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我的化合物的碳谱数据如下：167.75,145.19,144.99,144.05,143.32,130.94,128.86,128.54,127.43,120.97,114.27,107.74,106.76,101.07,65.60,59.52,56.08,52.96,51.32,36.43,30.58,29.73,28.83,19.21,13.76 希望大神可以给出最像的结构式和相应的碳谱位移值，以及参考文献。 |
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【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
super0820: 金币+10, ★★★很有帮助 2013-04-22 11:53:41
感谢参与，应助指数 +1
super0820: 金币+10, ★★★很有帮助 2013-04-22 11:53:41
|
1 . (-)-canadine 相似度:60% Natural Product Research 1996 8 299-302 Insecticidal Alkaloid Against Drosophila Melanogaster from Tubers of Corydalis Bulbosa Mitsuo Miyazawa; Kimio Yoshio; Yukio Ishikawa; Hiromu Kameoka Structure 13C NMR 碳谱模拟图 2 . (-)-sinactine 相似度:60% Magnetic Resonance in Chemistry 2004 42 882-886 1H and 13C NMR signal assignment of benzylisoquinoline alkaloids from Fumaria officinalis L. (Papaveraceae) Christoph Seger, Sonja Sturm, Eva-Maria Strasser, Ernst Ellmerer and Hermann Stuppner Structure 13C NMR 碳谱模拟图 3 . 四氢表小檗碱 相似度:60% Chinese Traditional and Herbal Drugs 2009 40 193-196 青风藤化学成分的研究(Ⅱ) 黄筑艳;张援虎;周岚;李焱;杨小生 Structure 13C NMR 碳谱模拟图 4 . (±)-5,6,13,14-tetrahydro-9-hexanoyloxy-10-methoxy-2,3-(methylenedioxy)-8H-dibenzo[a,g]quinolizine 相似度:60% Bioorganic & Medicinal Chemistry 2013 21 62-69 Chemical and microbial semi-synthesis of tetrahydroprotoberberines as inhibitors on tissue factor procoagulant activity Hai-Xia Ge, Jian Zhang, Ling Chen, Jun-Ping Kou, Bo-Yang Yu Structure 13C NMR 碳谱模拟图 |
3楼2013-04-20 07:09:25
wm0629
铁杆木虫 (著名写手)
- 应助: 341 (大学生)
- 金币: 6381.8
- 红花: 3
- 帖子: 1962
- 在线: 77.9小时
- 虫号: 2217415
- 注册: 2013-01-01
- 性别: GG
- 专业: 中药炮制
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
super0820: 金币+10, ★★★很有帮助 2013-04-22 11:53:29
感谢参与，应助指数 +1
super0820: 金币+10, ★★★很有帮助 2013-04-22 11:53:29
|
1 . (-)-canadine 相似度:60% Natural Product Research 1996 8 299-302 Insecticidal Alkaloid Against Drosophila Melanogaster from Tubers of Corydalis Bulbosa Mitsuo Miyazawa; Kimio Yoshio; Yukio Ishikawa; Hiromu Kameoka Structure 13C NMR 碳谱模拟图 2 . (-)-sinactine 相似度:60% Magnetic Resonance in Chemistry 2004 42 882-886 1H and 13C NMR signal assignment of benzylisoquinoline alkaloids from Fumaria officinalis L. (Papaveraceae) Christoph Seger, Sonja Sturm, Eva-Maria Strasser, Ernst Ellmerer and Hermann Stuppner Structure 13C NMR 碳谱模拟图 3 . 四氢表小檗碱 相似度:60% Chinese Traditional and Herbal Drugs 2009 40 193-196 青风藤化学成分的研究(Ⅱ) 黄筑艳;张援虎;周岚;李焱;杨小生 Structure 13C NMR 碳谱模拟图 4 . (±)-5,6,13,14-tetrahydro-9-hexanoyloxy-10-methoxy-2,3-(methylenedioxy)-8H-dibenzo[a,g]quinolizine 相似度:60% Bioorganic & Medicinal Chemistry 2013 21 62-69 Chemical and microbial semi-synthesis of tetrahydroprotoberberines as inhibitors on tissue factor procoagulant activity Hai-Xia Ge, Jian Zhang, Ling Chen, Jun-Ping Kou, Bo-Yang Yu Structure 13C NMR 碳谱模拟图 5 . (-)-tetrahydroberberine 相似度:60% Bioorganic & Medicinal Chemistry 2013 21 