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cai3575133金虫 (小有名气)
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[求助]
求助微谱数据，非常非常感谢
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化合物打谱溶剂为CDCl3。 化合物的碳谱数据：32.262, 110.155, 120.578, 122.951, 127.720, 128.460, 133.054, 135.602, 143.485, 170.077, 198.485 谢谢! |
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jasminelw
铁杆木虫 (正式写手)
- 应助: 269 (大学生)
- 金币: 8813.7
- 散金: 80
- 红花: 6
- 帖子: 972
- 在线: 604.2小时
- 虫号: 1858727
- 注册: 2012-06-13
- 专业: 天然有机化学
【答案】应助回帖
★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★ ★
感谢参与，应助指数 +1
cai3575133: 金币+15, ★有帮助, 好像都不是很准呀 2013-04-16 16:59:35
cai3575133(豆哥代发): 金币+10, 谢谢 2013-05-29 15:36:06
感谢参与，应助指数 +1
cai3575133: 金币+15, ★有帮助, 好像都不是很准呀 2013-04-16 16:59:35
cai3575133(豆哥代发): 金币+10, 谢谢 2013-05-29 15:36:06
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1 . (3E)-4-(furan-2-yl)-1-phenylbut-3-en-1-one C14H12O2 相似度:75% Indian Journal of Chemistry 2010 49B 573-577 Titanocene(III) chloride mediated reductive cleavage of arylcyclopropyl ketones M Paira,S K Mandal & S C Roy Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 2 . 5-chloro-3-hydroxy-1-methyl-2-oxo-3-trifluoromethylindole 相似度:72.7% Journal of Heterocyclic Chemistry 2008 45 969-972 Synthesis of new 3-(trifluoromethyl)-1H-indoles by reduction of trifluoromethyloxoindoles Moônica M. Bastos,Lúcia M. U. Mayer,Elza C. S. Figueira,Marcio Soares,Núbia Boechat and Warner B. Kover Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 3 . 2-(2-thienyl)benzimidazole 相似度:72.7% Heterocycles 2004 63 41-54 Indium-mediated Reductive Inter-molecular Coupling Reaction of 2-Nitroaniline with Aromatic Aldehydes to Benzimidazoles Byeong Hyo Kim,* Rongbi Han, Ji Sook Kim, Young Moo Jun, Woonphil Baik, and Byung Min Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 4 . 2-(3-thienyl)benzimidazole 相似度:72.7% Heterocycles 2004 63 41-54 Indium-mediated Reductive Inter-molecular Coupling Reaction of 2-Nitroaniline with Aromatic Aldehydes to Benzimidazoles Byeong Hyo Kim,* Rongbi Han, Ji Sook Kim, Young Moo Jun, Woonphil Baik, and Byung Min Lee Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 5 . 6-Methyl-1-phenyl-1H-benzotriazole C13H11N3 相似度:72.7% Helvetica Chimica Acta 2010 93 1350-1354 A Novel and Regiospecific Synthesis of 1-Aryl-1H-benzotriazoles via Copper(I)-Catalyzed Intramolecular Cyclization Reaction Qi-Lun Liu, Di-Di Wen, Chen-Chen Hang, Qiu-Lian Li and Yong-Ming Zhu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 6 . 2-(Thienoylethynyl)pyrrole C11H7NOS 相似度:72.7% Tetrahedron Letters 2004 45 6513-6516 Ethynylation of pyrroles with 1-acyl-2-bromoacetylenes on alumina: a formal ‘inverse Sonogashira coupling’ Boris A. Trofimov, Zinaida V. Stepanova, Lyubov’ N. Sobenina, Al’bina I. Mikhaleva, Igor A. Ushakov Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 7 . 4-[3-Oxo-(Z)-1-butenyl]-1-trityl-1H-pyrazole C26H22N2O 相似度:72.7% Heterocycles 2011 83 827-835 Heck-Mizoroki Reaction of 4-Iodo-1H-pyrazoles Yoshihide Usami,* Hayato Ichikawa, and Shinya Harusawa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 8 . 1-(phenylethynyl)benzotriazole C15H9N3 相似度:72.7% Heterocycles 2000 52 303-312 A Convenient Synthesis of New 1-Alkynyl-1H-benzotriazoles by Reaction of Alkynyl(phenyl)iodonium Salts with Benzotriazole Ion Tsugio Kitamura,* Norihiko Tashi, Kuniyuki Tsuda, Haiying Chen, and Yuzo Fujiwara* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 9 . 1-phenyl-1H-benzimidazole 相似度:72.7% European Journal of Organic Chemistry 2011 3353-3360 Cross-Coupling Reactions of Aryl Halides with Amines, Phenols, and Thiols Catalyzed by an N,N′-Dioxide–Copper(I) Catalytic System Haitao Yang, Chao Xi, Zhiwei Miao and Ruyu Chen Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 10 . 