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Vogel's Textbook of Quantitative Chemical Analysis
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Author: G.H. Jeffery / J. Bassett / J. Mendham / R.C. Denney ISBN: 0582446937 Publisher: John Wiley & Sons Inc Edition: 5th edition (November, 1989) Reviewer: Ed Urbansky, (Cincinnati, Ohio) This book is a standard in the field of analytical chemistry, especially wet chemistry. It is not intended to be a textbook for a quant course, unlike Dan Harris's Quantitative Chemical Analysis or Doug Skoog's Fundamentals of Analytical Chemistry, which are both excellent college texts. However, it is an outstanding ready-reference for chemists and chemistry graduate students. It is the authority for all sorts of chemical analyses, and it gives concise, complete background along with exact procedures, including problems likely to be encountered, precautions to be taken, or deficiencies of the method. It is well-indexed and quite complete is breadth and scope. General Contents: Fundamentals of Quantitative Chemical Analysis - Introduction - Fundamental Theoretical Principles of Reactions in Solution - Common Apparatus and Basic Techniques -- Balances -- Graduated Glassware -- Water for Laboratory Use -- General Apparatus -- Reagents and Standard Solutions -- Some Basic Techniques Errors, Statistics and Sampling - Errors and Statistics - Sampling Separative Techniques - Solvent Extraction -- Some Applications - Ion Exchange -- Applications in Analytical Chemistry - Column and Thin-Layer Liquid Chromatography - Gas Chromatography Titrimetry and Gravimetric - Titrimetric Analysis -- Theoretical Considerations -- Neutralisation Titrations -- Complexation Titrations -- Determination of Individual Cations -- Analysis of Mixtures of Cations -- Determination of Anions -- Precipitation Titrations -- Oxidation-Reduction Titrations -- Oxidations with Potassium Permanganate -- Oxidations with Potassium Dichromate -- Oxidations with Cerium (IV) Sulphate Solution -- Oxidation and Reduction Processes Involving Iodine: Iodometric Titrations -- Oxidations with Potassium Iodate -- Oxidations with Potassium Bromate -- The Reduction of Higher Oxidation States - Gravimetry -- Quantitative Separations Based Upon Precipitation Methods -- Practical Gravimetric Analysis -- Cations -- Anions Electroanalytical Methods - Electro-Gravimetry - Conductimetry - Coulometry -- Coulometry at Constant Current: Coulometric Titrations - Potentiometry -- Reference Electrodes -- Indicator Electrodes -- Ion-Selective Electrodes -- Instrumentation and Measurement of Cell -- Direct Potentiometry -- Potentiometric Titrations - Voltammetry -- Polarography -- Direct Current Polarography -- Stripping Voltammetry -- Amperometry -- Titrations with the Rotating Platinum Micro-Electrode -- Biamperometric Titrations Spectroanalytical Methods - Colorimetry and Spectrophotometry -- Experimental Colorimetric Determinations -- Cations -- Anions -- Some Typical Organic Compounds -- Experimental Determinations with Ultraviolet/Visible Spectrophotometer -- Determinations by Spectrophotometric Titration -- Some Nephelometric Determinations - Spectrofluorimetry -- Experimental - Infrared Spectrophotometry - Atomic Emission Spectroscopy - Atomic Absorption and Flame Emission Spectroscopy -- Flame Spectroscopy -- Experimental -- Selected Determinations -- Atomic Absorption Experiments -- Flame Emission Experiments Appendices - Relative Atomic Masses, 1985 - Index of Organic Chemical Reagents Concentrations of Aqueous Solutions of the Common Acids and of Aqueous Ammonia - Saturated Solutions of Some Reagents at 20ºC - Sources of Analysed Samples - Buffer Solutions and Secondary pH Standards - Dissociation Constants of Some Acids in Water at 25ºC - Acidic Dissociation Constants of Some Bases in Water at 25ºC - Polarographic Half-Wave Potentials - Resonance Lines for Atomic Absorption - Electronic Absorption Characteristics of Some Common Chromophores - Characteristic Infrared Absorption Bands - Percentage Points of the t-Distribution - f-Distribution - Critical Values of Q (P=0.05) - Critical Values of the Correlation p (P=0.05) - Four-Figure Logarithms - Equivalents and Normalities |
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