856-868 Asymmetric total synthesis and identification of tetrahydroprotoberberine derivatives as new antipsychotic agents possessing a dopamine D1, D2 and serotonin 5-HT1A multi-action profile Haifeng Sun, Liyuan Zhu, Huicui Yang, Wangke Qian, Lin Guo, Shengbin Zhou, Bo Gao, Zeng Li, Yu Zhou, Hualiang Jiang, Kaixian Chen, Xuechu Zhen, Hong Liu Structure 13C NMR 碳谱模拟图 6 . (+)-tetrahydroberberine 相似度:60% Bioorganic & Medicinal Chemistry 2013 21 856-868 Asymmetric total synthesis and identification of tetrahydroprotoberberine derivatives as new antipsychotic agents possessing a dopamine D1, D2 and serotonin 5-HT1A multi-action profile Haifeng Sun, Liyuan Zhu, Huicui Yang, Wangke Qian, Lin Guo, Shengbin Zhou, Bo Gao, Zeng Li, Yu Zhou, Hualiang Jiang, Kaixian Chen, Xuechu Zhen, Hong Liu Structure 13C NMR 碳谱模拟图 7 . (-)-Tetrahydroberberine 相似度:60% Journal of Agricultural and Food Chemistry 1998 46 1914-1919 Insecticidal Alkaloids from Corydalis bulbosa against Drosophila melanogaster Mitsuo Miyazawa, Kimio Yoshio, Yukio Ishikawa, and Hiromu Kameoka Structure 13C NMR 碳谱模拟图 8 . methyl (1S,4aS,5R,6R,8aS)-5-[2-(1-benzyl-1H-pyrrol-3-yl)ethyl]-6-hydroxy-6-hydroxymethyl-1,4a-dimethyldecahydronaphthalene-1-carboxylate C28H39NO4 相似度:57.6% Russian Journal of Organic Chemistry 2008 44 67-75 Synthetic transformations of higher terpenoids: XVI. Synthesis of decahydronaphtho[1,2-g]indoles from lambertianic acid S. V. Chernov, E. E. Shul’ts, M. M. Shakirov and G. A. Tolstikov Structure 13C NMR 碳谱模拟图 9 . canadine 相似度:56% Phytochemistry 1990 29 3331-3339 Assignments of1H and13C NMR resonances of some isoquinoline alkaloids Richard H.A.M. Janssen,Peter Wijkens,Cor Kruk,Hubertus W.A. Biessels,Francesco Menichini,Hubert G. Theuns Structure 13C NMR 碳谱模拟图 10 . corypalmine 相似度:56% China Journal of Chinese Materia Medica 2010 35 1272-1275 Alkaloids in stems and leaves of Stephania cepharantha HE Li; ZHANG Yuanhu; TANG Lijia; SONG Shaohui; SUN Qianyun Structure 13C NMR 碳谱模拟图 11 . 2-[2-N-(3,4,5,6-tetrachlorophthalimido)ethoxymethyl]-3-ethoxycarbonyl-4-(o-chlorophenyl)-5-met-hoxycarbonyl-6-methyl-1,4-dihydropyridine C28H23N2O7Cl5 相似度:56% Heterocycles 2005 65 23-35 Mild, Selective and High-Yield Oxidation of Hantzsch 1,4-Dihydropyridines with Lead(IV) Acetate Mladen Litvic,* Ivica Cepanec, Mirela Filipan, Karmen Kos, Anamarija Bartolincic, Vinka Druskovic, Mohamed Majed Tibi, and Vladimir Vinkovic Structure 13C NMR 碳谱模拟图 12 . (±)-5,6,13,14-tetrahydro-9-acetoxy-10-methoxy-2,3-(methylenedioxy)-8H-dibenzo[a,g]quinolizine 相似度:56% Bioorganic & Medicinal Chemistry 2013 21 62-69 Chemical and microbial semi-synthesis of tetrahydroprotoberberines as inhibitors on tissue factor procoagulant activity Hai-Xia Ge, Jian Zhang, Ling Chen, Jun-Ping Kou, Bo-Yang Yu Structure 13C NMR 碳谱模拟图 13 . (+)-5,6,13,14-tetrahydro-9-β-D-glucosyl-10-methoxy-2,3-(methylenedi oxy)-8H-dibenzo[a,g]quinolizine 相似度:56% Bioorganic & Medicinal Chemistry 2013 21 62-69 Chemical and microbial semi-synthesis of tetrahydroprotoberberines as inhibitors on tissue factor procoagulant activity Hai-Xia Ge, Jian Zhang, Ling Chen, Jun-Ping Kou, Bo-Yang Yu Structure 13C NMR 碳谱模拟图 14 . 