8-Chloro-4H-benzopyrazolo[1,5-d][1,4]diazepin-5(6H)-one C11H8ClN3O 相似度:72.7% Journal of Heterocyclic Chemistry 2012 49 221-226 Synthesis of novel benzopyrazolo[1,5]diazepines Joseph Raker, Yi Wang, Anthony D. Pechulis, James C. Haber, Michael A. Lynch and Stacey L. Spring Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 11 . bis(7-acetoxy-1-trifluoromethanesulfonylindol-6-yl)ethene C24H16N2O8F6S2 相似度:69.2% Heterocycles 2004 63 1839-1847 SnCl4-Promoted Ethenylation Reaction of Hydroxylated Heteroarenes Kensuke Akamatsu, Ryo Amemiya, and Masahiko Yamaguchi* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 12 . 3-Carboxy-2-methyl-1,10-phenanthroline C14H10N2O2 相似度:69.2% Archiv der Pharmazie 2006 339 201-206 In Vitro and in Vivo Antimalarial Activity of Derivatives of 1,10-Phenanthroline Framework Ange-Désiré Yapi, Alexis Valentin, Jean-Michel Chezal, Olivier Chavignon, Bernard Chaillot, Roseline Gerhardt, Jean-Claude Teulade and Yves Blache Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 13 . 1-[4-(1H-indazol-1-yl)phenyl]ethanone C15H12N2O 相似度:69.2% European Journal of Organic Chemistry 2011 4154-4159 Efficacy of C–N Coupling Reactions with a New Multinuclear Copper Complex Catalyst and Its Dissociation into Mononuclear Species Yan Zou, Haisheng Lin, Paul A. Maggard and Alexander Deiters Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 14 . harman 相似度:66.6% Chemical & Pharmaceutical Bulletin 1993 41 1169-1172 The 1H- and 13C-Nuclear Magnetic Resonance Spectra of Harman. Reinvestigation of the Assignments by One- and Two-Dimensional Methods Hiroko SEKI,Akihiro HASHIMOTO and Tohru HINO Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 15 . compound 1i 相似度:66.6% Chemical & Pharmaceutical Bulletin 1983 31 4172-4177 Electronic Properties of Anticonvulsant Amides. A C-13 Nuclear Magnetic Resonance Study of Phenylacetanilides CHISAKO YAMAGAMI,NARAO TAKAO and YOSHITO TAKEUCHI Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 16 . 1-(5-Methylfuran-2-yl)-3-(4-chlorophenyl)prop-2-en-1-one C15H14O2Cl 相似度:66.6% Archives of Pharmacal Research 2012 35 633-638 Design, Synthesis, and Anti-influenza Viral Activities of 1,3-Diarylprop-2-en-1-ones: A Novel Class of Neuraminidase Inhibitors Mayank Kinger, Yong Dae Park, Jeong Hoon Park, Min Goo Hur, Hyung Jae Jeong, Su-Jin Park,Woo Song Lee, Sang Wook Kim, and Seung Dae Yang Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 17 . 2-p-tolylbenzo[d]thiazole C14H11NS 相似度:66.6% Journal of Heterocyclic Chemistry 2006 43 1609-1612 Microwave-assisted “green” synthesis of 2-alkyl/arylbenzothiazoles in one pot: A facile approach to anti-tumor drugs Sukanta Kamila,Benjamin Koh and Edward R. Biehl Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 18 . 3-(benzotriazol-1-yl)-6-chloro-2H-indazole C13H8ClN5 相似度:66.6% Journal of Heterocyclic Chemistry 2010 47 98-111 n-Butyllithium-mediated reactions of 1-(2-azidoarylmethyl)- 1H-benzotriazoles with alkyl halides Taehoon Kim and Kyongtae Kim Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 19 . 3-(benzotriazol-1-yl)-5-chloro-2H-indazole C13H8ClN5 相似度:66.6% Journal of Heterocyclic Chemistry 2010 47 98-111 n-Butyllithium-mediated reactions of 1-(2-azidoarylmethyl)- 1H-benzotriazoles with alkyl halides Taehoon Kim and Kyongtae Kim Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 20 . 