauchi Structure 13C NMR 碳谱模拟图 35 . subapinoside 相似度:62.1% Planta Medica 1991 57 159-161 Subalpinoside (Si), an Unknown Oleandrigenin Glycoside and Other Cardenolides from Digitalis subalpina var. subalpina J. I Lichius, D. ElKhyari und M.Wichtl Structure 13C NMR 碳谱模拟图 36 . adonitoxigenin-3-[O-α-L(3'-O-acetyl)rharnnosido-] β-D-glucosid 相似度:62.1% Planta Medica 1986 52 68-70 Neue Cardenolide aus Adonis vernalis C. Winkler, M. Wichtl Structure 13C NMR 碳谱模拟图 37 . 20-hydroxyecdysone 20,22-monoacetonide 相似度:61.7% Chemistry & Biodiversity 2008 Vol. 5 707 Ecdysteroids from Vitex Species: Distribution and Compilation of Their 28C-NMR Spectral Data José G. Sena Filho, Jennifer Duringer, Gabriela L. A. Maia, Josean F. Tavares, Haroudo S. Xavier, Marcelo Sobral da Silva, Em.dio V. L. da-Cunha, and José M. Barbosa-Filho Structure 13C NMR 碳谱模拟图 38 . pterosterone-3-O-β-D-glucopyranoside C33H54O12 相似度:61.7% Chemistry & Biodiversity 2007 Vol. 4 2225 Ecdysteroid Glycosides from Sida rhombifolia L. Atul N. Jadhav, Rahul S. Pawar, Bharathi Avula, and Ikhlas A. Khan Structure 13C NMR 碳谱模拟图 |
3楼2013-04-20 07:20:27