1' ,4' ,16,17-tetrahydro-3β-hydroxy-6' -bromo-4' -methyl-(16α,17α)-androsta-5,16-dieno[17,16-b]quinoline C27H36BrNO 相似度:53.8% Steroids 2004 69 301-312 Synthesis of novel steroid-tetrahydroquinoline hybrid molecules and -homosteroids by intramolecular cyclization reactions Angéla Magyar, János Wölfling, Melanie Kubas, Jose Antonio Cuesta Seijo, Madhumati Sevvana, Regine Herbst-Irmer, Péter Forgó, Gyula Schneider Structure 13C NMR 碳谱模拟图 15 . compound 5c 相似度:53.5% Heterocycles 2007 73 729-742 Lithium Bromide-Promoted Three-Component Synthesis of Oxa-Bridged Tetracyclic Tetrahydroisoquinolines Aude Fayol, Eduardo González-Zamora, Michèle Bois-Choussy, and Jieping Zhu Structure 13C NMR 碳谱模拟图 16 . (-)-scoulerine C19H21NO4 相似度:52% Chemistry & Biodiversity 2008 Vol. 5 1335 DNA Topoisomerase I Inhibitory Alkaloids from Corydalis saxicola Xuanxuan Cheng, Dongmei Wang, Lin Jiang, and Depo Yang Structure 13C NMR 碳谱模拟图 17 . actinodaphnine 相似度:52% Planta Medica 2002 68 1042-1044 Cytotoxic Aporphine Alkaloids from Cassytha filiformis C.Stévigny,S.Block,M.C.De Pauw-Gillet,E.de Hoffmann, G.Llabrès,V.Adjakidjé,J.Quetin-Leclercq Structure 13C NMR 碳谱模拟图 18 . compound 1 C20H20O6N2 相似度:52% Chinese Chemical Letters 2005 16 367-368 A New Nitro Alkaloid from Corydalis saxicola Bunting Hui Liang LI, Wei Dong ZHANG, Wei ZHANG, Chuan ZHANG, Run Hui LIU Structure 13C NMR 碳谱模拟图 19 . 4-(tert-Butyldiphenylsilyloxy)-3'-hydroxy-3,4',5-trimethoxy-(Z)-stilbene C33H36O5Si 相似度:52% Journal of Natural Products 2010 73 399-403 An Efficient Synthetic Strategy for Obtaining 4-Methoxy Carbon Isotope Labeled Combretastatin A-4 Phosphate and Other Z-Combretastatins George R. Pettit, Mathew D. Minardi, Fiona Hogan and Pat M. Price Structure 13C NMR 碳谱模拟图 20 . methyl chamigrenate 相似度:52% Phytochemistry 1995 38 651-653 Sesquiterpenes and a phenolic compound from the liverwort Omphalanthus filiformis Motoo Tori, Katsuyuki Nakashima, Yoshinori Asakawa Structure 13C NMR 碳谱模拟图 21 . (R)-6β-NH-Ts-7β-methoxy-7,8-dihydro disinomenine C52H66N4O10S2 相似度:52% Bioorganic & Medicinal Chemistry 2011 19 3096-3104 Synthesis and biological evaluation of unique stereodimers of sinomenine analogues as potential inhibitors of NO production Peng Teng,Hai-Liang Liu, Zhang-Shuang Deng, Zhi-Bing Shi ,Yun-Mian He , Li-Li Feng,Qiang Xu ,Jian-Xin Li Structure 13C NMR 碳谱模拟图 22 . compund 6b C26H22N4O5 相似度:52% Journal of Heterocyclic Chemistry 2008 45 1051-1055 Synthesis of some oxazolyl-pyrazolyl; 1,4-Dihydropyridinyl-pyrazolyl and 1,2,3,4-tetrahydro pyrimidinyl-pyrazolyl coumarins Mehul A. Patel and Dinker I. Brahmbhatt Structure 13C NMR 碳谱模拟图 |
2楼2013-04-19 18:39:27
4楼2013-04-22 20:23:43