5-methyl-2-(4-nitrophenyl)benzoxazole C14H10N2O3 相似度:66.6% Heterocycles 2010 82 857-865 Simple Three Steps Synthesis of Potential Medicine for Metabolic Syndrome Kazuhiro Adachi, Kyosuke Michigami, and Masahiko Hayashi Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 21 . N-[5-(Carbazol-9-yl)-1-methyl-1H-imidazol-4-yl]acetamide C18H16N4O 相似度:66.6% Heterocycles 2007 71 2681-2688 Synthesis of 8-Substituted 12-Methyl-12H-imidazo[4', 5': 2, 3][1, 4]diazepino[6, 7, 1-jk]carbazoles Kayed A. Abu Safieh, Fouad H. Darras, Mikdad T. Ayoub, Mustafa M. El-Abadelah, Salim S. Sabri, and Wolfgang Voelter Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 22 . S-(benzoxazol-2-yl) thiobenzoate 相似度:66.6% Heterocycles 2004 62 313-324 Acylation and Alkoxycarbonylation of Benzoxazoline-2-thione and Benzothiazoline-2-thione Takehiko Nishio* and Kiyoko Shiwa Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 23 . (11aS)-1,10,11,11a-tetrahydro-5H-pyrrolo[2,1-c][1,4]benzodiazepine-5,11-dione C12H10N2O2 相似度:66.6% Heterocycles 2003 60 2023-2044 Approach to the Synthesis of (+)-Ifforestine. Model Studies Directed at the Tetracyclic Framework Gregory H. P. Roos* and Kim A. Dastlik Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 24 . 2-(1H-Benzimidazol-1-yl)-1-phenylethanone C15H12N2O 相似度:66.6% Bioorganic & Medicinal Chemistry Letters 2007 17 2233-2236 Synthesis and antimicrobial activity of some novel phenyl and benzimidazole substituted benzyl ethers Özden Özel Güven, Taner Erdoğan, Hakan Göker, Sulhiye Yıldız Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 25 . 1,3,5-tris(1,3-dithiole-2-ylidenephenylene)benzene 相似度:66.6% Tetrahedron Letters 2005 46 7871-7875 Probing the conformational changes upon oxidation in cross-conjugated architectures featuring vinylogous TTF units Rory Berridge, Peter J. Skabara, Raquel Andreu, Javier Garín, Jesús Orduna, Marta Torra Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 26 . t-Butyl3-acetoxy-4-dibromomethylbenzoate C14H16O4Br2 相似度:66.6% Bioorganic & Medicinal Chemistry 1994 2 757-771 Functionalized depsipeptides, substrates and inhibitors of β-lactamases and DD-peptidases D. Cabaret, J. Liu, M. Wakselman, R.F. Pratt, Y. Xub Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 27 . 2-(allylthio)-6-benzylpyrimidin-4(3H)-one C14H14N2OS 相似度:66.6% Bioorganic & Medicinal Chemistry 2010 18 3231-3237 Synthesis and biological evaluation of novel C5 halogen-functionalized S-DABO as potent HIV-1 non-nucleoside reverse transcriptase inhibitors Hua Qin, Chang Liu, Ying Guo, Ruiping Wang, Jianfang Zhang, Liying Ma, Zhili Zhang, Xiaowei Wang, Yuxin Cui, Junyi Liu Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 28 . (R)-3-methyl-7-(toluene-4-sulfinyl)-[1,2,3]triazolo-[1,5-a]pyridine C14H13N3OS 相似度:66.6% Tetrahedron 2007 63 10479-10485 Triazolopyridines. Part 25: Synthesis of new chiral ligands from [1,2,3]triazolo[1,5-a]pyridines Belén Abarca, Rafael Ballesteros, Rafael Ballesteros-Garrido, Françoise Colobert, Frédéric R. Leroux Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 29 . compound 1e C12H9BrO2 相似度:66.6% Indian Journal of Chemistry 2011 50B 593-604 Solvent free synthesis, spectral studies and antioxidant activities of some 6-substituted w-bromo-2-naphthyl ketones and their esters Thirunarayanan, G; Vanangamudi, G; Sathiyendran, V; Ravi, K Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 30 . N-benzylbenzimidazole 相似度:66.6% European Journal of Organic Chemistry 2011 2827-2835 Building Heterocyclic Systems with RC(OR)2+ Carbocations in Recyclable Brønsted Acidic Ionic Liquids: Facile Synthesis of 1-Substituted 1H-1,2,3,4-Tetrazoles, Benzazoles and Other Ring Systems with CH(OEt)3 and EtC(OEt)3 in [EtNH3][NO3] and [PMIM(SO3H)][O Gopalakrishnan Aridoss and Kenneth K. Laali Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 31 . 2-phenyl-6-vinyl-2,3,4,7-tetrahydrooxepine C14H16O1 相似度:66.6% European Journal of Organic Chemistry 2010 5232-5247 Ring-Closing of 1,7- and 1,8-Enynes of Propargylic O,O-Acetals by Ruthenium-Catalysed Intramolecular Metathesis Don Antoine Lanfranchi, Christophe Bour, Bastien Boff and Gilles Hanquet Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 32 . 3-(2-Hydroxy-6-oxocyclohex-1-enyl)isobenzofuran-1(3H)-one C14H12O4 相似度:66.6% Molecules 2013 18 1881-1896 Synthesis and Antiproliferative Activity of C-3 Functionalized Isobenzofuran-1(3H)-ones Róbson Ricardo Teixeira, Gustavo Costa Bressan, Wagner Luiz Pereira, Joana Gasperazzo Ferreira, Fabrício Marques de Oliveira and Deborah Campos Thomaz Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 33 . 1-[1-(3-Methoxybenzyl)-2-methyl-5-phenyl-1H-pyrrol-3-yl]ethanone C21H21NO2 相似度:64.2% Helvetica Chimica Acta 2009 92 2118-2124 Multicomponent Approach Towards the Synthesis of Substituted Pyrroles under Supramolecular Catalysis Using β-Cyclodextrin as a Catalyst in Water Under Neutral Conditions Sabbavarapu Narayana Murthy, Bandaru Madhav, Akkiligunta Vijay Kumar, Kakulapati Rama Rao, Yadavalli Venkata Durga Nageswar Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 34 . 1-Methyl-2-(3-chloro-6-nitrophenyl)benzimidazole 相似度:64.2% Bioorganic & Medicinal Chemistry 2011 19 2903-2910 2-Arylbenzothiazole, benzoxazole and benzimidazole derivatives as fluorogenic substrates for the detection of nitroreductase and aminopeptidase activity in clinically important bacteria Marie Cellier, Olivier J. Fabrega,Elizabeth Fazackerley, Arthur L. James ,Sylvain Orenga ,John D. Perry , Vindhya L. Salwatura, Stephen P. Stanforth Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 35 . compound 7 C20H17O4 相似度:64.2% Tetrahedron Letters 2000 41 7151-7155 Thalidomide metabolites and analogs. Part 2: Cyclic derivatives of 2-N-phthalimido-2S,3S (3-hydroxy) ornithine Frederick A. Luzzio, Elizabeth M. Thomas, William D. Figg Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 36 . (±)-5,6-dihydro-4H-indolo[3,2,1-de][1,5]naphthyridin-4-ol C14H12N2O 相似度:64.2% Journal of Heterocyclic Chemistry 2010 47 449-453 New polycyclic ring systems derived from canthin-4-one Andreas Puzik and Franz Bracher Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 37 . (R)-2-(1-(furan-3-yl)-3-oxo-3-phenylpropyl)malononitrile C16H14N2O2 相似度:64.2% Heterocycles 2009 79 573-582 Asymmetric Synthesis of 4-Substituted 2,6-Dioxopiperidine-3-carbonitrile by Using Thiourea-Catalyzed Asymmetric Michael Addition Tsubasa Inokuma, Yuuki Nagamoto, Shota Sakamoto, Hideto Miyabe, Kiyosei Takasu, and Yoshiji Takemoto Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 38 . 7,8-dihydro-6H-4a,5,11-triazabenzofluoren-9-one C14H11N3O 相似度:64.2% Heterocycles 2005 65 1121-1137 Synthesis of Polyfused Heterocycle Derivatives Containing the Dipyridoimidazole Core by Friedländer's Reaction: Access to Analogs of Ellipticine Nicolas Desbois, Jean-Michel Chezal, Florence Fauvelle, Jean-Claude Debouzy, Claire Lartigue, Alain Gueiffier, Yves Blache, Emmanuel Moreau, Jean-Claude Madelmont, Olivier Chavignon, and Jean-Claude Teulade* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 39 . 5-[4-(dipropylamino)phenyl]-10,20-diphenyl-15-propylporphyrin C47H45N5 相似度:64.2% Heterocycles 2005 65 2441-2450 One-pot Synthesis of A2BC-Type Free Base Porphyrins Yasser M. Shaker and Mathias O. Senge* Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- 40 . 2,3-dihydro-5-(2,3-dihydro-2-oxo-3-(2-pyridylmethyl)-1H-indol-3-yl)-3-(2-pyridylmethylene)-1H-indol-2-one C28H20N4O2 相似度:64.2% Archiv der Pharmazie 1996 329 541-549 Chemistry of Indoles Carrying a Basic Function,Part 31 Synthesis of Spiro[cyclopropane-1,3'[3H]indol]-2'(1'H)-ones with Antihypoxic Effects István Moldvai, Eszter Gács-Baitz, Mihály Balázs, Mária Incze and Csaba Szántay Structure 13C NMR 碳谱模拟图 -------------------------------------------------------------------------------- |
2楼2013-04-15 11:59:38